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ASTM D4139-04

(Guide)

Standard Guide for Determining Volatile and Nonvolatile Content of Pigments

Standard Guide for Determining Volatile and Nonvolatile Content of Pigments

SIGNIFICANCE AND USE
The nonvolatile content of raw materials may be used to determine the total nonvolatile content (solids) of paint and related coatings. Such information may be useful to coatings producers and users for the determination of the total solids available for film formation and for the estimation of the volatile organic content.
SCOPE
1.1 This guide is intended to aid in the selection of the proper ASTM test method for determining the volatile and nonvolatile content of pigments.
Note 1—Test methods for determining the composition of the volatile fraction are not covered by this guide.
1.2 The standards included are as follows:StandardSectionASTM DesignationInert or low hiding pigmentsD 280White pigments   D 280 Black pigments D 280D 1509Aluminum and zinc pigmentsD 280 D 480Blue pigments D 280 D 1135Green pigments   D 280 Yellow, orange, brown pigmentsD 280D 3724 Red pigments D 280Miscellaneous

General Information

Status
Historical
Publication Date
31-May-2004
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.31 - Pigment Specifications
Current Stage
Ref Project

Relations

Replaces
ASTM D4139-82(1999) - Standard Guide for Determining Volatile and Nonvolatile Content of Pigments
Effective Date
01-Jun-2004
Replaced By
ASTM D4139-04(2009) - Standard Guide for Determining Volatile and Nonvolatile Content of Pigments
Effective Date
01-Jun-2009

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ASTM D4139-04 - Standard Guide for Determining Volatile and Nonvolatile Content of PigmentsASTM D4139-04 - Standard Guide for Determining Volatile and Nonvolatile Content of Pigments
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ASTM D4139-04 - Standard Guide for Determining Volatile and Nonvolatile Content of Pigments
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D4139–04
Standard Guide for
1
Determining Volatile and Nonvolatile Content of Pigments
This standard is issued under the fixed designation D 4139; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope related coatings. Such information may be useful to coatings
producers and users for the determination of the total solids
1.1 This guide is intended to aid in the selection of the
available for film formation and for the estimation of the
proper ASTM test method for determining the volatile and
volatile organic content.
nonvolatile content of pigments.
NOTE 1—Test methods for determining the composition of the volatile 4. Procedure
fraction are not covered by this guide.
4.1 Inert or Low Hiding Pigments:
1.2 The standards included are as follows:
4.1.1 Test Methods D 280 contain Method A for pigments
Standard Section ASTM Designation that do not decompose at 110°C, using a time of2hat105to
Inert or low hiding pigments 4.1 D 280
110°C, and Method B for pigments that decompose at 110°C,
White pigments 4.2 D 280
using vacuum to remove the volatile material.
Black pigments 4.3 D 280
D 1509 4.1.1.1 Test Methods D 280 are applicable to anhydrous and
Aluminum and zinc pigments 4.4 D 280
hydrous aluminum silicate, barium sulfate, calcium, borosili-
D 480
cate, calcium carbonate, diatomaceous silica, magnesium sili-
Blue pigments 4.5 D 280
D 1135 cate, pumice, and wet ground mica pigments for determination
Green pigments 4.6 D 280
ofhygroscopicmoistureandothermattervolatileunderthetest
Yellow, orange, brown pigments 4.7 D 280
conditions.
D 3724
Red pigments 4.8 D 280
4.2 White Pigments—Test Methods D 280 are applicable to
Miscellaneous 4.9
titanium dioxide, white lead, and zinc sulfide pigments.
4.3 Black Pigments:
2. Referenced Documents
4.3.1 Test Methods D 280 are applicable to synthetic black
2
2.1 ASTM Standards:
iron oxide pigment.
D 280 Test Methods for Hygroscopic Moisture (and Other
4.3.2 TestMethodsD 1509isusedtodetermineheatingloss
Matter Volatile Under the Test Conditions) in Pigments
in carbon black pigment.
D 480 Test Methods for Sampling and Testing of Flaked
4.4 Aluminum and Zinc Pigments:
Aluminum Powders and Pastes
4.4.1 Test Methods D 480 include the determination of
D 1135 Test Methods for Chemical Analysis of Blue Pig-
nonvolatile matter in aluminum paste.
ments
4.4.2 Test Methods D 280 are applicable to zinc dust (me-
D 1509 Test Methods for Carbon Black—Heating Loss
tallic zinc powder).
D 3724 Specification for Synthetic Brown Iron Oxide Pig-
4.5 Blue Pigments:
ment
4.5.1 Test Methods D 280 are applicable to copper phthalo-
cyanine blue and ultramarine blue pigments.
3. Significance and Use
4.5.2 Test Methods D 1135 include the determination of
3.1 The nonvolatile content of raw materials may be used to
moisture in iron blue pigments by the Brabender moisture
determine the total nonvolatile content (solids) of paint and
tester and by toluene distillation.
4.6 Green Pigments—Test Methods
...

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1.1 This specification covers UNS N06002, UNS N06030, UNS N06035, UNS N06022, UNS N06200, UNS N10362, UNS N06230, UNS N06600, UNS N06617, UNS N06625, UNS N08020, UNS N08026, UNS N08024, UNS N08120, UNS N08926, UNS N08367, UNS N10242, UNS N10276, UNS N10665, UNS N10675, UNS N12160, UNS R20033, UNS N06059, UNS N06686, UNS N10629, UNS N08031, UNS N06045, UNS N06025, UNS N06699, and UNS R305562 billets and bars for reforging.  
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