Standard Test Methods for Chemical Analysis of Aluminum and Aluminum-Base Alloys (Withdrawn 2017)

SIGNIFICANCE AND USE
These test methods for the chemical analysis of metals and alloys are primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
Note—Shaded areas are suitable for sampling. FIG. 1 Type A and Type B Disks
SCOPE
1.1 These test methods cover the chemical analysis of aluminum and aluminum-base alloys having compositions within the following limits:
Beryllium, ppm0.3 to 100 Bismuth, %0.02 to 1.0 Boron, %0.005 to 0.060 Cadmium, %0.001 to 0.50 Chromium, %0.01 to 1.0 Copper, %0.01 to 20.0 Gallium, %0.001 to 0.05 Iron, %0.01 to 3.0 Lead, %0.01 to 1.0 Lithium, %0.001 to 4.0 Magnesium, %0.002 to 12.0 Manganese, %0.005 to 2.0 Nickel, %0.01 to 4.0 Silicon, %0.05 to 20.0 Tin, %0.03 to 1.0 Titanium, %0.002 to 0.30 Vanadium, %0.002 to 0.16 Zinc, %0.003 to 12.0 Zirconium, %0.01 to 0.30
1.2 The analytical procedures appear in the following sections:
Procedure Sections Beryllium:  Beryllium by Argon Plasma Optical Emission
Spectroscopy283 to 292  Beryllium by the Morin (Fluorometric) Test
Method1e Bismuth:  Bismuth by the Thiourea (Photometric) Method1a  Bismuth and Lead by the Atomic Absorption
Test Method 188 to 198 Boron:  Boron by the Carmine (Photometric) Test Method1e Cadmium:  Cadmium by the Atomic Absorption Test Method167 to 177 Chromium:  Chromium by the Diphenylcarbazide (Photometric)
Test Method1e  Chromium by the Persulfate Oxidation (Titrimetric)
Test Method1b  Chromium by the Atomic Absorption Test Method199 to 209 Copper:  Copper and Lead by the Electrolytic (Gravimetric)
Test Method 1c  Copper and Zinc by the Atomic Absorption
Spectometry Test Method 210 to 220  Copper by the Electrolytic (Gravimetric) Test Method303 to 311  Copper by the Neocuproine (Photometric)
Test Method1a Gallium:  Gallium by the Ion Exchange-Atomic Absorption
Test Method 312 to 323 Iron:  Iron by the 1,10-Phenanthroline (Photometric) Method 73 to 81  Iron and Manganese by the Atomic Absorption
Spectometry Method221 to 231 Lead:  Copper and Lead by the Electrolytic (Gravimetric)
Test Method1 c  Bismuth and Lead by the Atomic Absorption
Spectrometry Test Method188 to 198 Lithium:  Lithium by the Atomic Absorption Test Method324 to 334 Magnesium:  Magnesium by the Pyrophosphate (Gravimetric)
Method1 b  Magnesium by the Ethylenediamine Tetraacetate
(Titrimetric) Test Method1 e  Magnesium by the Atomic Absorption Spectrometry
Test Method232 to 242 Manganese:  Iron and Manganese by the Atomic Absorption
Spectrometry Test Method221 to 231  Manganese by the Periodate (Photometric)
Test Method 293 to 302 Nickel:  Nickel by the Dimethylglyoxime (Photometric)
Test Method1a  Nickel by the Dimethylglyoxime (Gravimetric)
Test Method1b  Nickel by the Atomic Absorption Spectrometry
Test Method243 to 253 Silicon:  Silicon by the Molybdisilicic Acid (Photometric)
Test Method1 e  Silicon by the Sodium Hydroxide-Perchloric Acid
(Gravimetric) Method1 e Tin:  Tin by the Iodate (Titrimetric) Test Method1 e Titanium:  Titanium by the Chromotropic Acid (Photometric)
Test Method 141 to 150  Titanium by the Diantipyrylmethane Photometric
Test Method 254 to 263 Vanadium:  Vanadium by an Extraction-Photometric Test Method
using N-Benzoyl-N-Phenylhydroxylamine 264 to 273 Zinc:  Zinc by the Ammonium Mercuric Thiocyanate or the
Zinc Oxide (Gravimetric) Test Method1b  Zinc by the Ethylenediamine Tetraacetate
(Titrimetric) Test Method1d  Copper and Zinc by the Atomic Absorption
Spectrometry Test Method210 to 220  Zinc by the Ion Exchange-EDTA Titrimetric
Test Method274 to 282 Zirconium:  Zirconium by the Arsenazo III (Photometric) Method178 to 187
1.3 The values stated in SI units are to be regard...

General Information

Status
Withdrawn
Publication Date
30-Jun-2011
Current Stage
Ref Project

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ASTM E34-11e1 - Standard Test Methods for Chemical Analysis of Aluminum and Aluminum-Base Alloys (Withdrawn 2017)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation: E34 − 11
Standard Test Methods for
1
Chemical Analysis of Aluminum and Aluminum-Base Alloys
ThisstandardisissuedunderthefixeddesignationE34;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1
ε NOTE—Editorial changes were made throughout in August 2012.
1. Scope
Procedure Sections
1e
Boron by the Carmine (Photometric) Test Method
1.1 These test methods cover the chemical analysis of
Cadmium:
aluminum and aluminum-base alloys having compositions Cadmium by the Atomic Absorption Test Method 167 to 177
Chromium:
within the following limits:
1e
Chromium by the Diphenylcarbazide (Photometric)
Beryllium, ppm 0.3 to 100
Test Method
Bismuth, % 0.02 to 1.0 1b
Chromium by the Persulfate Oxidation (Titrimetric)
Boron, % 0.005 to 0.060
Test Method
Cadmium, % 0.001 to 0.50
Chromium by the Atomic Absorption Test Method 199 to 209
Chromium, % 0.01 to 1.0
Copper:
1c
Copper, % 0.01 to 20.0
Copper and Lead by the Electrolytic (Gravimetric)
Gallium, % 0.001 to 0.05
Test Method
Iron, % 0.01 to 3.0
Copper and Zinc by the Atomic Absorption 210 to 220
Lead, % 0.01 to 1.0
Spectometry Test Method
Lithium, % 0.001 to 4.0
Copper by the Electrolytic (Gravimetric) Test Method 303 to 311
Magnesium, % 0.002 to 12.0 1a
Copper by the Neocuproine (Photometric)
Manganese, % 0.005 to 2.0
Test Method
Nickel, % 0.01 to 4.0
Gallium:
Silicon, % 0.05 to 20.0
Gallium by the Ion Exchange-Atomic Absorption 312 to 323
Tin, % 0.03 to 1.0
Test Method
Titanium, % 0.002 to 0.30
Iron:
Vanadium, % 0.002 to 0.16
Iron by the 1,10-Phenanthroline (Photometric) Method 73 to 81
Zinc, % 0.003 to 12.0
Iron and Manganese by the Atomic Absorption 221 to 231
Zirconium, % 0.01 to 0.30
Spectometry Method
Lead:
1.2 The analytical procedures appear in the following sec-
1 c
Copper and Lead by the Electrolytic (Gravimetric)
tions:
Test Method
Bismuth and Lead by the Atomic Absorption 188 to 198
Procedure Sections
Spectrometry Test Method
Beryllium:
Lithium:
Beryllium by Argon Plasma Optical Emission 283 to 292
Lithium by the Atomic Absorption Test Method 324 to 334
Spectroscopy
1e Magnesium:
Beryllium by the Morin (Fluorometric) Test
1 b
Magnesium by the Pyrophosphate (Gravimetric)
Method
Method
Bismuth:
1 e
1a Magnesium by the Ethylenediamine Tetraacetate
Bismuth by the Thiourea (Photometric) Method
(Titrimetric) Test Method
Bismuth and Lead by the Atomic Absorption 188 to 198
Magnesium by the Atomic Absorption Spectrometry 232 to 242
Test Method
Test Method
Boron:
Manganese:
Iron and Manganese by the Atomic Absorption 221 to 231
Spectrometry Test Method
1
These test methods are under the jurisdiction of ASTM Committee E01 on
Manganese by the Periodate (Photometric) 293 to 302
Analytical Chemistry for Metals, Ores, and Related Materials and are the direct
Test Method
responsibility of Subcommittee E01.04 on Aluminum and Magnesium.
Nickel:
1a
Current edition approved July 1, 2011. Published August 2011. Originally Nickel by the Dimethylglyoxime (Photometric)
published as E34–60T. Last previous edition E34–94(Reapproved2002). DOI: Test Method
1b
Nickel by the Dimethylglyoxime (Gravimetric)
10.1520/E0034-11E01.
1a
Test Method
Discontinued as of Feb. 25, 1983.
1b
Nickel by the Atomic Absorption Spectrometry 243 to 253
Discontinued as of May 29, 1981.
1c
Test Method
Discontinued as of Oct. 25, 1985.
1d Silicon:
Discontinued as of March 25, 1983.
1e
Discontinued as of July 1, 2011.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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´1
E34−11
1 e
E1479Practice for Describing and Specifying Inductively-
Silicon by the Molybdisilicic Acid (Photometric)
Test Method
Coupled Plasma Atomic Emission Spectrometers
1 e
Silicon by the Sodium Hydroxide-Perchloric Acid
E1601Practice for Conducting an Interlaboratory Study to
(Gravimetric) Method
Tin: Evaluate the Performance of an Analytical Method
1 e
Tin by the Iodate (Titrimetric) Test Method
Titanium:
3. Terminology
Titanium by the Chromotropic Acid (Photometric) 141 to 150
Test Method
3.1 Definitions—For definitions of terms used in this test
Titanium by the Diantipyrylmethane Photometric 254 to 263
method, refer to Terminology E135.
Test Method
Vanadium:
Vanadium by an Extraction-Photometric Test Method 264 to 273
4. Significance and Use
using N-Benzoyl-N-Phenylhydroxylamine
Zinc: 4.1 These test methods for the chemical analysis of metals
1b
Zinc by the Ammonium Mercuric Thiocyanate or the
and alloys are primarily intended to test such mat
...

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