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ASTM E1728-99

(Practice)

Standard Practice for Field Collection of Settled Dust Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry Techniques

Standard Practice for Field Collection of Settled Dust Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry Techniques

SCOPE
1.1 This practice covers the collection of settled dusts on hard surfaces using the wipe sampling method. These samples are collected in a manner that will permit subsequent digestion and determination of lead using laboratory analysis techniques such as Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES), Flame Atomic Absorption Spectrometry (FAAS), and Graphite Furnace Atomic Absorption Spectrometry (GFAAS).  
1.2 This practice is used to collect samples for subsequent determination of lead on a loading basis (micrograms of lead per area sampled). This practice cannot be used to collect samples for subsequent determination of lead on a concentration basis (micrograms of lead per gram of settled dust collected).  
1.3 This practice is not intended for collection of settled dust samples from rough or porous surfaces such as upholstery and carpeting.  
1.4 This practice does not address the sampling design criteria (that is, sampling plan that includes the number and location of samples) that are used for risk assessment and other purposes. To provide for valid conclusions, sufficient numbers of samples must be obtained as directed by a sampling plan.  
1.5 This practice contains notes that are explanatory and are not part of the mandatory requirements of this practice.  
1.6 The values stated in SI units are to be regarded as the standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Dec-1999
ICS
13.080.05 - Examination of soils in general
Technical Committee
E06 - Performance of Buildings
Current Stage
Ref Project

Relations

Replaced By
ASTM E1728-02 - Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Lead Determination
Effective Date
10-Jun-2002

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ASTM E1728-99 - Standard Practice for Field Collection of Settled Dust Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry TechniquesASTM E1728-99 - Standard Practice for Field Collection of Settled Dust Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry Techniques
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ASTM E1728-99 - Standard Practice for Field Collection of Settled Dust Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry Techniques
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Standards Content (Sample)

Designation: E 1728 – 99
Standard Practice for
Field Collection of Settled Dust Samples Using Wipe
Sampling Methods for Lead Determination by Atomic
1
Spectrometry Techniques
This standard is issued under the fixed designation E 1728; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope using the same reagents and equipment.
2.1.2 field blank—a wipe that is exposed to the same
1.1 This practice covers the collection of settled dusts on
handling as field samples except that no sample is collected (no
hard surfaces using a wipe sampling method. These samples
surface is actually wiped). Analysis results from field blanks
are collected in a manner that will permit subsequent digestion
provide information on the analyte background level in the
and determination of lead using laboratory analysis techniques
wipe combined with the potential contamination experienced
such as Inductively Coupled Plasma Atomic Emission Spec-
by samples collected within the batch resulting from handling.
trometry (ICP-AES), Flame Atomic Absorption Spectrometry
2.1.3 sampling location—a specific area within a sampling
(FAAS), and Graphite Furnace Atomic Absorption Spectrom-
site that is subjected to sample collection. Multiple sampling
etry (GFAAS).
locations are commonly designated for a single sampling site.
1.2 This practice is used to collect samples for subsequent
2.1.4 sampling site—a local geographical area that contains
determination of lead on a loading basis (micrograms of lead
the sampling locations. A sampling site is generally limited to
per area sampled). This practice cannot be used to collect
an area that is easily covered by walking.
samples for subsequent determination of lead on a concentra-
2.1.5 wipe—disposable towelettes moistened with a wetting
tion basis (micrograms of lead per gram of settled dust
agent (see 2.1.5.1 and 2.1.5.2). These towelettes are used to
collected).
collect the sample and to clean sampling equipment. Wipe
1.3 This practice is not intended for collection of settled
brands or sources selected for use shall not contain significant
dust samples from rough or porous surfaces such as upholstery
background lead levels (see 2.1.5.1). Wipe brands or sources
and carpeting.
selected for use shall be of adequate width and thickness to
1.4 This practice does not address the sampling design
perform the collection procedure (see 2.1.5.2).
criteria (that is, sampling plan that includes the number and
2.1.5.1 Discussion 1— Laboratory analysis on replicate
location of samples) that are used for risk assessment and other
blank wipes should be used to determine background lead
purposes. To provide for valid conclusions, sufficient numbers
levels prior to use in the field. Brands of wipes that contain aloe
of samples must be obtained as directed by a sampling plan.
should be avoided due to increased potential of significant
1.5 This practice contains notes that are explanatory and are
background lead in these wipes. Background lead levels less
not part of the mandatory requirements of this practice.
than 5 μg per wipe are considered insignificant for most
1.6 The values stated in SI units are to be regarded as the
investigative purposes.
standard.
2.1.5.2 Discussion 2— A thin wipe having dimensions of
1.7 This standard does not purport to address all of the
approximately 15 by 15 cm is recommended. Use of multiple
safety concerns, if any, associated with its use. It is the
or extra-thick wipes can cause problems with laboratory
responsibility of the user of this standard to establish appro-
analysis activities. Use of wipes with smaller dimensions may
priate safety and health practices and determine the applica-
not be capable of holding settled dust contained within the
bility of regulatory limitations prior to use.
sampling area.
2. Terminology 2.1.6 wipe sampling kit—a sealable rigid walled container
with 50 mL minimum volume (see discussion below) and a
2.1 Definitions:
separate container of clean uncontaminated wipes for use in
2.1.1 batch—a group of field or quality control (QC)
collecting samples. One container of bulk packed wipes is
samples that are collected or processed together at the same site
typically used for collection of multiple samples.
2.1.6.1 Discussion—Use of a resealable plastic bag for
1
This practice is under the jurisdiction of ASTM Committee E-6 on Performance
holding and transporting the settled dust wipe sample is not
of Buildings and is the direct responsibility of Subcommittee E06.23 on Lead Paint
recommended due to the potential losses of settled dust within
Abatement.
Current edition approved Dec. 10, 1999. Published March 2000. Originally
published as ES 30 – 94. Last previous edition E 1728 – 95.
Copyright © ASTM, 100 Barr Harbor Dr
...

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Standard Test Method for Determination of Sediment Retention Device (SRD) Effectiveness in Sheet Flow Applications

SIGNIFICANCE AND USE
5.1 This test method quantifies the effectiveness of a sediment retention device (SRD) by measuring the ability of the SRD to retain eroded sediments caused by sheet flowing water under full-scale conditions. This test method may also assist in identifying physical attributes of SRDs that contribute to their erosion control performance.  
5.2 The effectiveness of SRDs is installation dependent. Thus, replicating field installation techniques is an important aspect of this test method. This test method is full-scale and therefore, appropriate as an indication of product performance, for general comparison of product capabilities, and for assessment of product installation techniques.
Note 1: Test Method D5141 is an alternate test method for evaluating sediment retention device effectiveness, if it is not necessary to simulate field installation conditions.
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors: Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method establishes the guidelines, requirements and procedures for evaluating the ability of Sediment Retention Devices (SRDs) to retain sediment when exposed to sediment-laden water “sheet” flows.  
1.2 This test method is applicable to the use of an SRD as a vertical permeable interceptor designed to remove suspended soil from overland, nonconcentrated water flow. The function of an SRD is to trap and allow settlement of soil particles from sediment laden water. The purpose is to reduce the transport of eroded soil from a disturbed site by water runoff.  
1.3 The test method presented herein is intended to indicate representative performance and is not necessarily adequate for all purposes in view of the wide variety of possible sediments and performance objectives.  
1.4 Units—The values stated in either SI units or inch-pound units [given in brackets] are to be regarded separately as standard. Only SI units are used in equations and appendixes. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.5 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.5.1 The procedures used to specify how data are collected/recorded and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any consideration for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established...

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ASTM
ASTM D5633-21(Practice)
Standard Practice for Sampling with a Scoop

SIGNIFICANCE AND USE
5.1 This practice is intended for use in collecting samples of contaminated soils and similar materials.  
5.2 Scoops are used primarily for collecting samples near the surface. Subsurface samples can be obtained by first removing higher layers using a shovel or other suitable equipment and collecting the sample with the scoop.  
5.3 Because of their simplicity, scoops are useful in taking samples of waste materials where decontamination or disposal is a problem with other types of sampling equipment. Scoops are also suitable for use in rapid screening programs, pilot studies, and other semi-quantitative investigations.  
5.4 Samples should be collected in accordance with an appropriate work plan (see Practice D5283 and Guide D4687).
SCOPE
1.1 This practice covers the method and equipment used to collect surface and near-surface samples of soils and physically similar materials using a scoop.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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