ASTM D5113-97
(Test Method)Standard Test Method for Determining Adhesive Attack on Rigid Cellular Foam
Standard Test Method for Determining Adhesive Attack on Rigid Cellular Foam
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1.1 This test method covers a practical means of measuring the degree of rigid cellular polystyrene (RCPS) foam cavitation damage when an adhesive is used to bond this substrate.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation:D5113–97
Standard Test Method for
Determining Adhesive Attack on Rigid Cellular Foam
This standard is issued under the fixed designation D 5113; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 5. Significance and Use
1.1 This test method covers a practical means of measuring 5.1 Rigid foam such as RCPS is used in the building
thedegreeofrigidcellularpolystyrene(RCPS)foamcavitation construction industry. Because it is sensitive to certain compo-
damage when an adhesive is used to bond this substrate. nents contained in adhesives which cause it to dissolve, it is
1.2 The values stated in inch pound units are to be regarded important to have a test method to determine whether an
as the standard. The values given in parentheses are for adhesive is compatible with RCPS foam. This test method
information only. would help the end user decide which adhesive to use with
1.3 This standard does not purport to address all of the RCPS foam by quantitatively measuring the amount of cavi-
safety concerns, if any, associated with its use. It is the tation formed by the components contained in the adhesive.
responsibility of the user of this standard to establish appro-
6. Apparatus
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. 6.1 Circular Template, with an inside diameter of 1.0 in.
(25.4 mm) and a depth of ⁄4 in. (6.3 mm).
2. Referenced Documents
6.2 Circulating Air Oven, for elevated temperature testing,
2.1 ASTM Standards: capable of being held at 40 6 1°C (104° 6 1.8°F).
C 578 Specification for Preformed, Cellular Polystyrene
7. Materials
Thermal Insulation
7.1 For the test, use Type IV RCPS foam with a nominal
D 907 Terminology of Adhesives
thickness of 1.0 in. (25.4 mm).
3. Terminology
7.2 If another type is used, record the type, thickness and
3.1 Definitions: density.
3.1.1 Many terms in this standard are defined in Terminol-
8. Conditioning
ogy D 907.
8.1 Unless otherwise agreed upon by the purchaser and the
3.2 Definitions of Terms Specific to This Standard:
3.2.1 cavitation damage, n—as related to rigid cellular manufacturer, condition the test specimen and adhesive 24 h
prior to testing at 23 6 1°C (73.4 6 1.8°F) and 50 6 5%
polystyrene foam, the pitting and wearing away of the surface.
3.2.1.1 Discussion—Damage may include loss of material, relative humidity.
surface deformation, or any other changes in microstructure,
9. Procedure
properties, or appearance.
9.1 Prepare enough specimens so that two assemblies are
3.3 Abbreviations:
tested at both temperatures.
3.3.1 RCPS—Rigid cellular polystyrene.
9.1.1 Foreachtest,cuttwosectionsofRCPSinto3in.(76.2
4. Summary of Test Method
mm) by 3 in. specimens.
4.1 This test method consists of testing two RCPS sections 9.1.2 Place the template in the center of one of the speci-
mens.
bonded by adhesive and allowed to set for 24 h. Before
evaluation, the degree of cavitation
...
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SIGNIFICANCE AND USE
5.1 Rigid foam such as RCPS is used in the building construction industry. Because it is sensitive to certain components contained in adhesives which cause it to dissolve, it is important to have a test method to determine whether an adhesive is compatible with RCPS foam. This test method would help the end user decide which adhesive to use with RCPS foam by quantitatively measuring the amount of cavitation formed by the components contained in the adhesive.
SCOPE
1.1 This test method covers a practical means of measuring the degree of rigid cellular polystyrene (RCPS) foam cavitation damage when an adhesive is used to bond this substrate.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is designed to produce tensile property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors that influence the tensile response and should be reported include the following: material, methods of material preparation and lay-up, specimen stacking sequence, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, time at temperature, and volume percent reinforcement. Properties, in the test direction, which may be obtained from this test method include the following:
5.1.1 Ultimate tensile strength,
5.1.2 Ultimate tensile strain,
5.1.3 Tensile modulus of elasticity, and
5.1.4 Poissons ratio.
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1.1 This test method covers the determination of the tensile properties of metal matrix composites reinforced by continuous and discontinuous high-modulus fibers. Nontraditional metal matrix composites as stated in 1.1.6 also are covered in this test method. This test method applies to specimens loaded in a uniaxial manner tested in laboratory air at either room temperature or elevated temperatures. The types of metal matrix composites covered are:
1.1.1 Unidirectional laminates (all fibers aligned in a single direction) containing either continuous or discontinuous reinforcing fibers. Both longitudinal and transverse properties may be obtained.
1.1.2 0°/90° balanced crossply laminates containing either continuous or discontinuous reinforcing fibers.
1.1.3 Angleply laminates containing continuous reinforcing fibers, with layups that do not include 0° reinforcing fibers (that is, (±45)ns, (±30)ns, and so forth).
1.1.4 Multidirectional laminates containing continuous reinforcing fibers, with layups including 0° reinforcing fibers (that is, (0/±45/90)ns quasi-isotropic laminates, (0/±30)ns laminates, and so forth).
1.1.5 Laminates containing unoriented and random discontinuous fibers.
1.1.6 Directionally solidified eutectic composites.
1.2 The technical content of this standard has been stable since 1996 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this standard, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards. The standard therefore should not be considered to include any significant changes in approach and practice since 1996. Future maintenance of the standard will only be in response to specific requests and performed only as technical support allows.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is suitable for quality control, as a specification test, and for research. The results are measures of batch-to-batch uniformity and are useful in estimating reactivity.
5.1.1 The percent nitrogen can be used to characterize a polyol or indicate amounts of certain components in a polyol blend.
5.1.2 It is permissible to also express the results in equivalents of base per gram of sample, if desired.
SCOPE
1.1 This test method measures the basic constituents in polyols that are soluble in glacial acetic acid and reactive with perchloric acid. Samples containing 0.3 % to 10 % nitrogen have been evaluated by this method. This test method is applicable to polyether polyols and polyether polyol blends that are used in urethane reactions. (See Note 1.)
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This standard is equivalent to ISO 25761:08.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Rigid gas-filled closed-cell foam insulations include all cellular plastic insulations which rely on a blowing agent (or gas), other than air, for thermal resistance values. At the time of manufacture, the cells of the foam usually contain their highest percentage of blowing agent and the lowest percentage of atmospheric gases. As time passes, the relative concentrations of these gases change due primarily to diffusion. This results in a general reduction of the thermal resistance of the foam due to an increase in the thermal conductivity of the resultant cell gas mixture. These phenomena are typically referred to as foam aging.
5.1.1 For some rigid gas-filled closed-cell foam insulation products produced using blowing agent gases that diffuse very rapidly out of the full-thickness foam product, such as expanded polystyrene, there is no need to accelerate the aging process.
5.1.2 Physical gas diffusion phenomena occur in three dimensions. The one-dimensional form of the diffusion equations used in the development of this practice are valid only for planar geometries, that is, for specimens that have parallel faces and where the thickness is much smaller than the width and much smaller than the length.
Note 3: Please see Appendix X3 for a discussion of the theory of accelerated aging via thin slicing.
Note 4: Theoretical and experimental evaluations of the aging of insulation in radial forms, such as pipe insulation, have been made. (6) However, these practices have not evolved to the point of inclusion in the test standard.
5.2 The change in thermal resistance due to the phenomena described in 5.1 usually occurs over an extended period of time. Information regarding changes in the thermal resistance of these materials as a function of time is required in a shorter period of time so that decisions regarding formulations, production, and comparisons with other materials can be made.
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1.1 This test method covers a procedure for predicting the long-term thermal resistance (LTTR) of unfaced or permeably faced rigid gas-filled closed-cell foam insulations by reducing the specimen thickness to accelerate aging under controlled laboratory conditions (1-5) .2
Note 1: See Terminology, 3.2.1, for the meaning of the word aging within this standard.
1.2 Rigid gas-filled closed-cell foam insulation includes all cellular plastic insulations manufactured with the intent to retain a blowing agent other than air.
1.3 This test method is limited to unfaced or permeably faced, homogeneous materials. This method is applied to a wide range of rigid closed-cell foam insulation types, including but not limited to: extruded polystyrene, polyurethane, polyisocyanurate, and phenolic. This test method does not apply to impermeably faced rigid closed-cell foams or to rigid closed-cell bun stock foams.
Note 2: See Note 8 for more details regarding the applicability of this test method to rigid closed-cell bun stock foams.
1.4 This test method utilizes referenced standard test procedures for measuring thermal resistance. Periodic measurements are performed on specimens to observe the effects of aging. Specimens of reduced thickness (that is, thin slices) are used to shorten the time required for these observations. The results of these measurements are used to predict the long-term thermal resistance of the material.
1.5 The test method is given in two parts. The Prescriptive Method in Part A provides long-term thermal resistance values on a consistent basis that can be used for a variety of purposes, including product evaluation, specifications, or product comparisons. The Research Method in part B provides a general relationship between thermal conductivity, age, and product thickness.
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ABSTRACT
This specification covers the standards for the types, physical properties and dimensions of cellular polystyrene boards with or without facings or coatings made by molding (EPS) or extrusion (XPS) of expandable polystyrene proposed for use as thermal insulation. This specification, however, does not cover laminated products manufactured with any type of rigid board facer including fiberboard, perlite board, gypsum board, or oriented strand board. All thermal insulation shall be of uniform density and shall contain sufficient flame retardants to meet the oxygen index of requirements. They shall also meet the physical requirements such as thermal resistance, compressive resistance, flexural strength, water vapor permeance, water absorption, dimensional stability, and oxygen index specified herein.
SCOPE
1.1 This specification2 covers the types, physical properties, and dimensions of cellular polystyrene boards with or without facings or coatings made by molding (EPS) or extrusion (XPS) of expandable polystyrene. Products manufactured to this specification are intended for use as thermal insulation for temperatures from –65 to +165°F (–53.9 to +73.9°C). This specification does not apply to laminated products manufactured with any type of rigid board facer including fiberboard, perlite board, gypsum board, or oriented strand board.
1.1.1 Additional requirements for Types IV and XIII for pipe, tank, and equipment thermal insulation for temperatures from –320 to +165°F (–196 to +73.9°C) are contained in Annex A1.
1.2 The use of thermal insulation materials covered by this specification is potentially regulated by codes that address fire performance. For some end uses, specifiers need to also address the effect of moisture and wind pressure resistance. Guidelines regarding these end use considerations are included in Appendix X1.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Tests made on materials herein prescribed have the potential to give considerable value in comparing physical properties of different materials, in controlling manufacturing processes, and as a basis for writing specifications.
5.2 Before proceeding with these test methods, if appropriate, make reference to the specification associated with the material or product being tested. Any test specimen preparation, conditioning, dimensions, testing parameters, or combination thereof, covered in the ASTM materials or product specification shall take precedence over those mentioned in these test methods. If there are no relevant ASTM specifications, then the default conditions apply.
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1.1 These test methods cover the preparation of a standard-size test sample and basic tests for physical property determinations of microcellular urethane materials.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This test method establishes standard procedure for determining the tensile and tensile adhesion properties of rigid cellular plastics in the form of test specimens of standard shape under defined conditions of temperature, humidity, and testing machine speed. Tensile properties shall be measured using any of three types of specimens: Type A shall be the preferred specimen in those cases where enough sample material exists to form the necessary specimen; Type B shall be the preferred specimen when only smaller specimens are available, as in sandwich panels, etc.; Type C shall be the preferred specimen for the determination of tensile adhesive properties of a cellular plastic to a substrate as in a sandwich panel or the bonding strength of a cellular plastic to a single substrate. This test method requires the use of the following apparatuses: a constant-rate-of-crosshead-movement type testing machine; self-aligning type grips for holding test specimens; an extension indicator; and a lathe specimen cutter.
SCOPE
1.1 This test method covers the determination of the tensile and tensile adhesion properties of rigid cellular materials in the form of test specimens of standard shape under defined conditions of temperature, humidity, and testing machine speed.
1.2 Tensile properties shall be measured using any of three types of specimens:
1.2.1 Type A shall be the preferred specimen in those cases where enough sample material exists to form the necessary specimen.
1.2.2 Type B shall be the preferred specimen when only smaller specimens are available, as in sandwich panels, etc.
1.2.3 Type C shall be the preferred specimen for the determination of tensile adhesive properties of a cellular plastic to a substrate as in a sandwich panel (top and bottom substrate) or the bonding strength of a cellular plastic to a single substrate.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
Note 1: There is no known ISO equivalent to this test method.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This test method provides information regarding the behavior of cellular materials under compressive loads. Test data is obtained, and from a complete load-deformation curve it is possible to compute the compressive stress at any load (such as compressive stress at proportional-limit load or compressive strength at maximum load) and to compute the effective modulus of elasticity.
4.2 Compression tests provide a standard method of obtaining data for research and development, quality control, acceptance or rejection under specifications, and special purposes. The tests cannot be considered significant for engineering design in applications differing widely from the load - time scale of the standard test. Such applications require additional tests such as impact, creep, and fatigue.
4.3 Before proceeding with this test method, reference shall be made to the specification of the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or a combination thereof, covered in the materials specification shall take precedence over those mentioned in this test method. If there are no material specifications, then the default conditions apply.
SCOPE
1.1 This test method describes a procedure for determining the compressive properties of rigid cellular materials, particularly expanded plastics.
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method and ISO 844 are technically equivalent.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification establishes the composition and physical properties of rigid polyimide cellular foams intended for use as thermal and sound-isolating insulation in commercial and industrial environments. The polyimide insulations covered are classified into three types (Types I, II, and III) according to closed cell content, and into four grades (Grades 1, 2, 3, and 4) according to density. Type II insulation is further divided into two classes (Classes 1 and 2) according to upper temperature limits. Materials shall be manufactured from the appropriate monomers and necessary ingredients. Specimens shall be sampled, tested, and conform accordingly to the following physical property requirements: apparent thermal conductivity; water and gas permeability; density; percent closed cell; upper temperature limit; high temperature stability; compressive strength; compressive force deflection; water vapor transmission; steam aging characteristics (tensile strength, dimensional and weight changes), corrosiveness; chemical resistance; vertical burn characteristics (flame application and time, burn length, and dripping); specific optical smoke density for both flaming and non-flaming exposures; toxic smoke generation; surface burning characteristics (flame spread and smoke developed indices); combustion by-products (carbon monoxide, hydrogen fluoride, hydrogen chloride, nitrogen oxides, sulfur dioxide, and hydrogen cyanide); oxygen index, and 14 scale room burn.
SCOPE
1.1 This specification covers the composition and physical properties of polyimide foam insulation with nominal densities from 1.0 lb/ft3 to 8.0 lb/ft3 (16 kg/m3 to 128 kg/m3) and intended for use as thermal and sound-isolating insulation for temperatures from −423°F to +600°F (−253°C to +316°C) in commercial and industrial environments.
1.1.1 The annex shall apply to this specification for marine applications.
1.1.2 This standard is designed as a material specification and not a design document.
1.1.3 The values stated in Table 1 and Table 2 are not to be used as design values. It is the buyer’s responsibility to specify design requirements and obtain supporting documentation from the material supplier.
* = Not available consult manufacturer for additional information.
NA = Not Applicable
NB = A manufacturer can only claim conformance to this standard to the values reported in this table. The * notes are confidential data to the manufacturers and as such are not considered part of any qualifying requirements for the standard and only tell the user to inquire about that data.
* = Not available consult manufacturer for additional information.
NA = Not Applicable
NB = A manufacturer can only claim conformance to this standard to the values reported in this table. The * notes are confidential data to the manufacturers and as such are not considered part of any qualifying requirements for the standard and only tell the user to inquire about that data.
Note 1: The subject matter of this material specification is not covered by any other ASTM specification. There is no known ISO standard covering the subject of this standard.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical B...
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SIGNIFICANCE AND USE
4.1 This practice facilitates the selection and application of an insulation system for use at service temperatures between − 30 and + 107°C (−22 and + 225°F). Although the successful installation of spray-applied PUR/PIR is influenced by many factors, this practice treats those four areas found to be of major importance:
(1) Substrate preparation,
(2) Substrate priming,
(3) Insulation application, and
(4) Protective coatings.
4.2 Abrasive blasting, primer application, spray application of the insulation, and protective coating application each contribute their unique health and safety hazards to the job site and will be dealt with in more detail under their respective headings.
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1.1 This practice concerns itself with the substrate preparation and priming, the selection of the rigid cellular polyurethane system, and the protective insulation coatings for outdoor service equipment.
Note 1: For the purpose of this practice, polyurethane is defined to mean either polyurethane or polyisocyanurate and is hereafter referred to as “PUR/PIR.”
1.2 The values given in inch-pound are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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