Standard Specification for Performance-Graded Trinidad Lake Modified Asphalt Binder

ABSTRACT
This specification covers the standards for graded Trinidad Lake modified asphalt binders. Grading is related to the average seven-day maximum pavement design temperature, the intermediate pavement design temperature, and the minimum pavement design temperature. The Trinidad Lake modified asphalt binder shall be prepared by adding the Trinidad Lake asphalt modifier to base asphalt produced from the refining of petroleum crude. The base asphalt binder shall be homogenous, and free from water or any deleterious materials.
SCOPE
1.1 This specification covers performance-graded Trinidad Lake modified asphalt binders. Grading designations are related to the average seven-day maximum pavement design temperature, °C, the intermediate pavement design temperature, °C, and minimum pavement design temperature, °C.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
30-Apr-2021
Current Stage
Ref Project

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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:D6626 −15 (Reapproved 2021)
Standard Specification for
Performance-Graded Trinidad Lake Modified Asphalt Binder
This standard is issued under the fixed designation D6626; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Film of Asphalt (Rolling Thin-Film Oven Test)
D4402/D4402M TestMethodforViscosityDeterminationof
1.1 This specification covers performance-graded Trinidad
Asphalt at Elevated Temperatures Using a Rotational
Lake modified asphalt binders. Grading designations are re-
Viscometer
lated to the average seven-day maximum pavement design
D6521 Practice for Accelerated Aging of Asphalt Binder
temperature, °C, the intermediate pavement design
Using a Pressurized Aging Vessel (PAV)
temperature, °C, and minimum pavement design temperature,
D6648 Test Method for Determining the Flexural Creep
°C.
Stiffness of Asphalt Binder Using the Bending Beam
1.2 The values stated in SI units are to be regarded as
Rheometer (BBR)
standard. No other units of measurement are included in this
D6723 Test Method for Determining the Fracture Properties
standard.
of Asphalt Binder in Direct Tension (DT) (Withdrawn
1.3 This international standard was developed in accor- 2021)
dance with internationally recognized principles on standard-
D7175 Test Method for Determining the Rheological Prop-
ization established in the Decision on Principles for the erties of Asphalt Binder Using a Dynamic Shear Rheom-
Development of International Standards, Guides and Recom-
eter
mendations issued by the World Trade Organization Technical D7553 Test Method for Solubility of Asphalt Materials in
Barriers to Trade (TBT) Committee.
N-Propyl Bromide
2. Referenced Documents
3. Terminology
2.1 ASTM Standards:
3.1 Definitions:
D8 Terminology Relating to Materials for Roads and Pave-
3.1.1 Definitions for many terms common to asphalt cement
ments
are found in Terminology D8.
D92 Test Method for Flash and Fire Points by Cleveland
Open Cup Tester
4. Ordering Information
D95 Test Method for Water in Petroleum Products and
4.1 When ordering under this specification, include in the
Bituminous Materials by Distillation
purchase order the grade of Trinidad Lake modified asphalt
D140/D140M Practice for Sampling Asphalt Materials
binder required from Table 1 (for example,TLG 52-16 orTLG
D1754/D1754M Test Method for Effects of Heat andAir on
64-34).
Asphaltic Materials (Thin-Film Oven Test)
D2170/D2170M Test Method for Kinematic Viscosity of
5. Materials and Manufacture
Asphalts
5.1 Trinidad Lake modified asphalt binder shall be prepared
D2171/D2171M Test Method for Viscosity of Asphalts by
by the addition of Trinidad Lake asphalt modifier to base
Vacuum Capillary Viscometer
asphalt produced from the refining of petroleum crude, with or
D2872 Test Method for Effect of Heat and Air on a Moving
without the inclusion of organic or inorganic modifiers.
5.2 Modifiers may be any suitable form of Trinidad Lake
This specification is under the jurisdiction of ASTM Committee D04 on Road
asphalt that may include also organic or inorganic modifiers of
and Paving Materials and is the direct responsibility of Subcommittee D04.40 on
suitable manufacture and preparation, and that is dissolved,
Asphalt Specifications.
dispersed, or reacted in asphalt cement to enhance its perfor-
Current edition approved May 1, 2021. Published May 2021. Originally
mance.
approved 2001. Last previous edition approved in 2015 as D6626 – 15. DOI:
10.1520/D6626-15R21.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6626−15 (2021)
TABLE 1 Performance-Graded Trinidad Lake Modified Asphalt Binder Specification
Performance Grade TLG 46- TLG 52- TLG 58- TLG 64- TLG 70- TLG 76- TLG 82-
34 40 46 10 16 22 28 34 16 22 28 34 40 10 16 22 28 34 40 10 16 22 28 34 10 16 22 28 34 10 16 22 28 34
40 46 40
Average 7-day Maximum <46 <52 <58 <64 <70 <76 <82
Pavement Design
Temperature, °C
Intermediate Temperature, °C 10 7 4 25 22 19 16 25 22 19 16 13 31 28 25 34 31 28 37 34 31 28 25 40 37 34 31 28
13 10 7 22 19 26 25 22 19
Minimum Pavement Design >–34 >–40 >–46 >–10 >–16 >–22 >–28 >–16 >–22 >–28 >–34 >–10 >–16 >–22 >–28 >–10 >–16 >–22 >–28 >–10 >–16 >–22 >–28 >–10 >–16 >–22 >–28
A
Temperature, °C >–34 >–40 >–46 >–40 >–34 >–40 >–34 >–40 >–34 >–34
Original Modified Asphalt Binder
Flash Point Temp, Test 230
Method D92;min °C
Solubility, Test Method 77–90
D7553,%
Viscosity, Test Method 135
B
D4402/D4402M: max, 3
Pas, Test Temp, °C
C
Dynamic Shear, D7175:
...


NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6626 − 15 (Reapproved 2021)
Standard Specification for
Performance-Graded Trinidad Lake Modified Asphalt Binder
This standard is issued under the fixed designation D6626; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Film of Asphalt (Rolling Thin-Film Oven Test)
D4402/D4402M Test Method for Viscosity Determination of
1.1 This specification covers performance-graded Trinidad
Asphalt at Elevated Temperatures Using a Rotational
Lake modified asphalt binders. Grading designations are re-
Viscometer
lated to the average seven-day maximum pavement design
D6521 Practice for Accelerated Aging of Asphalt Binder
temperature, °C, the intermediate pavement design
Using a Pressurized Aging Vessel (PAV)
temperature, °C, and minimum pavement design temperature,
D6648 Test Method for Determining the Flexural Creep
°C.
Stiffness of Asphalt Binder Using the Bending Beam
1.2 The values stated in SI units are to be regarded as
Rheometer (BBR)
standard. No other units of measurement are included in this
D6723 Test Method for Determining the Fracture Properties
standard.
of Asphalt Binder in Direct Tension (DT) (Withdrawn
1.3 This international standard was developed in accor-
2021)
dance with internationally recognized principles on standard- D7175 Test Method for Determining the Rheological Prop-
ization established in the Decision on Principles for the
erties of Asphalt Binder Using a Dynamic Shear Rheom-
Development of International Standards, Guides and Recom- eter
mendations issued by the World Trade Organization Technical
D7553 Test Method for Solubility of Asphalt Materials in
Barriers to Trade (TBT) Committee. N-Propyl Bromide
2. Referenced Documents
3. Terminology
2.1 ASTM Standards:
3.1 Definitions:
D8 Terminology Relating to Materials for Roads and Pave-
3.1.1 Definitions for many terms common to asphalt cement
ments
are found in Terminology D8.
D92 Test Method for Flash and Fire Points by Cleveland
Open Cup Tester
4. Ordering Information
D95 Test Method for Water in Petroleum Products and
4.1 When ordering under this specification, include in the
Bituminous Materials by Distillation
purchase order the grade of Trinidad Lake modified asphalt
D140/D140M Practice for Sampling Asphalt Materials
binder required from Table 1 (for example, TLG 52-16 or TLG
D1754/D1754M Test Method for Effects of Heat and Air on
64-34).
Asphaltic Materials (Thin-Film Oven Test)
D2170/D2170M Test Method for Kinematic Viscosity of
5. Materials and Manufacture
Asphalts
5.1 Trinidad Lake modified asphalt binder shall be prepared
D2171/D2171M Test Method for Viscosity of Asphalts by
by the addition of Trinidad Lake asphalt modifier to base
Vacuum Capillary Viscometer
asphalt produced from the refining of petroleum crude, with or
D2872 Test Method for Effect of Heat and Air on a Moving
without the inclusion of organic or inorganic modifiers.
5.2 Modifiers may be any suitable form of Trinidad Lake
This specification is under the jurisdiction of ASTM Committee D04 on Road asphalt that may include also organic or inorganic modifiers of
and Paving Materials and is the direct responsibility of Subcommittee D04.40 on
suitable manufacture and preparation, and that is dissolved,
Asphalt Specifications.
dispersed, or reacted in asphalt cement to enhance its perfor-
Current edition approved May 1, 2021. Published May 2021. Originally
mance.
approved 2001. Last previous edition approved in 2015 as D6626 – 15. DOI:
10.1520/D6626-15R21.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6626 − 15 (2021)
TABLE 1 Performance-Graded Trinidad Lake Modified Asphalt Binder Specification
Performance Grade TLG 46- TLG 52- TLG 58- TLG 64- TLG 70- TLG 76- TLG 82-
34 40 46 10 16 22 28 34 16 22 28 34 40 10 16 22 28 34 40 10 16 22 28 34 10 16 22 28 34 10 16 22 28 34
40 46 40
Average 7-day Maximum <46 <52 <58 <64 <70 <76 <82
Pavement Design
Temperature, °C
Intermediate Temperature, °C 10 7 4 25 22 19 16 25 22 19 16 13 31 28 25 34 31 28 37 34 31 28 25 40 37 34 31 28
13 10 7 22 19 26 25 22 19
Minimum Pavement Design >–34 >–40 >–46 >–10 >–16 >–22 >–28 >–16 >–22 >–28 >–34 >–10 >–16 >–22 >–28 >–10 >–16 >–22 >–28 >–10 >–16 >–22 >–28 >–10 >–16 >–22 >–28
A
Temperature, °C >–34 >–40 >–46 >–40 >–34 >–40 >–34 >–40 >–34 >–34
Original Modified Asphalt Binder
Flash Point Temp, Test 230
Method D92; min °C
Solubility, Test Method 77–90
D7553, %
Viscosity, Test Method 135
B
D4402/D4402M: max, 3
Pas, Test Temp, °C
C
Dynamic Shear, D7175: G*/ 46 52 58 64 70 76 82
sinδ, min, 1.00 kPa Test
Temp at 10 rad/s, °C
Rolling
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D6626 − 15 D6626 − 15 (Reapproved 2021)
Standard Specification for
Performance Graded Performance-Graded Trinidad Lake
Modified Asphalt Binder
This standard is issued under the fixed designation D6626; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers performance graded performance-graded Trinidad Lake modified asphalt binders. Grading
designations are related to the average seven-day maximum pavement design temperature, °C, the intermediate pavement design
temperature, °C, and minimum pavement design temperature, °C.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2.1 ASTM Standards:
D8 Terminology Relating to Materials for Roads and Pavements
D92 Test Method for Flash and Fire Points by Cleveland Open Cup Tester
D95 Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
D140D140/D140M Practice for Sampling Asphalt Materials
D1754D1754/D1754M Test Method for Effects of Heat and Air on Asphaltic Materials (Thin-Film Oven Test)
D2170D2170/D2170M Test Method for Kinematic Viscosity of Asphalts
D2171D2171/D2171M Test Method for Viscosity of Asphalts by Vacuum Capillary Viscometer
D2872 Test Method for Effect of Heat and Air on a Moving Film of Asphalt (Rolling Thin-Film Oven Test)
D4402D4402/D4402M Test Method for Viscosity Determination of Asphalt at Elevated Temperatures Using a Rotational
Viscometer
D6521 Practice for Accelerated Aging of Asphalt Binder Using a Pressurized Aging Vessel (PAV)
D6648 Test Method for Determining the Flexural Creep Stiffness of Asphalt Binder Using the Bending Beam Rheometer (BBR)
D6723 Test Method for Determining the Fracture Properties of Asphalt Binder in Direct Tension (DT) (Withdrawn 2021)
D7175 Test Method for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer
D7553 Test Method for Solubility of Asphalt Materials in N-Propyl Bromide
This specification is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.40 on Asphalt
Specifications.
Current edition approved Dec. 1, 2015May 1, 2021. Published January 2016May 2021. Originally approved 2001. Last previous edition approved in 20092015 as
D6626 – 09.D6626 – 15. DOI: 10.1520/D6626-15.10.1520/D6626-15R21.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
The last approved version of this historical standard is referenced on www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6626 − 15 (2021)
3. Terminology
3.1 Definitions:
3.1.1 Definitions for many terms common to asphalt cement are found in Terminology D8.
4. Ordering Information
4.1 When ordering under this specification, include in the purchase order the grade of Trinidad Lake modified asphalt binder
required from Table 1 (for example, TLG 52-16 or TLG 64-34).
5. Materials and Manufacture
5.1 Trinidad Lake modified asphalt binder shall be prepared by the addition of Trinidad Lake Asphaltasphalt modifier to base
asphalt produced from the refining of petroleum crude, with or without the inclusion of organic or inorganic modifiers.
5.2 Modifiers may be any suitable form of Trinidad Lake Asphaltasphalt that may include also organic or inorganic modifiers of
suitable manufacture and preparation, and that is dissolved, dispersed, or reacted in asphalt cement to enhance its performance.
5.3 The base asphalt binder shall be homogeneous, free from water and deleterious materials, and shall not foam when heated to
175 °C.175 °C.
5.4 The base asphalt binder shall be at least 99.0 % soluble in N-Propyl Bromide as determined by Test Method D7553.
5.5 The grades of asphalt binder shall conform to the requirements given in Table 1.
6. Sampling
6.1 The materials shall be sampled in accordance with Practice D140D140/D140M.
7. Test Methods
7.1 The properties outlined in 5.3 – 5.5 shall be determined in accordance with Practice D6521 and Test Methods D92, D95,
D1754D1754/D1754M, D2872, D4402D4402/D4402M, D6521, D6648, D6723, D7175, and D7553.
8. Inspection and Certification
8.1 Inspection and certification of the material shall be agreed upon between the purchaser and the seller. Specific requirements
shall be made part of the purchase contract.
9. Rejection and Rehearing
9.1 If the results of any test do not conform to the requirements of this specification, re-testingretesting to determine conformity
is performed as indicated in the purchase order or as otherwise agreed upon between the purchaser and the seller.
10. Keywords
10.1 asphalt binder; asphalt cement; direct tension; flash point; graded specifications; modifier; pressure aging; rheology;
Trinidadtrinidad lake asphalt
D6626 − 15 (2021)
TABLE 1 Performance Graded Performance-Graded Trinidad Lake Modified Asphalt Bi
...

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