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ASTM D5395-97

(Specification)

Standard Specification for Reclaimed Methylene Chloride

Standard Specification for Reclaimed Methylene Chloride

SCOPE
1.1 This specification covers the grade of methylene chloride typically needed in various industries for noncritical applications, such as in paint stripping formulations. It may be used as a reference document by purchasers or by persons establishing in-house methylene chloride recovery programs.

General Information

Status
Historical
Publication Date
09-May-1997
ICS
71.080.20 - Halogenated hydrocarbons
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.02 - Vapor Degreasing
Current Stage
Ref Project

Relations

Replaced By
ASTM D5395-03 - Standard Specification for Reclaimed Methylene Chloride
Effective Date
10-Jun-2003

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ASTM D5395-97 - Standard Specification for Reclaimed Methylene ChlorideASTM D5395-97 - Standard Specification for Reclaimed Methylene Chloride
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ASTM D5395-97 - Standard Specification for Reclaimed Methylene Chloride
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 5395 – 97
Standard Specification for
1,2
Reclaimed Methylene Chloride
This standard is issued under the fixed designation D 5395; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
TABLE 1 Physical Properties
1. Scope
Property Specification Test Method
1.1 This specification covers the grade of methylene chlo-
Specific gravity, 25/25 1.318 to 1.323 D 2111
ride typically needed in various industries for noncritical
Acidity, as HCl, ppm, max 1.0 D 2989
applications, such as in paint stripping formulations. It may be
Water, ppm, max 500 D 3401 or E1064
used as a reference document by purchasers or by persons
Appearance Clear and free from D 3741
suspended matter
establishing in-house methylene chloride recovery programs.
Color, Pt-Co, max 50 D 2108
Nonvolatile residue, ppm, max 50 D 2109
2. Referenced Documents
Chloride, ppm, max 1.0 D 2988
Assay, weight % 95.0 D 3447
2.1 ASTM Standards:
1,1,1-Trichloroethane content, 0.5 D 3447
D 2108 Test Method for Color of Halogenated Organic
weight %, max
Solvents and Their Admixtures (Platinum-Cobalt Scale)
D 2109 Test Methods for Nonvolatile Matter in Haloge-
taining Halogenated Organic Solvents
nated Organic Solvents and Their Admixtures
E 1064 Test Method for Water in Organic Liquids by
D 2111 Test Methods for Specific Gravity of Halogenated
Coulometric Karl Fischer Titration
Organic Solvents and Their Admixtures
D 2988 Test Method for Water-Soluble Halide Ion in Halo-
3. Properties
genated Organic Solvents and Their Admixtures
3.1 Reclaimed methylene chloride shall meet the require-
D 2989 Test Method for Acidity-Alkalinity of Halogenated
ments of Table 1.
Organic Solvents and Their Admixtures
D 3401 Test Methods for Water in Halogenated Organic
4. Packaging and Package Marking
Solvents and Their Admixtures
4.1 Industrial or commercial quantities shall be packaged
D 3447 Test Method for Purity of Trichlorotrifluoroe
...

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1.1 These test methods cover the determination of nonvolatile matter in halogenated organic solvents and admixtures.  
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1.2.2 Test Method B—For halogenated organic solvents or admixtures having more than 50 ppm nonvolatile matter or where precision of ±0.001 % (10 ppm) is satisfactory.  
1.2.3 Test Method C—For low-boiling halogenated organic solvents or their admixtures (for example, methylene chloride, trichlorotrifluoroethane) that may superheat and cause bumping while evaporating to dryness with steam. A precision of greater than ±10 ppm can be attained.  
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1.2.5 Test Method E—For halogenated organic solvents or admixtures and where precision better than ±10 ppm is required.  
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