This Technical Specification describes the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS). The method is applicable for a concentration range for PFOS in the extract solution of 0,5 μg/l to 50 μg/l.

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This Technical Specification describes the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS).
The method is applicable for a concentration range for PFOS in the extract solution of 0,5 µg/l to 50 µg/l.
WARNING - Persons using this Technical Specification should be familiar with normal laboratory practice. This Technical Specification does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions.
IMPORTANT - It is absolutely essential that tests conducted in accordance with this Technical Specification be carried out by suitably qualified staff.

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This document specifies the method for the determination of yield strength increase by the effect of heat treatment (Bake-Hardening-Index) for steel.
NOTE   This test is applied in particular, to steels showing a mechanism of bake hardening, which are specially intended for automotive industry.

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Specifies a method, the principle of which is based on evaporation of a test portion under specified conditions, using special apparatus, and weighing of the residue after evaporation. Details the procedure and provides information on the expression of results and the data to be included in the test report.

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Applicable to products the acidity of which is between 2 mol and 200 mol of univalent acid per kg. Two procedures are given: one is applicable to liquid products (R11, R113, etc.) and the other one to gaseous (R12, R22, etc.). The principle consists in extraction of the acids by water. Titration of the acids in the aqueous phase with standard volumetric sodium hydroxide solution in the presence of bromocresol green as indicator. A figure shows an apparatus for absorption of acids for products which are gaseous at ordinary temperatures.

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Applicable for sampling from containers (cylinders, drums, tanks, etc.). Sampling of the product in a steel cylinder, previously cleaned, dried and evacuated. The stainless steel cylinder shall be capable of withstanding an internal pressure of at least 3 MPa (30 bar). The cylinder is filled to the filling ratio allowed by the safety considerations. Details are given in the relevant international standards for the products considered. The samples shall be taken only from the liquefied phase. A diagram of the sampling assembly is shown in a figure.

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These methods are applicable to products not contaminated by an axtraneous phase (for example, water). Accidental pollution is also considered. Three cases are considered: small containers, large containers and continuous sampling. The procedure consists in formation of a blended bulk sample, representing the whole of the batch, by mixing several samples. The number and the method of taking of the elementary samples will depend on the number and capacity of containers.

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Covers a method applicable to products having water contents in the range between 2 and 100 mg/kg. Uses a principle consisting in the passage of a vaporized test portion through two weighed absoprtion tubes containing a phosphorus(V) oxide absorption mixture, and calculation of the water content from the increase in mass of the absorption tubes.

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Describes a method applicable to products having inert gas content equal to or greater than 0,005 % (V/V). The principle is based on detection of inert gas from test portion s taken from the liquid or gaseous phase and analysis under such conditions that none of the gases are retained irreversibly by the stationary phase.

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Establishes a standard layout for methods for the determination of volatile components and gives general information on these methods. Takes into account the general layout of methods of chemical analysis given in ISO 78/2 and the recommendations given in ISO 2718.

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Specifies a method, the principle of which is based on the analysis of a vaporzed test portion and determination of the contents of impurities. The calibration factors used for this determination are obtained by analysis of external methyl chloride calibration mixtures containing known quantities of the impurities under consederation.

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Covers a method permitting measurement of temperature differences of 0,5 °C. Should not be considered as an analytical method, but as a test for identification and indication of the purity of a product. Is based on evaporation by boiling of a known volume of the product under test and measurement of the temperatures corresponding to the evaporation of 5 and 95 % of the initial volume of the liquid.

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Specifies procedures for determining the acidity , the residue on evaporation and the water content by the Karl Fischer method. The acidity test is applicable to products having acidities, expressed as hydrochloric acid, between 1 and 50 mg/kg. For determination of ressidue on evaporation the method specified in ISO 2210 is recommended which is applicable to products leaving a residue on evaporation equal to or greater than 5 mg/kg. The method for determination of water content is applicable to products having water contents between 5 and 200 mg/kg.

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Specifies the sampling, the determination of ditillation characteristics, the determination of density at 20 °C, the determination of residue on evaporation, the determination of water and the determination of acidity. The determination of distillation characteristics indicates the difference between the temperatures corresponding to the collection of two volumes of distillate, V0 and V1. These two volumes will be indicated in the specification pf product agreed between th intersted parties. Replaces ISO Recommendation R 1697-1970.

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Specifies the sampling, the determination of distillation characteristics, the determination of density at 20 °C, the determination of water, the measurement of colour and the determination of acidity. The determination of distillation characteristics indicates either the temperatures corresponding to the collection of each of two volumes of distillate, V0 and V1, or the difference between these two volumes.These two volumes will be indicated in the specification of the product adreed between the interested parties. Replace ISO Recommendation R 1870-1970.

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Specifies the sampling, the determination of distillation characteristics, the determination of density at 20 °C, the determination of crystallizing point, the determination of residue on evaporation, the determination of water and the determination of acidity. The determination of distillation characteristics indicates the difference between the temperatures corresponding to the collection of two volumes of destillate, V0 and V1. These two volumes will be indicated in the specification of product agreed between the interested parties. Replaces ISO Recommendation R 1698-1970.

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Specifies the sampling, the determination of distillation characteristics, the determination of density at 20 °C, the determination of crystallizing point and the determination of p- and o-chlorotoluene content. The determination of distillation characteristics indicates the difference between the temperatures corresponding to the collection of two volumes of distillate, V0 and V1. These two volumes will be indicated in the specification of product agreed between the interested parties. For the determination of p-chlorotoluene, reading, from the crystallizing point diagram or from a table, of the p-chlorotoluene content corresponding to the crystallizing point of the sample. Replaces ISO Recommendation R 1695-1970.

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Specifies the sampling, the determination of distillation characteristics, the determination of density at 20 °C, the determination of crystallizing point and the determination of o- and p-chlorotoluene content. The determination of distillation characteristics indicates the difference between the temperatures corresponding to the collection of two volumes of distillate, V0 and V1. These two volumes will be indicated in the specification of product agreed between the interested parties. For the determination of o-chlorotoluene, reading, from the crystallizing point diagram or from a table, of the o-chlorotoluene content corresponding to the crystallizing point of the sample. Replaces ISO Recommendation R 1696-1970.

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Specifies the sampling, the determination of residue on evaporation, the determination of distillation characteristics, the determination of density at 20 °C, the determination of acidity, the determination of water and the measurement of colour. The determination of distillation characteristics indicates either the temperatures corresponding to the collection of each of two volumes of distillate, V0 and V1, or the difference between these two volumes. These two volumes will be indicated in the specification for dichloromethan agreed between the interested parties. Replaces ISO Recommendation R 1869-1970.

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Specifies a simple method for detecting the presence of certain impurities (generally water) which, dissolved at ambient temperature, cause the formation of cloudiness when the product is cooled to a sufficiently low temperature. The principle consists in determination of the temperature at which cloudiness appears in the clear sample, when it is gradually cooled under specified conditions. - Replaces ISO Recommendation R 1394-1970.

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The method does not apply when the halogenated materials hydrolyse at ambient temperature. The principle is based on the titration of the acidity of the aqueous extract from a test portion with a standard volumetric sodium hydroxide solution in the presence of bromocresol green as indicator. - Replaces ISO Recommendation R 1393-1970.

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Specifies the sampling, the determination of crystallizing point, the determination of residue on evaporation.

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Characterizes the product and gives the main impurities. Specifies methods for the determination of the crystallizing point and density and the procedure of the gas chromatographic analysis. Details the principle of determination of the product and its impurities, especially benzal chloride, benzaldehyde, toluene, chlorotoluene, etc., by the gaschromatography (relates to ISO 2818).

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Specifies the sampling, the determination of the distillation characteristics subjected to the modifications appropriate for this product, of the water content, of the density at 20 0C and of the crystallizing point. Has also been approved by the IUPAC.

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Specifies the sampling, the determination of distillation characteristics, of the density at 20 0C, of residue on evaporation, of the water content, of the acidity and the measurement of colour in Hazen units. Has also been approved by the IUPAC.

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The method specified can also be applied to other liquids behaving, in respect or evaporation, like halogenated hydrocarbons. The principle consists in evaporation of a test sample in a special apparatus in a platinum or borosilicate glass dish. Such an arrangement is shown in a figure. Weighing of the residue obtained after evaporation and drying at 110 °C to constant mass.

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The document specifies the sampling, the measurement of colour in Hazen units, determination of distillation characteristics, determination of density at 20 °C, determination of residue on evaporation, determination of water content, determination of the cloud point and the determination of carbon disulphide content. The principle of the CS2 determination is based on reaction of the carbon disulphide, in the presence of Cu(II) ions and diethylamine, to form copper diethyldithiocarbamate. This compound is soluble in the product which is tested giving a yellow colour the intensity of which is a function of the carbon disulphide content.

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