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ASTM D6509/D6509M-16(2023)

(Specification)

Standard Specification for Atactic Polypropylene (APP) Modified Bituminous Base Sheet Materials Using Glass Fiber Reinforcements

Standard Specification for Atactic Polypropylene (APP) Modified Bituminous Base Sheet Materials Using Glass Fiber Reinforcements

ABSTRACT
This specification covers prefabricated modified bituminous sheet materials with glass fiber reinforcement, which use atactic polypropylene (APP) as the primary modifier and which are intended for use as a base sheet in the fabrication of multiple ply roofing and waterproofing membranes. The high temperature stability and low temperature unrolling shall be tested to meet the requirements prescribed.
SCOPE
1.1 This specification covers prefabricated modified bituminous sheet materials with glass fiber reinforcement, which use atactic polypropylene (APP) as the primary modifier and which are intended for use as a base sheet in the fabrication of multiple ply roofing and waterproofing membranes.  
1.2 This is a material specification only. Issues regarding the suitability of specific roof constructions or application techniques are beyond the scope of this specification.  
1.3 The specified tests and property limits used to characterize the sheet materials covered by this specification are intended to establish minimum properties. In-place roof system design criteria, such as fire resistance, field strength, impact/puncture resistance, material compatibility, uplift resistance, the need for field applied coatings, and others, are factors beyond the scope of this material specification.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.5 The following precautionary statement pertains only to the test method portion, Section 8, of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Jan-2023
ICS
83.120 - Reinforced plastics
Technical Committee
D08 - Roofing and Waterproofing
Drafting Committee
D08.04 - Felts, Fabrics and Bituminous Sheet Materials
Current Stage
Ref Project

Relations

Refers
ASTM D1079-20 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-May-2020
Refers
ASTM D1079-18e1 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
15-Dec-2018
Refers
ASTM D1079-18 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
15-Dec-2018
Refers
ASTM D5147/D5147M-18 - Standard Test Methods for Sampling and Testing Modified Bituminous Sheet Material
Effective Date
01-Jul-2018
Refers
ASTM D1079-16 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-Feb-2016
Refers
ASTM D5147/D5147M-14 - Standard Test Methods for Sampling and Testing Modified Bituminous Sheet Material
Effective Date
01-Jan-2014
Refers
ASTM D1079-13 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-Mar-2013
Refers
ASTM D1079-13e1 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-Mar-2013
Refers
ASTM D5147/D5147M-11a - Standard Test Methods for Sampling and Testing Modified Bituminous Sheet Material
Effective Date
01-May-2011
Refers
ASTM D5147/D5147M-11 - Standard Test Methods for Sampling and Testing Modified Bituminous Sheet Material
Effective Date
01-Jan-2011
Refers
ASTM D5636/D5636M-94(2011)e1 - Standard Test Method for Low Temperature Unrolling of Felt or Sheet Roofing and Waterproofing Materials
Effective Date
01-Jan-2011
Refers
ASTM D1079-10 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-Sep-2010
Refers
ASTM D1079-09 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-Jul-2009
Refers
ASTM D1079-08a - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-Feb-2008
Refers
ASTM D1079-08 - Standard Terminology Relating to Roofing and Waterproofing
Effective Date
01-Jan-2008

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ASTM D6509/D6509M-16(2023) - Standard Specification for Atactic Polypropylene (APP) Modified Bituminous Base Sheet Materials Using Glass Fiber ReinforcementsASTM D6509/D6509M-16(2023) - Standard Specification for Atactic Polypropylene (APP) Modified Bituminous Base Sheet Materials Using Glass Fiber Reinforcements
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ASTM D6509/D6509M-16(2023) - Standard Specification for Atactic Polypropylene (APP) Modified Bituminous Base Sheet Materials Using Glass Fiber Reinforcements
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D6509/D6509M − 16 (Reapproved 2023)
Standard Specification for
Atactic Polypropylene (APP) Modified Bituminous Base
Sheet Materials Using Glass Fiber Reinforcements
This standard is issued under the fixed designation D6509/D6509M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
1.1 This specification covers prefabricated modified bitumi- 2.1 ASTM Standards:
nous sheet materials with glass fiber reinforcement, which use D1079 Terminology Relating to Roofing and Waterproofing
atactic polypropylene (APP) as the primary modifier and which D5147/D5147M Test Methods for Sampling and Testing
are intended for use as a base sheet in the fabrication of Modified Bituminous Sheet Material
multiple ply roofing and waterproofing membranes. D5636/D5636M Test Method for Low-Temperature Unroll-
ing of Felt or Sheet Roofing and Waterproofing Materials
1.2 This is a material specification only. Issues regarding the
suitability of specific roof constructions or application tech-
3. Terminology
niques are beyond the scope of this specification.
3.1 Definitions—For definitions of terms used in this
1.3 The specified tests and property limits used to charac-
specification, refer to Terminology D1079.
terize the sheet materials covered by this specification are
intended to establish minimum properties. In-place roof system
4. Materials and Manufacture
design criteria, such as fire resistance, field strength, impact/
4.1 In the manufacturing process, the reinforcement is
puncture resistance, material compatibility, uplift resistance,
impregnated and coated on both sides in an APP-modified
the need for field applied coatings, and others, are factors
bituminous coating. The APP-modified bituminous coating
beyond the scope of this material specification.
shall be permitted to be compounded with a mineral stabilizer.
1.4 The values stated in either SI units or inch-pound units
4.2 The base sheet shall be permitted to be surfaced with
are to be regarded separately as standard. The values stated in
mineral matter to prevent sticking in the roll. The reverse side
each system may not be exact equivalents; therefore, each
shall be permitted to be covered with a thin polyolefin film or
system shall be used independently of the other. Combining
with other surfacing that will not interfere with adhesion or
values from the two systems may result in non-conformance
bonding of the sheet during application.
with the standard.
5. Physical Properties
1.5 The following precautionary statement pertains only to
the test method portion, Section 8, of this specification. This
5.1 The sheet shall conform to the minimum physical
standard does not purport to address all of the safety concerns,
properties described in Table 1.
if any, associated with its use. It is the responsibility of the user
5.2 The finished product shall not crack or be so sticky as to
of this standard to establish appropriate safety, health, and
cause tearing or other material damage upon being unrolled at
environmental practices and determine the applicability of
any product temperature between 4 °C and 60 °C [40 °F and
regulatory limitations prior to use.
140 °F].
1.6 This international standard was developed in accor-
dance with internationally recognized principles on standard-
6. Dimensions, Mass, and Permissible Variations
ization established in the Decision on Principles for the
6.1 The finished product shall conform to the following
Development of International Standards, Guides and Recom-
dimensions and variations:
mendations issued by the World Trade Organization Technical
6.1.1 The width of the roll shall be as agreed upon between
Barriers to Trade (TBT) Committee.
the purchaser and the supplier and shall not vary more than
1 %.
This specification is under the jurisdiction of ASTM Committee D08 and is the
direct responsibility of Subcommittee D08.04 on Felts, Fabrics and Bituminous
Sheet Materials. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Feb. 1, 2023. Published February 2023. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2000. Last previous edition approved in 2016 as D6509/D6509M – 16. Standards volume information, refer to the standard’s Document Summary page on
DOI: 10.1520/D6509_D6509M-16R23. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6509/D6509M − 16 (2023)
TABLE 1 Physical Properties of Atactic Polypropylene (APP)-
men. It shall be free of visible defects, such as holes, ragged or
Modified Bituminous Base Sheet Materials Using Glass Fiber
untrue edges, breaks, cracks, tears, and protrusions.
Reinforcements
7.2 When unrolled on a smooth plane, the sheet shall be
NOTE 1—The properties in this table are “as manufactured” unless
straight and true so that the lap will mate with an adjacent
otherwise noted.
sheet, within the tolerance for the lap without wrinkles,
Pro
...

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4.1 Composite materials consist by definition of a reinforcement phase in a matrix phase. In addition, ceramic matrix composites (CMCs) often contain measurable porosity which interacts with the reinforcement and matrix. And SiC-SiC composites often use a fiber interface coating which has an important mechanical function. The composition and structure of these different constituents in the CMC are commonly tailored for a specific application with detailed performance requirements. The tailoring involves the selection of the reinforcement fibers (composition, properties, morphology, etc.), the matrix (composition, properties, and morphology), the composite structure (component fractions, reinforcement architecture, interface coatings, porosity structure, microstructure, etc.), and the fabrication conditions (forming, assembly, forming, densification, finishing, etc.). The final engineering properties (physical, mechanical, thermal, electrical, etc.) can be tailored across a broad range with major directional anisotropy in the properties.  
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Standard Guide for Development of Specifications for Fiber Reinforced Carbon-Carbon Composite Structures for Nuclear Applications

SIGNIFICANCE AND USE
4.1 Composite materials consist by definition of a reinforcement phase in a matrix phase. In addition, carbon-carbon composites often contain measurable porosity which interacts with the reinforcement and matrix. The composition and structure of the C-C composite are commonly tailored for a specific application with detailed performance requirements. The tailoring involves the selection of the reinforcement fibers (composition, properties, morphology, etc), the matrix (composition, properties, and morphology), the composite structure (component fractions, reinforcement architecture, porosity structure, microstructure, etc.), and the fabrication conditions (forming, assembly, forming, densification, finishing, etc.). The final engineering properties (physical, mechanical, thermal, electrical, etc.) can be tailored across a broad range with major directional anisotropy in the properties.  
4.2 Specifications for specific C-C composite components covering materials, material processing, and fabrication procedures are developed to provide a basis for fabricating reproducible and reliable structures. Designer/users/producers have to write C-C composite specifications for specific applications with well-defined composition, structure, properties and processing requirements. But with the extensive breadth of selection in composition, structure, and properties in C-C composites, it is virtually impossible to write a "generic" composite specification applicable to any and all C-C composite applications that has the same type of structure and details of the commonly-used specifications for metal alloys. This guide is written to assist the designer/user/producer in developing a comprehensive and detailed material specification for a specific CMC application/component with a particular focus on nuclear applications.  
4.3 The purpose of this guide is to provide guidance on how to specify the constituents, the structure, the desired engineering properties (physical, chemical, ...
SCOPE
1.1 This document is a guide to preparing material specifications for fiber reinforced carbon-carbon (C-C) composite structures (flat plates, rectangular bars, round rods, and tubes) manufactured specifically for structural components in nuclear reactor core applications. The carbon-carbon composites consist of carbon/graphite fibers (from PAN, pitch, or rayon precursors) in a carbon/graphite matrix produced by liquid infiltration/pyrolysis and/or by chemical vapor infiltration.  
1.2 This guide provides direction and guidance for the development of a material specification for a specific C-C composite component or product for nuclear reactor applications. The guide considers composite constituents and structure, physical and chemical properties, mechanical properties, thermal properties, performance durability, methods of testing, materials and fabrication processing, and quality assurance. The C-C composite materials considered here would be suitable for nuclear reactor core applications where neutron irradiation-induced damage and dimensional changes are a significant design consideration. (1-4)2  
1.3 The component specification is to be developed by the designer/purchaser/user. The designer/purchaser/user shall define and specify in detail any and all application-specific requirements for necessary design, manufacturing, and performance factors of the ceramic composite component. This guide for material specifications does not directly address component/product-specific issues, such as geometric tolerances, permeability, bonding, sealing, attachment, and system integration.  
1.4 This guide is specifically focused on C-C composite components and structures with flat panel, solid rectangular bar, solid round rod, or tubular geometries.  
1.5 This specification may also be applicable to C-C composites used for other structural applications discounting the nuclear-specific chemical purity and irradiation behavior f...

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ASTM
ASTM D7028-07(2024)(Test Method)
Standard Test Method for Glass Transition Temperature (DMA Tg) of Polymer Matrix Composites by Dynamic Mechanical Analysis (DMA)

SIGNIFICANCE AND USE
5.1 This test method is designed to determine the glass transition temperature of continuous fiber reinforced polymer composites using the DMA method. The DMA Tg value is frequently used to indicate the upper use temperature of composite materials, as well as for quality control of composite materials.
SCOPE
1.1 This test method covers the procedure for the determination of the dry or wet (moisture conditioned) glass transition temperature (Tg) of polymer matrix composites containing high-modulus, 20 GPa (> 3 × 106 psi), fibers using a dynamic mechanical analyzer (DMA) under flexural oscillation mode, which is a specific subset of the Dynamic Mechanical Analysis (DMA) method.  
1.2 The glass transition temperature is dependent upon the physical property measured, the type of measuring apparatus and the experimental parameters used. The glass transition temperature determined by this test method (referred to as “DMA Tg”) may not be the same as that reported by other measurement techniques on the same test specimen.  
1.3 This test method is primarily intended for polymer matrix composites reinforced by continuous, oriented, high-modulus fibers. Other materials, such as neat resin, may require non-standard deviations from this test method to achieve meaningful results.  
1.4 The values stated in SI units are standard. The values given in parentheses are non-standard mathematical conversions to common units that are provided for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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