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ASTM D3025-07

(Practice)

Standard Practice for Standardizing Cotton Fiber Test Results by Use of Calibration Cotton Standards

Standard Practice for Standardizing Cotton Fiber Test Results by Use of Calibration Cotton Standards

SCOPE
1.1 This practice covers the use of reference standard cottons for the standardization of instruments and techniques used to test cotton fibers in various laboratories.
1.2 Standardization may be achieved by application of a correction factor based on the reference standards, or by modification of the technique in use. Note 1
When reference standards are used to develop correction factors, or to adjust an operator's technique, no instrument calibration processes are involved. The term "Calibration" is properly used for the application or assignment of permanent scales or marks to an instrument. Adjustments can be made to specific instruments and accessories such as orifices, metallic strips, or cellophane sheets, in order to obtain the prescribed values with a specific instrument. Since an operator's technique or the interpretation of a method or procedure is inherently variable, it cannot be calibrated, that is, assigned a permanent, definite value. The use of reference standards, however, affords a means for standardizing techniques and checking the reliability of observed results.
1.3 This practice recognizes two types of reference standards: (1) calibration cotton standards (see ) and (2) working cotton standards (see ).
1.4 The instructions included in this practice can be used with cotton fibers in any form suitable for testing with the particular instrument to be used.
1.5 The instructions in the practice are applicable to cotton fibers but can also be applied to specific blends of cotton and other fibers, or to other fibers that can be tested with the instruments designed for testing cotton fibers. No information is available, however, to show that test procedures standardized with reference cotton samples are equally reliable with various cotton fiber blends or with other fibers.Note 2
Standardization procedures covered in this practice are recommended for use with the following: Test Methods D 1440, D 1445, D 1447, and D 1448.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-2006
ICS
59.060.10 - Natural fibres
Technical Committee
D13 - Textiles
Drafting Committee
D13.11 - Cotton Fibers
Current Stage
Ref Project

Relations

Replaces
ASTM D3025-01 - Standard Practice for Standardizing Cotton Fiber Test Results by Use of Calibration Cotton Standards
Effective Date
01-Jan-2007
Referred By
ASTM D7139-20 - Standard Terminology for Cotton Fibers
Effective Date
01-Jan-2007
Referred By
ASTM D1447-07(2021) - Standard Test Method for Length and Length Uniformity of Cotton Fibers by Photoelectric Measurement
Effective Date
01-Jan-2007
Referred By
ASTM D1445/D1445M-12(2021) - Standard Test Method for Breaking Strength and Elongation of Cotton Fibers (Flat Bundle Method)
Effective Date
01-Jan-2007

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ASTM D3025-07 - Standard Practice for Standardizing Cotton Fiber Test Results by Use of Calibration Cotton StandardsASTM D3025-07 - Standard Practice for Standardizing Cotton Fiber Test Results by Use of Calibration Cotton Standards
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ASTM D3025-07 - Standard Practice for Standardizing Cotton Fiber Test Results by Use of Calibration Cotton Standards
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D3025–07
Standard Practice for
Standardizing Cotton Fiber Test Results by Use of
1
Calibration Cotton Standards
This standard is issued under the fixed designation D3025; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.6 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
1.1 This practice covers the use of reference standard
responsibility of the user of this standard to consult and
cottons for the standardization of instruments and techniques
establish appropriate safety and health practices and deter-
used to test cotton fibers in various laboratories.
mine the applicability of regulatory limitations prior to use.
1.2 Standardization may be achieved by application of a
correction factor based on the reference standards, or by
2. Referenced Documents
modification of the technique in use.
2
2.1 ASTM Standards:
NOTE 1—When reference standards are used to develop correction
D123 Terminology Relating to Textiles
factors, or to adjust an operator’s technique, no instrument calibration
D1440 Test Method for Length and Length Distribution of
processes are involved. The term “Calibration” is properly used for the
Cotton Fibers (Array Method)
application or assignment of permanent scales or marks to an instrument.
D1445 Test Method for Breaking Strength and Elongation
Adjustments can be made to specific instruments and accessories such as
of Cotton Fibers (Flat Bundle Method)
orifices, metallic strips, or cellophane sheets, in order to obtain the
prescribedvalueswithaspecificinstrument.Sinceanoperator’stechnique
D1447 Test Method for Length and Length Uniformity of
or the interpretation of a method or procedure is inherently variable, it
Cotton Fibers by Photoelectric Measurement
cannot be calibrated, that is, assigned a permanent, definite value.The use
D1448 Test Method for Micronaire Reading of Cotton
of reference standards, however, affords a means for standardizing
Fibers
techniques and checking the reliability of observed results.
D7139 Terminology for Cotton Fibers
1.3 This practice recognizes two types of reference stan-
3. Terminology
dards: (1) calibration cotton standards (see 6.1) and (2)
working cotton standards (see 6.2).
3.1 For all terminology relating to D13.11, Cotton Fibers,
1.4 The instructions included in this practice can be used
refer to Terminology D7139.
with cotton fibers in any form suitable for testing with the
3.1.1 The following terms are relevant to this standard:
particular instrument to be used.
calibration cotton standard, reference standard, working cotton
1.5 The instructions in the practice are applicable to cotton
standard.
fibers but can also be applied to specific blends of cotton and
3.2 For all other terminology related to textiles, refer to
other fibers, or to other fibers that can be tested with the
Terminology D123.
instruments designed for testing cotton fibers. No information
4. Summary of Practice
isavailable,however,toshowthattestproceduresstandardized
with reference cotton samples are equally reliable with various
4.1 Testing instruments are adjusted in accordance with
cotton fiber blends or with other fibers.
engineering principles to ensure that they correspond properly
to the manufacturer’s calibration scales and instructions for the
NOTE 2—Standardization procedures covered in this practice are rec-
operation of the instrument.
ommended for use with the following: Test Methods D1440, D1445,
D1447, and D1448. 4.2 Technicians are instructed to operate testings instru-
ments in a consistent manner utilizing appropriate prescribed
ASTM methods.
1
ThispracticeisunderthejurisdictionofASTMCommitteeD13onTextilesand
2
is the direct responsibility of Subcommittee D13.11 on Cotton Fibers. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Jan. 1, 2007. Published January 2007. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1972. Last previous edition approved in 2001 as D3025–01. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D3025-07. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D3025–07
4.3 Specimens of the working cotton standard or calibration tion of the established values, testing may be started on
cotton standard are tested before and periodically during the samples of cotton fiber to be tested. If the
...

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ASTM D2462-22(Test Method)
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5.1 Test Method D2462 for testing for moisture in wool is considered satisfactory for acceptance testing of commercial shipments since current estimates of between-laboratory precision are acceptable.  
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ASTM D2525-22(Practice)
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5.1 This recommended practice furnishes directions for the sampling of wool of the various forms indicated in Section 1, in order that correct probability statements may be made about the relationship between the sample mean and the population mean. If these statements are to be correct, certain conditions, which are stated, must hold.  
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ASTM D2130-22(Test Method)
Standard Test Method for Diameter of Wool and Other Animal Fibers by Microprojection

SIGNIFICANCE AND USE
5.1 This test method specifies a sampling and testing procedure for the measurement of average fiber diameter and variation in diameter of animal fibers as required in Test Method D2968.  
5.2 Test Method D2130 for testing wool and other animal fibers for average fiber diameter is considered satisfactory for acceptance testing of commercial shipments since current estimates of between-laboratory precision are acceptable and the method has been used extensively in the trade for acceptance testing. In cases of disagreement arising from differences in values reported by the purchaser and the seller when using this method for acceptance testing, the statistical bias, if any, between the laboratory of the purchaser and the laboratory of the seller should be determined with each comparison being based on the testing of specimens randomly drawn from one sample of material of the type being evaluated.
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Note 1: This test method may also be applied to any fibers having a round cross section and accordingly may be used many times for melt-spun man-made fibers such as polyamides, polyesters, and glass; also it may be applied to a limited number of polyacrylics and regenerated cellulose type fibers. The values given in Appendix X1 for density and correction factors, however, apply only to wool and should not be used for other fibers. For suitable values for the density of other fibers, see Table 5 in Test Methods D629, Quantitative Analysis of Textiles.
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Standard Test Method for Med and Kemp Fibers in Wool and Other Animal Fibers by Microprojection

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1.1 This test method covers the determination of the breaking tenacity of wool fibers as a flat bundle with a 1/8 in. (3.2 mm) clamp separation.  
1.2 This test method is especially adapted to the fiber bundle clamps and strength testing instruments specified, but may be used on other tensile testing machines when equipped with appropriate adapters to accommodate the prescribed clamps.  
1.3 This test method is applicable to wool in any form which can be hand-combed into small bundles of parallelized fibers.  
Note 1: Other test methods for measuring breaking tenacity of fiber bundles include Test Methods D1294, D1445, and D540.  
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ASTM D1576-22(Test Method)
Standard Test Method for Moisture in Wool by Oven-Drying

SIGNIFICANCE AND USE
5.1 Test Method D2462 for the determination of the moisture in wool by distillation with toluene is the preferred method for testing wool for moisture for the acceptance testing of commercial shipments. If, however, the purchaser and the supplier agree, Test Method D1576 for the determination of the moisture in wool by oven drying may be used instead. Comparative tests as directed in 5.1.1, may be advisable.  
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1.1 This test method covers the determination of the amount of moisture present in ordinary commercial and industrial samples of wool in all forms except grease wool, using the oven-drying technique.  
1.2 Formulas for calculating the moisture content (as-received basis) and moisture regain (oven-dried basis) are given. It is always important to use the correct term which corresponds to the basis used in the calculation (see 12.2.1).  
Note 1: The determination of moisture content for textile materials in general is covered in Test Methods D2654, and an optimal method for determining the moisture in wool by distillation with toluene is covered in Test Method D2462. A method for sampling wool for the determination of moisture in wool is covered in Practice D2525. The oven-drying method has been adapted for cotton in Test Method D2495.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D1574-22(Test Method)
Standard Test Method for Extractable Matter in Wool and Other Animal Fibers

SIGNIFICANCE AND USE
5.1 Test Method D1574 is considered satisfactory for acceptance testing since the method has been used extensively in the trade for acceptance testing.  
5.1.1 In case of a dispute arising from differences in reported test results when using Test Method D1574 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens that are as homogeneous as possible and that are from a lot of material of the type in question. The test specimens should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-test for unpaired data and an acceptable probability level chosen by the two parties before the testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results in the light of the known bias.  
5.2 This test method may be used to estimate the quantity of oil, grease, and waxy materials remaining on or in wool fibers after scouring, or the quantity of lubricant added before carding or remaining after carding, or the quantity of such materials added or removed in subsequent processing operations.  
5.3 The residues obtained in this test may be subjected to chemical analysis for identification and assay of the component materials, if desired.  
5.4 The specified solvent in this test method does not remove some materials, such as soaps, that may be present in wool and hence in some cases may reflect more closely the added content of some extractables in wool such as oils. When such materials are present and an estimate of their quantity is desired, some other solvent or combination of solvents should be used as spec...
SCOPE
1.1 This test method covers the determination of the amount of extractable matter in samples of all forms of wool, except grease wool, that is extractable with a non-flammable vapor degreasing and cleaning solvent.  
1.2 This test method does not cover the determination of the amounts of different components in the extracted matter nor their identification.  
1.3 This test method is suitable for use with other animal fibers.  
Note 1: The determination of extractable matter in yarns and in felts is covered in Test Methods D2257 and D461. For the determination of alcohol-extractable matter in oven-dry scoured wool, refer to Test Methods D584 and D1334.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See 5.4 and Note 3.  
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ASTM D1294-22(Test Method)
Standard Test Method for Tensile Strength and Breaking Tenacity of Wool Fiber Bundles 1-in. (25.4 mm) Gage Length

SIGNIFICANCE AND USE
5.1 Test Method D1294 for the determination of tensile strength may be used for the acceptance testing of commercial shipments of wool, but caution is advised since technicians may fail to get good agreement between results. Comparative tests as directed in 5.1.1 may be advisable.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative test should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative test that are as homogenous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
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1.1 This test method covers the determination of the breaking force (or load) and estimation of the tensile strength and tenacity of wool fiber bundles with a 1-in. (25.4 mm) gage length. A procedure for preparation of the fiber bundle is included.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. Because the instrument is calibrated in inch-pound units, inch-pound units are shown first, contrary to Committee D13 policy.  
Note 1: For other methods of measuring breaking tenacity of fiber bundles, refer to Test Methods D1445 and D2524.
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1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D8394-21(Test Method)
Standard Test Method for Automated Measurement of Maturity, Fineness, Ribbon Width, and Micronaire of Cotton Fibers

SIGNIFICANCE AND USE
5.1 Cotton fiber that is on average finer and more mature is more desirable than coarse or immature fiber, although distinction between these qualities cannot be made quickly and accurately using current test methods. Immature fibers break more easily during processing and have a tendency to form into neps (small entanglements) during processing in the spinning mill. These consequences adversely affect yarn and fabric quality and appearance. Yarn and fabric produced from immature fiber is typically also less lustrous and does not take up dye consistently so yarn and fabric appearance may be different after dyeing.  
5.2 Maturity has a high positive correlation with fiber length and strength but genetic differences and differences in fiber wall thickness caused by plant diseases, soil, and water conditions during the growing season interfere with this relationship.  
5.2.1 Fine fibers are required for fine count yarn manufacture and fiber fineness affects yarn count, evenness and strength. Both fineness and ribbon width are strong genetic traits evident between species and affected by growing conditions within species.  
5.2.2 Micronaire has traditionally been used as a measure of fiber fineness although the value actually measures fiber specific surface area or surface area per unit weight. As a result, micronaire varies concomitantly with both maturity and fineness (see Fig. 2). Maturity and fineness are related to micronaire via Lord’s equation.4
FIG. 2 Relationship Between Micronaire (X), Fineness (H), and Maturity (M)  
5.3 Cottonscope values have been judged against fineness, maturity and ribbon width values produced by examination of thousands of individual, magnified fiber cross-sections. Relationships with equivalent values by these and other older test methods are highly significant5,6 particularly if the number of cross-sections analyzed is high (>3000) and the cross-sections are carefully prepared and measured. Cottonscope measures approximately 20,...
SCOPE
1.1 This test method covers the determination of linear density (gravimetric fineness hereafter stated as fineness), maturity, micronaire, and ribbon width of cotton fibers from a loose, chemically untreated sample taken before harvest, during ginning, during mill processing or unraveled from raw (undyed) yarn or fabric.  
1.2 This test method requires the use of an integrated instrument, for example, the Cottonscope (see Fig. 1), that measures the maturity, fineness, ribbon width, and micronaire of cotton fiber.2
FIG. 1 Cottonscope Instrument
Note 1: For another test method to determine the maturity of cotton fibers, refer to Test Method D1442.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D6961/D6961M-09(2021)(Test Method)
Standard Test Method for Color Measurement of Flax Fiber

SIGNIFICANCE AND USE
5.1 Few standards exist to objectively judge flax quality. Color is an important factor in the quality of flax fiber. Natural variations in raw flax fiber, various processing steps, fiber blending, and a wide range of end uses contribute to the need for a standard method of objectively measuring the color of flax fiber. Spectrophotometic data provide an accurate, precise determination of the color of flax fiber. Colorimetric data are obtained through specimen measurement by combining specimen spectral data with data representing a CIE standard observer and a CIE standard illuminant, as described in Practice E308.  
5.2 If there are differences of practical significance between reported test results for two (or more) laboratories, comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative test that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that fiber sample type must be adjusted in consideration of the known bias.
SCOPE
1.1 This test method covers the instrumental color measurement of flax fiber.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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