ASTM E1363-18

Standard Test Method for Temperature Calibration of Thermomechanical Analyzers

SIGNIFICANCE AND USE
5.1 Thermomechanical analyzers are employed in their various modes of operation (penetration, expansion, flexure, etc.) to characterize a wide range of materials. In most cases, the value to be assigned in thermomechanical measurements is the temperature of the transition (or event) under study. Therefore, the temperature axis (abscissa) of all TMA thermal curves must be accurately calibrated either by direct reading of a temperature sensor or by adjusting the programmer temperature to match the actual temperature over the temperature range of interest.
SCOPE
1.1 This test method describes the temperature calibration of thermomechanical analyzers from −50 °C to 1500 °C. (See Note 1.)  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Warning—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7 and Note 11.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

• Status: Historical
• Publication Date: 30-Nov-2018
• ICS: 17.200.20 - Temperature-measuring instruments
• Technical Committee: E37 - Thermal Measurements
• Drafting Committee: E37.10 - Fundamental, Statistical and Mechanical Properties

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E1363 − 18
Standard Test Method for
1
Temperature Calibration of Thermomechanical Analyzers
This standard is issued under the fixed designation E1363; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* E473 Terminology Relating to Thermal Analysis and Rhe-
ology
1.1 This test method describes the temperature calibration
E3142 Test Method for Thermal Lag of Thermal Analysis
of thermomechanical analyzers from −50 °C to 1500 °C. (See
Apparatus
Note 1.)
1.2 The values stated in SI units are to be regarded as
3. Terminology
standard. No other units of measurement are included in this
3.1 Definitions:
standard.
3.1.1 The terminology relating to thermal analysis appear-
1.3 Warning—Mercury has been designated by many regu-
ing in Terminology E473 shall be considered applicable to this
latory agencies as a hazardous substance that can cause
document.
serious medical issues. Mercury, or its vapor, has been
demonstrated to be hazardous to health and corrosive to
4. Summary of Test Method
materials. Use caution when handling mercury and mercury-
containing products. See the applicable product Safety Data
4.1 An equation is developed for the linear correlation of the
Sheet (SDS) for additional information. The potential exists
experimentally observed program temperature and the actual
that selling mercury or mercury-containing products, or both,
melting temperature for known melting standards. This is
is prohibited by local or national law. Users must determine
accomplished through the use of a thermomechanical analyzer
legality of sales in their location.
with a penetration probe to obtain the onset temperatures for
1.4 This standard does not purport to address all of the
two melting point standards. An alternate, one-point method of
safety concerns, if any, associated with its use. It is the
temperature calibration is also given for use over very narrow
responsibility of the user of this standard to establish appro-
temperature ranges. (See Note 2.)
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
NOTE 1—This test method may be used for calibrating thermomechani-
Specific precautionary statements are given in Section 7 and
cal analyzers at temperatures outside this range of temperature. However,
Note 11. the accuracy of the calibration will be no better than that of the
temperature standards used.
1.5 This international standard was developed in accor-
NOTE 2—It is possible to develop a more elaborate method of
dance with internationally recognized principles on standard-
temperature calibration using multiple (more than two) fusion standards
ization established in the Decision on Principles for the
and quadratic regression analysis. Since most modern instruments are
Development of International Standards, Guides and Recom-
capable of heating rates which are essentially linear in the region of use,
mendations issued by the World Trade Organization Technical
the procedure given here is limited to a two-point calibration.
Barriers to Trade (TBT) Committee.
5. Significance and Use
2. Referenced Documents
2
5.1 Thermomechanical analyzers are employed in their
2.1 ASTM Standards:
various modes of operation (penetration, expansion, flexure,
etc.) to characterize a wide range of materials. In most cases,
1
This test method is under the jurisdiction of ASTM Committee E37 on Thermal
the value to be assigned in thermomechanical measurements is
Measurements and is the direct responsibility of Subcommittee E37.10 on
Fundamental, Statistical and Mechanical Properties.
the temperature of the transition (or event) under study.
Current edition approved Dec. 1, 2018. Published January 2019. Originally
Therefore, the temperature axis (abscissa) of all TMA thermal
approved in 1990. Last previous edition approved in 2016 as E1363 – 16. DOI:
10.1520/E1363-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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E1363 − 18
curves must be accurately calibrated either by direct reading of 7. Hazards
a temperature sensor or by adjusting the programmer tempera-
7.1 This test method may involve the use of hazardo
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E1363 − 16 E1363 − 18
Standard Test Method for
1
Temperature Calibration of Thermomechanical Analyzers
This standard is issued under the fixed designation E1363; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 This test method describes the temperature calibration of thermomechanical analyzers from −50 °C to 1500°C. 1500 °C.
(See Note 1.)
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 ThisWarning— standard is similar to ISO 11359–1 but addresses a larger temperature range and utilizes additional
calibration materials.Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious
medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use caution
when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional
information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national
law. Users must determine legality of sales in their location.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7 and Note 11.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
E473 Terminology Relating to Thermal Analysis and Rheology
E3142 Test Method for Thermal Lag of Thermal Analysis Apparatus
3
2.2 Other Standards:
ISO 11359–1 Thermomechanical Analysis (TMA)-Part 1: General Principles
3. Terminology
3.1 Definitions:
3.1.1 The terminology relating to thermal analysis appearing in Terminology E473 shall be considered applicable to this
document.
4. Summary of Test Method
4.1 An equation is developed for the linear correlation of the experimentally observed program temperature and the actual
melting temperature for known melting standards. This is accomplished through the use of a thermomechanical analyzer with a
penetration probe to obtain the onset temperatures for two melting point standards. An alternate, one-point method of temperature
calibration is also given for use over very narrow temperature ranges. (See Note 2.)
NOTE 1—This test method may be used for calibrating thermomechanical analyzers at temperatures outside this range of temperature. However, the
accuracy of the calibration will be no better than that of the temperature standards used.
NOTE 2—It is possible to develop a more elaborate method of temperature calibration using multiple (more than two) fusion standards and quadratic
1
This test method is under the jurisdiction of ASTM Committee E37 on Thermal Measurements and is the direct responsibility of Subcommittee E37.10 on Fundamental,
Statistical and Mechanical Properties.
Current edition approved Dec. 1, 2016Dec. 1, 2018. Published January 2017January 2019. Originally approved in 1990. Last previous edition approved in 20132016 as
E1363 – 13.E1363 – 16. DOI: 10.1520/E1363-16.10.1520/E1363-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1363 − 18
regression analysis. Since most modern instruments are capable of heating rates which are essentially linear in the region of use, the procedure given here
is limited to a two-point calibration.
5. Si
...