ASTM E2082-12
(Guide)Standard Guide for Descriptive Analysis of Shampoo Performance
Standard Guide for Descriptive Analysis of Shampoo Performance
SIGNIFICANCE AND USE
6.1 The methods outlined in this guide can be used to qualitatively and quantitatively describe the performance and sensory characteristics of shampoos.
6.2 The methods described in this guide may be used for product formulation and research guidance as well as for quality control.
6.3 These methods may be used by individuals who familiarize themselves with these procedures and who have previous experience with sensory evaluation.
6.4 Variables that may affect results include, but are not limited to, water conditions (for example, hardness), hair type, and hair condition. These variables should be controlled or accounted for in the experimental design.
6.5 These are suggested procedures and are not intended to exclude alternate methods, which may effectively provide the same or similar results.
SCOPE
1.1 The objective of this guide is to provide procedures which may be used in the design, execution, and analysis of studies to quantitatively assess the objective sensory attributes of shampoos. This is one of many appropriate techniques used in the hair-care industry. These attributes can then be used to define performance of shampoos and to provide direction in product formulation, research guidance testing, and claim substantiation. This guide includes the sensory properties involved in dispensing a product, as well as the attributes pertinent to shampooing swatches, half and whole heads. Although this guide is specific to shampoos, the procedures should be applicable to most hair-care products.
1.2 Guidelines are provided for the definition of terminology, procedures for manipulation of products, identification/selection of hair type, and assessor training. References for rating scales are not provided in this guide. The user should be aware that some sensory practices may require the use of attribute references (anchors) when training the assessors.
General Information
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Designation: E2082 − 12
Standard Guide for
1
Descriptive Analysis of Shampoo Performance
This standard is issued under the fixed designation E2082; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope ASTM STP758 Guidelines for the Selection andTraining of
Sensory Panel Members
1.1 The objective of this guide is to provide procedures
4
2.3 Code of Federal Regulations:
which may be used in the design, execution, and analysis of
21 CFR 50.25 Protection of Human Subjects—Elements of
studies to quantitatively assess the objective sensory attributes
Informed Consent
of shampoos. This is one of many appropriate techniques used
in the hair-care industry. These attributes can then be used to
3. Terminology
define performance of shampoos and to provide direction in
3.1 Definitions—Definitions of terms other than those given
product formulation, research guidance testing, and claim
as follows appear in Terminology E253.
substantiation. This guide includes the sensory properties
involved in dispensing a product, as well as the attributes
3.2 Definitions:
pertinent to shampooing swatches, half and whole heads.
3.2.1 cosmetologist—a licensed, trained professional who
Although this guide is specific to shampoos, the procedures
has been certified by state or government agencies to apply
should be applicable to most hair-care products.
hair-care products to human heads. These individuals may be
alternately described as beauticians, stylists, hairdressers, or
1.2 Guidelines are provided for the definition of
cosmetologists.
terminology, procedures for manipulation of products,
identification/selection of hair type, and assessor training. 3.2.2 subjects—those individuals recruited to participate in
References for rating scales are not provided in this guide. The a study for the quality or condition of their hair, to serve as
user should be aware that some sensory practices may require sample carriers.
the use of attribute references (anchors) when training the
3.2.3 trained panel—a group of assessors who have been
assessors.
formally trained to evaluate the visual and tactile properties of
shampoo or hair, using a standard descriptive analysis method
2. Referenced Documents
which quantifies attributes on a rating scale over a set time
2
2.1 ASTM Standards:
period. The number may vary depending on the complexity of
E253 Terminology Relating to Sensory Evaluation of Mate-
the test and the skill of the assessor.
rials and Products
3
4. Equipment
2.2 ASTM Publications:
ASTM Manual 13 Descriptive Analysis Testing for Sensory
4.1 The following equipment may be used during the
Evaluation
evaluation process:
ASTMManual26 SensoryTestingMethods:SecondEdition
4.1.1 General:
ASTM Manual 30 Relating Consumer, Descriptive, and
4.1.1.1 Light Source—A consistent light source is recom-
Laboratory Data to Better Understand Consumer Re- mended for use during evaluation of shine or luster. It is
sponses
important to control the amount of light as well as the angle
and distance from the hair.
4.1.1.2 Water Source—Temperature and hardness should be
1
This guide is under the jurisdiction of ASTM Committee E18 on Sensory
consistent. If controlled temperature sinks are used, they
Evaluation and is the direct responsibility of Subcommittee E18.07 on Personal
should all have the same, consistent flow rate.
Care and Household Evaluation.
Current edition approved Oct. 15, 2012. Published December 2012. Originally 4.1.1.3 Blow Dryer—Specifications should be documented
approved in 2000. Last previous edition approved in 2006 as E2082 – 06. DOI:
(that is, wattage, voltage, power level, air velocity, and
10.1520/E2082-12.
temperature).
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
4.1.1.4 Syringes/Pipettes, Petri Dishes.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3 4
Available from ASTM International Headquarters, 100 Barr Harbor Drive, PO AvailablefromU.S.GovernmentPrintingOfficeSuperintendentofDocuments,
Box C700, West Conshohocken, PA 19428-2959 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2082 − 12
4.1.1.5 Towels (cloth or paper, or both).
Comparative Overview of Shampoo Testing Using Trained Evaluators
Swatches versus Subjects
4.1.1.6 Combs—It is recommended that all combs be iden-
Swatch Subject: Half or
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2082 − 06 E2082 − 12
Standard Guide for
1
Descriptive Analysis of Shampoo Performance
This standard is issued under the fixed designation E2082; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 The objective of this guide is to provide procedures which may be used in the design, execution, and analysis of studies to
quantitatively assess the objective sensory attributes of shampoos. This is one of many appropriate techniques used in the hair-care
industry. These attributes can then be used to define performance of shampoos and to provide direction in product formulation,
research guidance testing, and claim substantiation. This guide includes the sensory properties involved in dispensing a product,
as well as the attributes pertinent to shampooing tresses, half and whole heads. Although this guide is specific to shampoos, the
procedures should be applicable to most hair-care products.
1.2 Guidelines are provided for the definition of terminology, procedures for manipulation of products, identification/selection
of hair type, and assessor training. References for rating scales are not provided in this guide. The user should be aware that some
sensory practices may require the use of attribute references (anchors) when training the assessors.
2. Referenced Documents
2
2.1 ASTM Standards:
E253 Terminology Relating to Sensory Evaluation of Materials and Products
3
2.2 ASTM Publications:
ASTM Manual 13 Descriptive Analysis Testing for Sensory Evaluation
ASTM Manual 26 Sensory Testing Methods: Second Edition
ASTM Manual 30 Relating Consumer, Descriptive, and Laboratory Data to Better Understand Consumer Responses
ASTM STP 758 Guidelines for the Selection and Training of Sensory Panel Members
4
2.3 Code of Federal Regulations:
21 CFR 50.25 Protection of Human Subjects—Elements of Informed Consent
3. Terminology
3.1 Definitions—Definitions of terms other than those given as follows appear in Terminology E253.
3.2 Definitions:
3.2.1 cosmetologist—a licensed, trained professional who has been certified by state or government agencies to apply hair-care
products to human heads. These individuals may be alternately described as beauticians, stylists, hairdressers, or cosmetologists.
3.2.2 subjects—those individuals recruited to participate in a study for the quality or condition of their hair, to serve as sample
carriers.
3.2.3 trained panel—a group of assessors who have been formally trained to evaluate the visual and tactile properties of
shampoo or hair, using a standard descriptive analysis method which quantifies attributes on a rating scale over a set time period.
The number may vary depending on the complexity of the test and the skill of the assessor.
4. Equipment
4.1 The following equipment may be used during the evaluation process:
4.1.1 General:
1
This guide is under the jurisdiction of ASTM Committee E18 on Sensory Evaluation and is the direct responsibility of Subcommittee E18.07 on Personal Care and
Household Evaluation.
Current edition approved April 1, 2006Oct. 15, 2012. Published April 2006December 2012. Originally approved in 2000. Last previous edition approved in 20002006 as
E2082 – 00.E2082 – 06. DOI: 10.1520/E2082-06.10.1520/E2082-12.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from ASTM International Headquarters, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959
4
Available from U.S. Government Printing Office Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E2082 − 12
4.1.1.1 Light Source—A consistent light source is recommended for use during evaluation of shine or luster. It is important to
control the amount of light as well as the angle and distance from the hair.
4.1.1.2 Water Source—Temperature and hardness should be consistent. If controlled temperature sinks are used, they should all
have the same, consistent flow rate.
4.1.1.3 Blow Dryer—Specific
...










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