Standard Test Method for Accelerated Aging of Liquid Water-Emulsion Floor Polishes

SIGNIFICANCE AND USE
This test method is not absolute but does give an indication of the useful shelf-life of a liquid water-emulsion floor polish. Will indicate whether a polish will gel or remain a usable liquid over the desired storage life of the product. It should be noted that polishes of different composition types will vary in useful storage life under identical storage conditions.
SCOPE
1.1 This test method covers the storage stability of liquid water-emulsion floor polishes.
1.2 Storage for 30 days at 52°C (125°F), while not a guarantee of one year stability at 21°C (70°F), is believed to be a more reliable indicator of storage stability than similar tests of shorter duration.
Note 1—The 60 specular gloss on black glass determined by Test Method D 1455, may be used to confirm this observation. A substantial difference in gloss between aged and unaged samples is an indication of instability. A shelf stability of one year can be reasonably expected of the material in question if duplicate samples remain unchanged for 30 days at 52 1.1°C (125 2°F). If one or both duplicates show more than slight viscosity increases or slight creaming, other evidence of stability must be sought.1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
31-Aug-2004
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ASTM D1791-93(2004) - Standard Test Method for Accelerated Aging of Liquid Water-Emulsion Floor Polishes
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D1791–93 (Reapproved 2004)
Standard Test Method for
Accelerated Aging of Liquid Water-Emulsion Floor Polishes
This standard is issued under the fixed designation D 1791; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Apparatus
1.1 This test method covers the storage stability of liquid 4.1 Flint Glass Bottles, 4-oz (125 mL) capacity.
water-emulsion floor polishes. 4.2 Drying Oven, capable of maintaining the temperature of
1.2 Storage for 30 days at 52°C (125°F), while not a the emulsion samples at 52 6 1.1°C (125 6 2°F).
guarantee of one year stability at 21°C (70°F), is believed to be
5. Sample
a more reliable indicator of storage stability than similar tests
5.1 The sample shall be thoroughly representative of the
of shorter duration.
material in question, and the portion used for the test shall be
NOTE 1—The 60° specular gloss on black glass determined by Test
thoroughly representative of the sample itself.
Method D 1455, may be used to confirm this observation. A substantial
5.2 Test samples shall be prepared in duplicate for each
difference in gloss between aged and unaged samples is an indication of
material in question.
instability.Ashelf stability of one year can be reasonably expected of the
material in question if duplicate samples remain unchanged for 30 days at
6. Procedure
52 6 1.1°C (125 6 2°F). If one or both duplicates show more than slight
viscosity increases or slight creaming, other evidence of stability must be
6.1 Transfer 100 mL of the emulsion to a clean, dry test
sought.
bottle and hand tighten the screw cap.
1.3 This standard does not purport to address all of the
6.2 Place the test set or series inverted in a drying oven
safety problems, if any, associated with its use. It is the
capable of maintaining the temperature of the emulsions at 52
responsibility of the user of this standard to establish appro-
6 1.1°C (125 6 2°F).
priate safety and health practices and determine the applica-
6.3 Observe the samples daily for the first 14 days and
bility of regulatory limitations prior to use.
thereafter twice weekly (for example, Monday and Thursday)
for the remainder of the 30-day storage period. Samples should
2. Referenced Documents
be examined as rapidly as possible with a minimum of
2.1 ASTM Standards:
agitation, and returned to the oven. Do not loosen the cap.
D 1455 Test Method for 60° Specular Gloss of Emulsion
7. Report
Floor Polish
7.1 The report shall include the following recorded at the
3. Significance and Use
time of each observation on a suitable data sheet:
3.1 This test method is not absolute but does give an
7.1.1 Date.
indication of the useful shelf-life of a liquid water-emulsion
7.1.2 Number of days in test.
floor polish. Will indicate whether a polish will gel or remain
7.1.3 Condition of the emulsion us
...

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