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ASTM C225-85(2022)

(Test Method)

Standard Test Methods for Resistance of Glass Containers to Chemical Attack

Standard Test Methods for Resistance of Glass Containers to Chemical Attack

SIGNIFICANCE AND USE
3.1 The solubility of glass in contact with food, beverages, or pharmaceutical products is an important consideration for the safe packaging and storage of such materials. Autoclave conditions are specified since sterilization is often employed for the packaging of the product. It also represents one of the most extreme conditions, particularly of temperature, that containers will ordinarily experience. Any of the three test methods described may be used to establish specifications for conformity to standard values, either as specified by a customer, an agency, or “The United States Pharmacopeia:”  
3.1.1 Test Method B-A  is intended particularly for testing glass containers primarily destined for containment of products with a pH under 5.  
3.1.2 Test Method B-W  is intended particularly for testing glass containers to be used for products with a pH of 5.0 or over.  
3.1.3 Test Method P-W  is a hydrolytic autoclave test primarily intended for evaluating samples from untreated glass containers. It is often useful for testing the resistance of containers of too small capacity to permit measurements of solubility on the unbroken article by the B-W test method. Yielding the water resistance of the bulk glass, it can also be used in conjunction with the B-W test method to distinguish whether the internal surface of a container has been treated to improve its durability.  
3.2 All three test methods are suitable for specification acceptance.
SCOPE
1.1 These test methods cover the evaluation of the resistance of glass containers to chemical attack. Three test methods are presented, as follows:  
1.1.1 Test Method B-A  covers autoclave tests at 121 °C on bottles partially filled with dilute acid as the attacking medium.  
1.1.2 Test Method B-W  covers autoclave tests at 121 °C on bottles partially filled with distilled water as the attacking medium.  
1.1.3 Test Method P-W  covers autoclave tests at 121 °C on powdered samples with pure water as the attacking medium.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Jun-2022
ICS
81.040.30 - Glass products
Technical Committee
C14 - Glass and Glass Products
Drafting Committee
C14.02 - Chemical Properties and Analysis
Current Stage
Ref Project

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ASTM C225-85(2022) - Standard Test Methods for Resistance of Glass Containers to Chemical AttackASTM C225-85(2022) - Standard Test Methods for Resistance of Glass Containers to Chemical Attack
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ASTM C225-85(2022) - Standard Test Methods for Resistance of Glass Containers to Chemical Attack
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C225 − 85 (Reapproved 2022)
Standard Test Methods for
1
Resistance of Glass Containers to Chemical Attack
This standard is issued under the fixed designation C225; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope D1125 Test Methods for Electrical Conductivity and Resis-
tivity of Water
1.1 These test methods cover the evaluation of the resis-
D1193 Specification for Reagent Water
tanceofglasscontainerstochemicalattack.Threetestmethods
E11 Specification for Woven Wire Test Sieve Cloth and Test
are presented, as follows:
Sieves
1.1.1 Test Method B-A covers autoclave tests at 121 °C on
E691 Practice for Conducting an Interlaboratory Study to
bottles partially filled with dilute acid as the attacking medium.
Determine the Precision of a Test Method
1.1.2 Test Method B-W covers autoclave tests at 121 °C on
bottles partially filled with distilled water as the attacking
3. Significance and Use
medium.
1.1.3 Test Method P-W covers autoclave tests at 121 °C on 3.1 The solubility of glass in contact with food, beverages,
powdered samples with pure water as the attacking medium. or pharmaceutical products is an important consideration for
the safe packaging and storage of such materials. Autoclave
1.2 The values stated in SI units are to be regarded as the
conditions are specified since sterilization is often employed
standard. The values in parentheses are for information only.
for the packaging of the product. It also represents one of the
1.3 This standard does not purport to address all of the
most extreme conditions, particularly of temperature, that
safety concerns, if any, associated with its use. It is the
containers will ordinarily experience. Any of the three test
responsibility of the user of this standard to establish appro-
methods described may be used to establish specifications for
priate safety, health, and environmental practices and deter-
conformity to standard values, either as specified by a
mine the applicability of regulatory limitations prior to use.
customer, an agency, or “The United States Pharmacopeia:”
1.4 This international standard was developed in accor-
3.1.1 Test Method B-A is intended particularly for testing
dance with internationally recognized principles on standard-
glasscontainersprimarilydestinedforcontainmentofproducts
ization established in the Decision on Principles for the
with a pH under 5.
Development of International Standards, Guides and Recom-
3.1.2 Test Method B-W is intended particularly for testing
mendations issued by the World Trade Organization Technical
glass containers to be used for products with a pH of 5.0 or
Barriers to Trade (TBT) Committee.
over.
3.1.3 Test Method P-W is a hydrolytic autoclave test primar-
2. Referenced Documents
ily intended for evaluating samples from untreated glass
2
2.1 ASTM Standards:
containers. It is often useful for testing the resistance of
A569/A569M Specification for Steel, Carbon (0.15
containers of too small capacity to permit measurements of
Maximum,Percent),Hot-RolledSheetandStripCommer-
solubility on the unbroken article by the B-W test method.
3
cial
Yielding the water resistance of the bulk glass, it can also be
used in conjunction with the B-W test method to distinguish
whether the internal surface of a container has been treated to
1
improve its durability.
These test methods are under the jurisdiction of ASTM Committee C14 on
Glass and Glass Products and are the direct responsibility of Subcommittee C14.02
3.2 All three test methods are suitable for specification
on Chemical Properties and Analysis.
acceptance.
Current edition approved July 1, 2022. Published July 2022. Originally approved
in 1949. Last previous edition approved 2014 as C225 – 85 (2014). DOI: 10.1520/
C0225-85R22.
4. Purity of Reagents
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.1 Reagent grade chemicals shall be used in all tests.
Standards volume information, refer to the standard’s Document Summary page on
Unless otherwise indicated, it is intended that all reagents shall
the ASTM website.
3
conform to the specifications of the Committee on Analytical
Withdrawn. The last approved version of this historical standard is referenced
on www.astm.org. Reagents of the American Chemical Soci
...

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ASTM C1648-12(2023)(Guide)
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SIGNIFICANCE AND USE
4.1 Measurement—The refractive index at any wavelength of a piece of homogeneous glass is a function, primarily, of its composition, and secondarily, of its state of annealing. The index of a glass can be altered over a range of up to 1×10-4 (that is, 1 in the fourth decimal place) by the changing of an annealing schedule. This is a critical consideration for optical glasses, that is, glasses intended for use in high performance optical instruments where the required value of an index can be as exact as 1×10-6. Compensation for minor variations of composition are made by controlled rates of annealing for such optical glasses; therefore, the ability to measure index to six decimal places can be a necessity; however, for most commercial and experimental glasses, standard annealing schedules appropriate to each are used to limit internal stress and less rigorous methods of test for refractive index are usually adequate. The refractive indices of glass ophthalmic lens pressings are held to 5×10-4 because the tools used for generating the figures of ophthalmic lenses are made to produce curvatures that are related to specific indices of refraction of the lens materials.  
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1.1 This guide identifies and describes seven test methods for measuring the index of refraction of glass, with comments relevant to their uses such that an appropriate choice of method can be made. Four additional methods are mentioned by name, and brief descriptive information is given in Annex A1. The choice of a test method will depend upon the accuracy required, the nature of the test specimen that can be provided, the instrumentation available, and (perhaps) the time required for, or the cost of, the analysis. Refractive index is a function of the wavelength of light; therefore, its measurement is made with narrow-bandwidth light. Dispersion is the physical phenomenon of the variation of refractive index with wavelength. The nature of the test-specimen refers to its size, form, and quality of finish, as described in each of the methods herein. The test methods described are mostly for the visible range of wavelengths (approximately 400 μm to 780 μm); however, some methods can be extended to the ultraviolet and near infrared, using radiation detectors other than the human eye.  
1.1.1 List of test methods included in this guide:
1.1.1.1 Becke line (method of central illumination),
1.1.1.2 Apparent depth of microscope focus (the method of the Duc de Chaulnes),
1.1.1.3 Critical Angle Refractometers (Abbe type and Pulfrich type),
1.1.1.4 Metricon2 system,
1.1.1.5 Vee-block refractometers,
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1.1.1.7 Specular reflectance.  
1.1.2 Test methods presented by name only (see Annex A1):
1.1.2.1 Immersion refractometers,
1.1.2.2 Interferometry,
1.1.2.3 Ellipsometry, and
1.1.2.4 Method of oblique illumination.  
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Standard Test Methods for Polariscopic Examination of Glass Containers

SIGNIFICANCE AND USE
4.1 These two test methods are provided for evaluating the quality of annealing. These test methods can be used in the quality control of glass containers or other products made of similar glass compositions, where the degree of annealing must be verified to ensure quality products. These test methods apply to glass containers manufactured from commercial soda-lime-silica glass compositions.
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1.1 These test methods describe the determination of relative optical retardation associated with the state of anneal of glass containers. Two alternative test methods are covered as follows:    
Sections  
Test Method A—Comparison with Reference Standards
Using a Polariscope  
6 – 9  
Test Method B—Determination with Polarimeter  
10 – 12  
1.2 Test Method A is useful in determining retardations less than 150 nm, while Test Method B is useful in determining retardations less than 565 nm.  
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Standard Test Method for Bake and Boil Testing of Laminated Glass

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5.1 It is generally recognized that excess moisture and air within an interlayer will cause bubble formation in a laminate when exposed to heat or UV radiation, or both. These may be caused by initial moisture and air in the interlayer and be generated by thermal exposure. The purpose of this test method is to measure quantitatively the laminate stability under controlled conditions, specifically in relation to the formation of bubbles in the body of the laminate.  
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1.1 The purpose of this test method is to measure quantitatively the laminate stability under controlled conditions, specifically in relation to the formation of bubbles in a laminate with heat exposure.  
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SIGNIFICANCE AND USE
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Standard Test Method for Young's Modulus, Shear Modulus, and Poisson's Ratio for Glass and Glass-Ceramics by Resonance

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1.1 This test method covers the determination of the elastic properties of glass and glass-ceramic materials. Specimens of these materials possess specific mechanical resonance frequencies which are defined by the elastic moduli, density, and geometry of the test specimen. Therefore the elastic properties of a material can be computed if the geometry, density, and mechanical resonance frequencies of a suitable test specimen of that material can be measured. Young's modulus is determined using the resonance frequency in the flexural mode of vibration. The shear modulus, or modulus of rigidity, is found using torsional resonance vibrations. Young's modulus and shear modulus are used to compute Poisson's ratio, the factor of lateral contraction.  
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Note 1: Elastic here means that an application of stress within the elastic limit of that material making up the body being stressed will cause an instantaneous and uniform deformation, which will cease upon removal of the stress, with the body returning instantly to its original size and shape without an energy loss. Glass and glass-ceramic materials conform to this definition well enough that this test is meaningful.
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1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
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1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
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SIGNIFICANCE AND USE
4.1 Measurement—The refractive index at any wavelength of a piece of homogeneous glass is a function, primarily, of its composition, and secondarily, of its state of annealing. The index of a glass can be altered over a range of up to 1×10-4 (that is, 1 in the fourth decimal place) by the changing of an annealing schedule. This is a critical consideration for optical glasses, that is, glasses intended for use in high performance optical instruments where the required value of an index can be as exact as 1×10-6. Compensation for minor variations of composition are made by controlled rates of annealing for such optical glasses; therefore, the ability to measure index to six decimal places can be a necessity; however, for most commercial and experimental glasses, standard annealing schedules appropriate to each are used to limit internal stress and less rigorous methods of test for refractive index are usually adequate. The refractive indices of glass ophthalmic lens pressings are held to 5×10-4 because the tools used for generating the figures of ophthalmic lenses are made to produce curvatures that are related to specific indices of refraction of the lens materials.  
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where vD is defined in 3.2 and nD, nF, and nC are the indices of refraction at the emission lines defined in 3.2.  
4.2.1 Some modern usage sp...
SCOPE
1.1 This guide identifies and describes seven test methods for measuring the index of refraction of glass, with comments relevant to their uses such that an appropriate choice of method can be made. Four additional methods are mentioned by name, and brief descriptive information is given in Annex A1. The choice of a test method will depend upon the accuracy required, the nature of the test specimen that can be provided, the instrumentation available, and (perhaps) the time required for, or the cost of, the analysis. Refractive index is a function of the wavelength of light; therefore, its measurement is made with narrow-bandwidth light. Dispersion is the physical phenomenon of the variation of refractive index with wavelength. The nature of the test-specimen refers to its size, form, and quality of finish, as described in each of the methods herein. The test methods described are mostly for the visible range of wavelengths (approximately 400 μm to 780 μm); however, some methods can be extended to the ultraviolet and near infrared, using radiation detectors other than the human eye.  
1.1.1 List of test methods included in this guide:
1.1.1.1 Becke line (method of central illumination),
1.1.1.2 Apparent depth of microscope focus (the method of the Duc de Chaulnes),
1.1.1.3 Critical Angle Refractometers (Abbe type and Pulfrich type),
1.1.1.4 Metricon2 system,
1.1.1.5 Vee-block refractometers,
1.1.1.6 Prism spectrometer, and
1.1.1.7 Specular reflectance.  
1.1.2 Test methods presented by name only (see Annex A1):
1.1.2.1 Immersion refractometers,
1.1.2.2 Interferometry,
1.1.2.3 Ellipsometry, and
1.1.2.4 Method of oblique illumination.  
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SCOPE
1.1 These test methods cover the measurement of solar energy transmittance and reflectance (terrestrial) of materials in sheet form. Method A, using a spectrophotometer, is applicable for both transmittance and reflectance and is the referee method. Method B is applicable only for measurement of transmittance using a pyranometer in an enclosure and the sun as the energy source. Specimens for Method A are limited in size by the geometry of the spectrophotometer while Method B requires a specimen 0.61 m2 (2 ft2). For the materials studied by the drafting task group, both test methods give essentially equivalent results.  
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4.1 Sampling of decorated glass containers for the TCLP can vary greatly, resulting from the size and shape of the article relative to the amount of ceramic decoration on the ware. Breaking the glass can cause some of the pieces to have no decoration on them, and others to be heavily decorated and more likely to leach lead and cadmium under the TCLP test. This method provides an effective tool to homogenize the glass containers so that reproducible results can be attained from the TCLP test.
SCOPE
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1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C148-17(2022)(Test Method)
Standard Test Methods for Polariscopic Examination of Glass Containers

SIGNIFICANCE AND USE
4.1 These two test methods are provided for evaluating the quality of annealing. These test methods can be used in the quality control of glass containers or other products made of similar glass compositions, where the degree of annealing must be verified to ensure quality products. These test methods apply to glass containers manufactured from commercial soda-lime-silica glass compositions.
SCOPE
1.1 These test methods describe the determination of relative optical retardation associated with the state of anneal of glass containers. Two alternative test methods are covered as follows:    
Sections  
Test Method A—Comparison with Reference Standards
Using a Polariscope  
6 – 9  
Test Method B—Determination with Polarimeter  
10 – 12  
1.2 Test Method A is useful in determining retardations less than 150 nm, while Test Method B is useful in determining retardations less than 565 nm.  
Note 1: The apparent temper number as determined by these test methods depends primarily on (1) the magnitude and distribution of the residual stress in the glass, (2) the thickness of the glass (optical path length at the point of grading), and (3) the composition of the glass. For all usual soda-lime silica bottle glass compositions, the effect of the composition is negligible. In an examination of the bottom of a container, the thickness of glass may be taken into account by use of the following formula, which defines a real temper number, TR, in terms of the apparent temper number, TA, and the bottom thickness, t:
This thickness should be measured at the location of the maximum apparent retardation. Interpretation of either real or apparent temper number requires practical experience with the particular ware being evaluated.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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