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ASTM E3281-21

(Guide)

Standard Guide for NAPL Mobility and Migration in Sediments – Screening Process to Categorize Samples for Laboratory NAPL Mobility Testing

Standard Guide for NAPL Mobility and Migration in Sediments – Screening Process to Categorize Samples for Laboratory NAPL Mobility Testing

SIGNIFICANCE AND USE
4.1 NAPLs (for example, chlorinated solvents, petroleum products, and creosote) can be emplaced in sediments through a variety of mechanisms (Guide E3248). Dense non-aqueous phase liquids (DNAPLs) are more dense than water, whereas light non-aqueous phase liquids (LNAPLs) are less dense than water.  
4.2 Standardized guidance and test methods currently exist for assessing NAPL mobility at upland sites, from organizations such as ASTM (Guides E2531 and E2856), Interstate Technology & Regulatory Council (1)3 and the American Petroleum Institute (2, 3).  
4.3 Guide E3248 provides guidance regarding when a NAPL movement evaluation is warranted. After confirming that NAPL is present and evaluating nature and extent as appropriate, the next step in any NAPL movement evaluation is to evaluate if NAPL is mobile or immobile at the pore scale—this is done using tiered or weight of evidence (WOE) approaches. This guide provides a structured process to select samples to submit to the laboratory for NAPL mobility testing that is part of a NAPL movement evaluation.  
4.4 This guide may be used by various parties involved in sediment corrective action programs, including regulatory agencies, project sponsors, environmental consultants, toxicologists, risk assessors, site remediation professionals, environmental contractors, and other stakeholders.  
4.5 This guide should be used in conjunction with other reference material (refer to Section 2 and References) that direct the user in developing and implementing sediment assessment programs.  
4.6 This guide is related to Guide E3163, concerning sediment analytical techniques used during sediment programs. It is related to Guide E3248, which discusses generic models for the emplacement and advection of NAPL in sediments.  
4.7 This guide does not replace the need for engaging competent persons to evaluate NAPL emplacement and movement in sediments. Activities necessary to develop a conceptual site model should be conducted by p...
SCOPE
1.1 This guide is designed for general application at a wide range of sediment sites where non-aqueous phase liquid (NAPL) is present or suspected to be present in the sediment. This guide describes a process to use field screening methods, specifically visual observations, and the results of shake tests, to categorize the relative amount of NAPL present in a sample. This categorization can then be utilized to select co-located sediment samples for laboratory testing to determine if the NAPL in the sample interval is mobile or immobile at the pore scale, or any other chemical or physical testing.  
1.1.1 There is no current industry standard methodology to select sediment samples for laboratory NAPL mobility testing; the use of different methodologies is possible. This guide focuses on a selection process that uses visual observations and shake tests. This process has the advantage of being simple to use and, if applied in a disciplined manner, has been demonstrated to provide good results in the field.  
1.2 This guide is intended to inform, complement, and support characterization and remedial efforts performed under international, federal, state, and local environmental programs but not supersede local, state, federal, or international regulations. The users of this guide should review existing information and data available for a sediment site to determine applicable regulatory agency requirements and the most appropriate entry point into and use of this guide.  
1.3 ASTM International (ASTM) standard guides are not regulations; they are consensus standard guides that may be followed voluntarily to support applicable regulatory requirements. This guide may be used in conjunction with other ASTM guides developed for assessing sediment sites.  
1.4 This guide does not address methods and means of sample collection (Guide E3163).  
1.5 Units—The values stated in SI or CGS units are to be regarded as the standard. N...

General Information

Status
Historical
Publication Date
31-Mar-2021
ICS
13.080.01 - Soil quality and pedology in general
Technical Committee
E50 - Environmental Assessment, Risk Management and Corrective Action
Drafting Committee
E50.04 - Corrective Action
Current Stage
Ref Project

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ASTM E3281-21 - Standard Guide for NAPL Mobility and Migration in Sediments – Screening Process to Categorize Samples for Laboratory NAPL Mobility TestingASTM E3281-21 - Standard Guide for NAPL Mobility and Migration in Sediments – Screening Process to Categorize Samples for Laboratory NAPL Mobility Testing
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ASTM E3281-21 - Standard Guide for NAPL Mobility and Migration in Sediments – Screening Process to Categorize Samples for Laboratory NAPL Mobility Testing
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E3281 − 21
Standard Guide for
NAPL Mobility and Migration in Sediments – Screening
Process to Categorize Samples for Laboratory NAPL
1
Mobility Testing
This standard is issued under the fixed designation E3281; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.5 Units—The values stated in SI or CGS units are to be
regarded as the standard. No other units of measurement are
1.1 This guide is designed for general application at a wide
included in this standard.
range of sediment sites where non-aqueous phase liquid
1.6 This standard does not purport to address all of the
(NAPL) is present or suspected to be present in the sediment.
safety concerns, if any, associated with its use. It is the
This guide describes a process to use field screening methods,
responsibility of the user of this standard to establish appro-
specifically visual observations, and the results of shake tests,
priate safety, health, and environmental practices and deter-
tocategorizetherelativeamountofNAPLpresentinasample.
mine the applicability of regulatory limitations prior to use.
This categorization can then be utilized to select co-located
1.7 This international standard was developed in accor-
sediment samples for laboratory testing to determine if the
dance with internationally recognized principles on standard-
NAPLin the sample interval is mobile or immobile at the pore
scale, or any other chemical or physical testing. ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
1.1.1 There is no current industry standard methodology to
select sediment samples for laboratory NAPLmobility testing; mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
the use of different methodologies is possible. This guide
focusesonaselectionprocessthatusesvisualobservationsand
2. Referenced Documents
shake tests. This process has the advantage of being simple to
2
use and, if applied in a disciplined manner, has been demon-
2.1 ASTM Standards:
strated to provide good results in the field.
D2487Practice for Classification of Soils for Engineering
Purposes (Unified Soil Classification System)
1.2 This guide is intended to inform, complement, and
D2488Practice for Description and Identification of Soils
support characterization and remedial efforts performed under
(Visual-Manual Procedures)
international, federal, state, and local environmental programs
D7203Practice for Screening Trichloroethylene (TCE)-
but not supersede local, state, federal, or international regula-
Contaminated Media Using a Heated Diode Sensor
tions. The users of this guide should review existing informa-
E2531Guide for Development of Conceptual Site Models
tion and data available for a sediment site to determine
and Remediation Strategies for Light Nonaqueous-Phase
applicableregulatoryagencyrequirementsandthemostappro-
Liquids Released to the Subsurface
priate entry point into and use of this guide.
E2856Guide for Estimation of LNAPL Transmissivity
1.3 ASTM International (ASTM) standard guides are not
E3163Guide for Selection and Application of Analytical
regulations; they are consensus standard guides that may be
Methods and Procedures Used during Sediment Correc-
followed voluntarily to support applicable regulatory require-
tive Action
ments. This guide may be used in conjunction with other
E3248GuideforNAPLMobilityandMigrationinSediment
ASTM guides developed for assessing sediment sites.
–Conceptual Models for Emplacement and Advection
1.4 This guide does not address methods and means of
F2534Guide for Visually Estimating Oil Spill Thickness on
sample collection (Guide E3163).
Water
1
ThisguideisunderthejurisdictionofASTMCommitteeE50onEnvironmental
2
Assessment, Risk Management and CorrectiveAction and is the direct responsibil- For referenced ASTM standards, visit the ASTM website, www.astm.org, or
ity of Subcommittee E50.04 on Corrective Action. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Current edition approved April 1, 2021. Published June 2021. DOI: 10.1520/ Standards volume information, refer to the standard’s Document Summary page on
E3281–21 the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E3281 − 21
3. Terminology 4.5 This guide should be used in conjunction with other
reference material (refer to Section 2 and References) that
3.1 Definitions:
direct the user in developing
...

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4.1 Hydrophobic organic liquids (for example, petroleum hydrocarbons, coal tars) may exist in the environment for long periods of time as NAPLs. Standardized guidance and test methods do not exist to assess NAPL movement (both pore-scale mobility and NAPL body-scale migration) in sediment. Literature searches have resulted in a limited body of available and applicable research. Current research has focused on site-specific sediment NAPL movement evaluation approaches.  
4.2 Standardized guidance and test methods currently exist for assessing NAPL mobility and migration at upland sites, from organizations such as ASTM International (Guides E2531 and E2856), Interstate Technology and Regulatory Council (2), and the American Petroleum Institute (3, 4). Approaches commonly used in upland sites may or may not be applicable for any given sediment site. This guide provides perspectives on the applicability of various methodologies for specific sediment conditions.  
4.3 This guide describes various methodologies that are useful in sediment NAPL movement evaluation, such as laboratory test methods, calculation approaches, and field observation interpretation. The guide then provides frameworks to evaluate the data generated from these methodologies to determine if the NAPL observed in the sediments under in situ conditions exhibits movement of any kind.  
4.4 Important exposure pathways in upland sites are usually not applicable to sediment sites. The U.S. Environmental Protection Agency notes, “Contaminants in the biologically active layer of the surface sediment at a site often drive exposure” (5). In aquatic environments, benthic organisms live in the surface sediment to maintain access to oxygenated overlying water. These benthic organisms are at the base of the food chain. If NAPL in subsurface sediment is not migrating, the NAPL will not move into the surface sediment and result in exposure to benthic organisms. NAPL that is stable and only present in subsurface se...
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1.1 This guide discusses methodologies that can be applied to evaluate the potential for the movement (that is, pore-scale mobility or NAPL body-scale migration) of non-aqueous phase liquid (NAPL) in sediments. NAPL movement assessment in sediments is significantly different than in upland soils. As such, the frameworks for evaluating NAPL movement in upland soils have limited applicability for sediments. In particular, because upland NAPL conceptual site models may not be applicable to many sediment sites, this guide provides a framework to evaluate whether NAPL is mobile (at the pore scale) or migrating (at the NAPL body scale) in sediments.  
1.2 Assessment of the potential for NAPL to move in sediment is important for several reasons, including (but not limited to) evaluation of risk to potential receptors, the need for potential remedial action, and potential remedial strategies. For example, if the NAPL is migrating, sensitive receptors may be impacted and this will influence the choice and timing of any remedy selected for an area of the sediment site. If the NAPL is not mobile or migrating, then remedial actions may not be warranted.  
1.3 This guide is applicable at sediment sites where NAPL has been identified in the sediment by various screening methods and the need for a NAPL movement evaluation is warranted (Guide E3248).  
1.4 Petroleum hydrocarbon, coal tar, and other tar NAPLs (including fuels, oils, and creosote) are the primary focus of this guide. These forms of contamination are commonly related to historical operations at refineries, petroleum distribution terminals, manufactured gas plants (MGPs), and various large industrial sites.  
1.5 Although certain technical aspects of this guide apply to other NAPLs (for example, dense NAPLs [DNAPLs] such as chlorinated hydrocarbon solvents), this guide does not completely address the additional complexities of those DNAPLs.  
1.6 The goal of this guide...

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Standard Guide for NAPL Mobility and Migration in Sediments – Screening Process to Categorize Samples for Laboratory NAPL Mobility Testing

SIGNIFICANCE AND USE
4.1 NAPLs (for example, chlorinated solvents, petroleum products, and creosote) can be emplaced in sediments through a variety of mechanisms (Guide E3248). Dense non-aqueous phase liquids (DNAPLs) are more dense than water, whereas light non-aqueous phase liquids (LNAPLs) are less dense than water.  
4.2 Standardized guidance and test methods currently exist for assessing NAPL mobility at upland sites, from organizations such as ASTM (Guides E2531 and E2856), Interstate Technology & Regulatory Council (1)3 and the American Petroleum Institute (2, 3).  
4.3 Guide E3248 provides guidance regarding when a NAPL movement evaluation is warranted. After confirming that NAPL is present and evaluating nature and extent as appropriate, the next step in any NAPL movement evaluation is to evaluate if NAPL is mobile or immobile at the pore scale—this is done using tiered or weight of evidence (WOE) approaches. This guide provides a structured process to select samples to submit to the laboratory for NAPL mobility testing that is part of a NAPL movement evaluation.  
4.4 This guide may be used by various parties involved in sediment corrective action programs, including regulatory agencies, project sponsors, environmental consultants, toxicologists, risk assessors, site remediation professionals, environmental contractors, and other stakeholders.  
4.5 This guide should be used in conjunction with other reference material (refer to Section 2 and References) that direct the user in developing and implementing sediment assessment programs.  
4.6 This guide is related to Guide E3163, concerning sediment analytical techniques used during sediment programs. This relates to Guide E3248, which discusses generic models for the emplacement and advection of NAPL in sediments. It is related to Guide E3268, which describes sample collection, field screening and sample handling considerations in NAPL movement evaluations. And this is related to Guide E3282, which describes evaluation met...
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1.1 This guide is designed for general application at a wide range of sediment sites where non-aqueous phase liquid (NAPL) is present or suspected to be present in the sediment. This guide describes a process to use field screening methods, specifically visual observations, and the results of shake tests, to categorize the relative amount of NAPL present in a sample. This categorization can then be utilized to select co-located sediment samples for laboratory testing to determine if the NAPL in the sample interval is mobile or immobile at the pore scale, or any other chemical or physical testing.  
1.1.1 There is no current industry standard methodology to select sediment samples for laboratory NAPL mobility testing; the use of different methodologies is possible. This guide focuses on a selection process that uses visual observations and shake tests. This process has the advantage of being simple to use and, if applied in a disciplined manner, has been demonstrated to provide good results in the field.  
1.2 This guide is intended to inform, complement, and support characterization and remedial efforts performed under international, federal, state, and local environmental programs but not supersede local, state, federal, or international regulations. The users of this guide should review existing information and data available for a sediment site to determine applicable regulatory agency requirements and the most appropriate entry point into and use of this guide.  
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4.1 Ebullition is ubiquitous in sediment and is primarily a significant concern when there is associated NAPL/contaminant transport, resulting in exposure risk to humans, ecological receptors, or both. Ebullition may also be a concern when capping has been chosen as part of a site remedy.  
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1.1 This guide addresses the processes that lead to (or influence) ebullition-facilitated nonaqueous phase liquid (NAPL)/contaminant transport, methods for quantifying that transport, considerations for sample timing, sampling procedures, and use of results in extrapolating an annual ebullition-facilitated NAPL/contaminant load to a site, or a portion of a site. This guide is not intended to address remediation of sites where ebullition-facilitated transport of NAPL/contaminants is occurring, fate and transport of contaminants subsequent to the ebullition transport mechanism, the measurement of contaminant concentrations within the gas bubbles, ebullition-associated human health and ecological risk, NAPL advection, or determining the depth of ebullition below the mudline. Additionally, gas transport without NAPL/contaminants is possible in areas with gas generation and limited NAPL contamination of the sediment, which is covered in this guide. Ebullition should be evaluated at sites where sediment capping is anticipated.  
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SIGNIFICANCE AND USE
4.1 Many contaminants, including chlorinated solvents and petroleum products, enter the subsurface in the form of an immiscible liquid, known as a NAPL. Understanding the potential emplacement and transport mechanism for NAPL in sediment is an important element of an overall conceptual site model (CSM) that forms a basis for (1) investigating the nature and extent of NAPL, (2) evaluating if (and how) human and ecological receptors may be exposed to NAPL, and (3) assessing remedial alternatives. In addition, demonstrating the potential movement of NAPL in sediments is hampered by the lack of standardized terminology and characterization protocols, thus necessitating this guide.  
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1.5 BMPs implemented under this guide should address all three aspects of sustainability: environmental, economic and social, while assuring that human health and safety as well as ecological risks are addressed. The goal of implementing BMPs is to take actions to address the sustainable objectives identified for the site.  
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SIGNIFICANCE AND USE
4.1 Understanding the potential emplacement and transport mechanism for NAPL in sediment is an important element of an overall conceptual site model (CSM) that forms a basis for (1) investigating the nature and extent of NAPL, (2) evaluating if (and how) human and ecological receptors may be exposed to NAPL, and (3) assessing remedial alternatives. In addition, demonstrating the potential movement of NAPL in sediments to regulators and other stakeholders has been historically hampered by the lack of standardized terminology and characterization protocols. The complexity of NAPL movement in sediment, and the lack of agreed upon methods for analysis and interpretation of site data, has led to uncertainty in corrective action decision-making. This has sometimes resulted in misleading expectations about remedial outcomes. The emplacement and transport mechanisms for NAPL in sediments are different from those in upland environments, due to a variety of physical, geochemical, and biological differences between sediment and upland environments, thus necessitating this guide.  
4.2 This guide is intended to supplement the CSM developed according to the principles outlined in the contaminated sites conceptual site model Guide E1689, the standard guide for developing a CSM for Light Non-Aqueous Phase Liquid (LNAPL) sites Guide E2531, and the Risk-Based Corrective Action (RBCA) Guides E1739 and E2081, by considering conditions for NAPL emplacement and movement (that is, advection) that are unique to a sediment environment. This guide will aid users in understanding the unique and fundamental characteristics of sediment environments that influence the occurrence and behavior of NAPL in sediments. Understanding the sources of NAPL encountered in sediment, the mechanisms for NAPL to become emplaced in sediments, and the site characteristics that influence the advective movement of NAPL within the sediment column will aid in identifying specific data requirements necessary to inv...
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1.1 This guide is designed for general application to a wide range of sediment sites where non-aqueous phase liquid (NAPL) is present or suspected to be present. This guide describes multiple emplacement mechanisms that can result in NAPL presence within the sediment stratigraphic profile and how the characteristics of the sediment, aquatic environment, and NAPL properties influence NAPL movement within sediments. This guide provides example conceptual models for NAPL emplacement in sediments in order to establish a common framework that can be used to assess conditions influencing NAPL movement by means of advection.  
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5.3 This test method is a performance test, but can also be used for acceptance testing to determine product conformance to project specifications. For project-specific conformance, unique project-specific conditions should be considered. Caution is advised since information regarding laboratory specific precision is incomplete at this time, and differences in soil and other environmental and geotechnical conditions may affect ECP performance.  
5.4 This standard can also be used as a comparative tool for evaluating the erosion control characteristics of different ECPs and can also be used to gain agency approvals.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method is used to evaluate the ability of erosion control products (ECP) to protect slopes from rainfall-induced erosion using an adjustable tilting bed slope. The standard slopes range from 2:1 to 4:1 (H:V) having a target rainfall intensity of 3.5 in./h [90 mm/h].  
1.2 There are three main elements the ECPs must have the ability to perform: 1. Absorb the impact force of raindrops, thereby reducing soil particle loosening and detachment through “splash” mechanisms; 2. Slow runoff and encourage infiltration, thereby reducing soil particle displacement and transport through “overland flow” mechanisms; and 3. Trap soil particles beneath the ECP. When comparing data from different ECPs under consideration, it is important to keep the test conditions the same for the ECPs being evaluated, for example, the rainfall intensity rate and the slope.  
1.3 The results of this test method can be used to evaluate performance and acceptability, and can be used to compare the effectiveness of different ECPs. This method provides a comparative evaluation of an ECP to baseline bare soil conditions under controlled and documented conditions. This test method can provide information about a product that is under consideration for a specific application where no performance information currently exists.  
1.4 This test method covers the use of three different soil types, ECP installation: sprayed, rolled, or dry applied, and a runoff collection procedure. This test is typically performed indoors, but may be performed outside as long as certain requirements are met. Partially enclosed facilities are acceptable providing the environmental conditions are met.  
1.5 Units—The values stated in either inch-pound units or SI units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Reporting of test results in units other than inch-pound shall not be regarded as nonconformance with this standard.  
1.5.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In the system, the pound (lbf) represents a unit of force (weight), while the units for mass is slugs. The slug unit is n...

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ASTM
ASTM D7047-23(Test Method)
Standard Test Method for Swell Volume of Plantago Insularis (Ovata, Psyllium)

SIGNIFICANCE AND USE
5.1 The meaning of the test is related to the manufacturing and end use of the material, to determine characteristics of products.  
5.2 A manufacturer of raw psyllium will base the grade of psyllium produced on multiple properties of which swell volume is one.  
5.3 Erosion control contractors and those writing erosion control specifications will use this test method to evaluate the grade of psyllium being used as a hydraulically applied erosion control product. The swell volume will help determine the application rate of psyllium needed to meet the erosion control performance criteria.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 The purpose of this quantitative test method is to provide a means of determining the swell volume plantago insularis (Ovata, Psyllium).  
1.2 The volume of swell reflects the amount of hydrophilic mucilloid present in psyllium. The higher the grade of psyllium the higher the swell volume, thus a greater percent of mucilloid present. For the erosion control industry, the higher the swell volume of the psyllium the greater it’s bonding strength and relative performance.  
1.3 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.4.1 For purposes of comparing, a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal or significant digits in the specified limits.  
1.4.2 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user's objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D6519/D6519M-23(Practice)
Standard Practice for Sampling of Soil Using the Hydraulically Operated Stationary Piston Sampler

SIGNIFICANCE AND USE
5.1 Hydraulically operated stationary piston samplers are used to gather soil samples for laboratory or field testing and analysis for geologic investigations, soil chemical composition studies, and water quality investigations. The sampler is sometimes used when attempts to recover unstable soils with thin-walled tubes, Practice D1587/D1587M, are unsuccessful. Examples of a few types of investigations in which hydraulic stationary piston samplers may be used include building site foundation studies containing soft sediments, highway and dam foundation investigations where softer soil formation need evaluation, wetland crossings utilizing floating structures, and hazardous waste site investigations. Hydraulically operated stationary piston samplers provide specimens necessary to determine the physical and chemical composition of soils and, in certain circumstances, contained pore fluids (see Guide D6169/D6169M).  
5.2 Hydraulically operated stationary piston samplers can provide relatively intact soil samples of soft or loose formation materials for testing to determine accurate information on the physical characteristics of that soil. Samples of soft formation materials can be tested to determine numerous soil characteristics such as; soil stratigraphy, particle size, water content, permeability, shear strength, compressibility, and so forth. The chemical composition of soft formation soils can also be determined from the sample if provisions are made to ensure that clean, decontaminated tools are used in the sample gathering procedure. Field-extruded samples can be field-screened or laboratory-analyzed to determine the chemical composition of soil and contained pore fluids. Using sealed or protected sampling tools, cased boreholes, and proper advancement techniques can help in the acquisition of good representative samples. A general knowledge of subsurface conditions at the site is beneficial.  
5.3 The use of this practice may not be the correct method for inv...
SCOPE
1.1 This practice covers a procedure for sampling of cohesive, organic, or fine-grained soils, or combination thereof, using a thin-walled metal tube that is inserted into the soil formation by means of a hydraulically operated piston. It is used to collect relatively intact soil samples suitable for laboratory tests to determine structural and chemical properties for geotechnical and environmental site characterizations.  
1.1.1 Guidance on preservation and transport of samples in accordance with Practice D4220/D4220M may apply. Samples for classification may be preserved using procedures similar to Class A. In most cases, a thin-walled tube sample can be considered as Class B, C, or D. Refer to Guide D6169/D6169M for use of the hydraulically operated stationary piston soil sampler for environmental site characterization. This sampling method is often used in conjunction with rotary drilling methods such as fluid rotary; Guide D5783; and hollow stem augers, Practice D6151/D6151M. Sampling data shall be reported in the field log in accordance with Guide D5434.  
1.2 The hydraulically operated stationary piston sampler is limited to soils and unconsolidated materials that can be penetrated with the available hydraulic pressure that can be applied without exceeding the structural strength of the thin-walled tube. This standard addresses typical hydraulic piston samplers used on land or shallow water in drill holes. The standard does not address specialized offshore samplers for deep marine applications that may or may not be hydraulically operated. This standard does not address operation of other types of mechanically advanced piston samplers. For information on other soil samplers, refer to Guide D6169/D6169M.  
1.3 Units—The values stated in either inch-pound units or SI units [presented in brackets] are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, e...

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ASTM
ASTM D8298/D8298M-23(Test Method)
Standard Test Method for Determination of Erosion Control Products (ECP) Performance in Protecting Slopes from Continuous Rainfall-Induced Erosion Using a Tilted Bed Slope

SIGNIFICANCE AND USE
5.1 This test method utilizes large-scale testing equipment and procedures established at a variety of testing laboratories over the last 30 years.  
5.2 This method is useful in evaluating ECPs and their installation to reduce soil loss and sediment concentrations when exposed to defined rainfall conditions and improving water quality exiting the area disturbed by earthwork activity by reducing suspended solids and turbidity.  
5.3 This test method is a performance test, but can also be used for acceptance testing to determine product conformance to project specifications. For project-specific conformance, unique project-specific conditions should be considered. Caution is advised since information regarding laboratory specific precision is incomplete at this time, and differences in soil and other environmental and geotechnical conditions may affect ECP performance.  
5.4 This standard can also be used as a comparative tool for evaluating the erosion control characteristics of different ECPs and can also be used to gain agency approvals.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method is used to evaluate the ability of erosion control products (ECP) to protect slopes from rainfall-induced erosion using an adjustable tilting bed slope. The standard slopes range from 2.5:1 to 4:1 (H:V) having target rainfall intensities between 4.0 and 5.0 in./h [100 and 125 mm/h].  
1.2 There are three main elements the ECPs must have the ability to perform: 1. Absorb the impact force of raindrops, thereby reducing soil particle loosening and detachment through “splash” mechanisms; 2. Slow runoff and encourage infiltration, thereby reducing soil particle displacement and transport through “overland flow” mechanisms; and 3. Trap soil particles beneath the ECP. When comparing data from different ECPs under consideration, it is important to keep the test conditions the same for the ECPs being evaluated, for example, the rainfall intensity rate and the slope.  
1.3 The results of this test method can be used to evaluate performance and acceptability, and can be used to compare the effectiveness of different ECPs. This method provides a comparative evaluation of an ECP to baseline bare soil conditions under controlled and documented conditions. This test method can provide information about a product that is under consideration for a specific application where no performance information currently exists.  
1.4 This test method covers the use of three different soil types, ECP installation: sprayed, rolled, or dry applied, and a runoff collection procedure. This test is typically performed indoors, but may be performed outside as long as certain requirements are met. Partially enclosed facilities are acceptable providing the environmental conditions are met.  
1.5 Units—The values stated in either inch-pound units or SI units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Reporting of test results in units other than inch-pound shall not be regarded as nonconformance with this standard.  
1.5.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In the system, the pound (lbf) represents a unit of force (weight), while the units for mass is s...

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