Standard Practices for Referencing Suprathreshold Odor Intensity

SCOPE
1.1 These practices are designed to outline a preferred means for referencing the odor intensities of a material in the suprathreshold region.
1.2 The general objective is to reference the odor intensity rather than other odor properties of a sample.  
1.3 These practices are designed to reference the odor intensity on the ASTM Odor Intensity Referencing Scale of any odorous material. This is done by a comparison of the odor intensity of the sample to the odor intensities of a series of concentrations of the reference odorant, which is 1-butanol ( -butanol).  
1.4 The method by which the reference odorant vapors are to be presented for evaluation by the panelists is specified. The manner by which the test sample is presented will depend on the nature of the sample, and is not defined herein.  
1.5 Test sample presentation should be consistent with good standard practice (1)  and should be explicitly documented in the test report.
1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Apr-1999
Technical Committee
Drafting Committee
Current Stage
Ref Project

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ASTM E544-99 - Standard Practices for Referencing Suprathreshold Odor Intensity
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Designation:E544–99
Standard Practices for
1
Referencing Suprathreshold Odor Intensity
This standard is issued under the fixed designation E544; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 3.2 concentration—a series of concentrations of 1-butanol
in odorless air, nitrogen, or the water diluent, made to specific
1.1 These practices are designed to outline a preferred
reference dilutions which serve as the reference scale, volume
means for referencing the odor intensities of a material in the
basis, of 1-butanol diluted air or in water. In the latter case, the
suprathreshold region.
temperature of the solution during the test should be reported.
1.2 The general objective is to reference the odor intensity
3.3 dynamic scale—the reference scale in which vapor
rather than other odor properties of a sample.
dilutions are prepared by continuous mixing of vapors of
1.3 These practices are designed to reference the odor
1-butanol with an odorless gas, such as air, to yield constant
intensity on the ASTM Odor Intensity Referencing Scale of
dilutions of vapor in the gas.
anyodorousmaterial.Thisisdonebyacomparisonoftheodor
3.4 panelists—the individuals who compare the odor inten-
intensity of the sample to the odor intensities of a series of
sity of the sample to the reference scale. These individuals
concentrations of the reference odorant, which is 1-butanol
should be able to do this with a consistency described in 5.5.
(n-butanol).
3.5 perceived (sensory) odor intensity—the intensity of an
1.4 The method by which the reference odorant vapors are
odor sensation which is independent of the knowledge of the
tobepresentedforevaluationbythepanelistsisspecified.The
odorant concentration.
manner by which the test sample is presented will depend on
3.6 sample—a material in any form exhibiting an odor that
the nature of the sample, and is not defined herein.
needs to be measured.
1.5 Testsamplepresentationshouldbeconsistentwithgood
2
3.7 static scale—the reference scale in which dilutions of
standard practice (1) and should be explicitly documented in
1-butanolinwaterarepreparedinflasksandpresentedforodor
the test report.
intensity comparison from the flasks.
1.6 This standard does not purport to address all of the
3.8 suprathreshold odor intensity—perceived (sensory) in-
safety concerns, if any, associated with its use. It is the
tensity of the odor in that intensity region in which the odor is
responsibility of the user of this standard to establish appro-
clearly experienced.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. SeeAnnexA1 for
4. Summary of Practice
specific safety data.
4.1 Thereferenceodorantusedtogenerateanodorintensity
2. Referenced Documents scale is 1-butanol (n-butanol). The reasons for its selection are
summarized in Appendix X1. A geometric progression scale
2.1 ASTM Standards:
3
witharatioof2isrecommended,thatis,ascaleinwhicheach
D1292 Test Method for Odor in Water
reference dilution differs in its 1-butanol concentration from
3. Terminology
the preceding dilution by a factor of 2.
4.2 Two procedures, A and B, are described in these
3.1 ASTM odor intensity referencing scale—a series of
recommended practices. They differ in the method by which
1-butanol dilutions used to establish which concentration
the diluted 1-butanol vapors are prepared.
exhibits an odor intensity matching that of the sample.
NOTE 1—The relationships between the odor intensity of 1-butanol
concentrations in air and in water have not been evaluated. Translation of
Procedure B data to the numerical values of Procedure A is not possible
1
These practices are under the jurisdiction of ASTM Committee E-18 on
at this time.
Sensory Evaluation of Materials and Products and are the direct responsibility of
4.2.1 In Procedure A, hereafter referred to as the dynamic
Subcommittee E18.04 on Fundamentals of Sensory.
Current edition approved April 10, 1999. Published July 1999. Originally
scale method, a dynamic-dilution apparatus is used. This is
published as E544 – 75. Last previous edition E544 – 75(1997).
equipped with a series of sniffing ports from which constant
2
Theboldfacenumbersinparenthesesrefertothelistofreferencesattheendof
concentrationsof1-butanolemergeatconstantvolumetricflow
these recommended practices.
3
Annual Book of ASTM Standards, Vol 11.01. rates in air.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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E544
4.2.2 InProcedure
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