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ASTM D3012-04

(Test Method)

Standard Test Method for Thermal-Oxidative Stability of Propylene Plastics Using a Specimen Rotator Within an Oven

Standard Test Method for Thermal-Oxidative Stability of Propylene Plastics Using a Specimen Rotator Within an Oven

SCOPE
1.1 This test method provides a means for estimating the resistance of polypropylene, in molded form, to accelerated aging by heat in the presence of air using a forced draft oven.
1.2 The stability determined by this test method is not directly related to the suitability of the material for use when different environmental conditions prevail and shall not be used to predict performance.Note 1
The specified thermal levels in this test method are considered sufficiently severe to cause failure of commercial grades of heat-stable polypropylene within a reasonable period of time. If desired, lower temperatures can be applied to estimate the performance of polypropylene with lower heat stabilities.
1.3 The values stated in SI units are to be regarded as the standard. The values in brackets are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.Note 2
This test method and ISO 4577-1983 are technically similar but different in preparation of test specimens, thickness of test specimen, measurement of the number of air flow changes in the ovens, and the number of air changes per hour required.
1.4 The purpose of this appendix is to provide a secondary method for determining the number of air exchanges that occur within the forced draft oven used for measurement of thermal oxidative stability.

General Information

Status
Historical
Publication Date
29-Feb-2004
ICS
83.080.20 - Thermoplastic materials
Technical Committee
D20 - Plastics
Drafting Committee
D20.15 - Thermoplastic Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D3012-00 - Standard Test Method for Thermal-Oxidative Stability of Propylene Plastics Using a Specimen Rotator Within an Oven
Effective Date
01-Mar-2004
Replaced By
ASTM D3012-07 - Standard Test Method for Thermal-Oxidative Stability of Polypropylene Using a Specimen Rotator Within an Oven
Effective Date
01-Mar-2007
Referred By
ASTM D4000-23 - Standard Classification System for Specifying Plastic Materials
Effective Date
01-Mar-2004
Referred By
ASTM D4101-17e1 - Standard Classification System and Basis for Specification for Polypropylene Injection and Extrusion Materials
Effective Date
01-Mar-2004

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ASTM D3012-04 - Standard Test Method for Thermal-Oxidative Stability of Propylene Plastics Using a Specimen Rotator Within an OvenASTM D3012-04 - Standard Test Method for Thermal-Oxidative Stability of Propylene Plastics Using a Specimen Rotator Within an Oven
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ASTM D3012-04 - Standard Test Method for Thermal-Oxidative Stability of Propylene Plastics Using a Specimen Rotator Within an Oven
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D3012–04
Standard Test Method for
Thermal-Oxidative Stability of Polypropylene Using a
1
Specimen Rotator Within an Oven
This standard is issued under the fixed designation D 3012; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope* D 4101 Specification for Polypropylene Injection and Ex-
trusion Materials
1.1 This test method provides a means for estimating the
D 5374 Test Methods for Forced-Convection Laboratory
resistance of polypropylene, in molded form, to accelerated
Ovens for Evaluation of Electrical Insulation
aging by heat in the presence of air using a forced draft oven.
E 1 Specification for ASTM Thermometers
1.2 The stability determined by this test method is not
E 77 Test Method for Inspection and Verification of Ther-
directly related to the suitability of the material for use when
mometers
different environmental conditions prevail and shall not be
E 220 Test Method for Calibration of Thermocouples by
used to predict performance.
Comparison Techniques
NOTE 1—Thespecifiedthermallevelsinthistestmethodareconsidered
E 608 Specification for Metal-Sheathed Base-Metal Ther-
sufficiently severe to cause failure of commercial grades of heat-stable
mocouples
polypropylene within a reasonable period of time. If desired, lower
E 644 Test Methods for Testing Industrial Resistance Ther-
temperatures can be applied to estimate the performance of polypropylene
mometers
with lower heat stabilities.
E 691 Practice for Conducting an Interlaboratory Study to
1.3 The values stated in SI units are to be regarded as the
Determine the Precision of a Test Method
standard. The values in brackets are for information only.
E 1137 Specification for Industrial Platinum Resistance
1.4 This standard does not purport to address all of the
Thermometers
safety concerns, if any, associated with its use. It is the
3
2.2 ISO Standard:
responsibility of the user of this standard to establish appro-
ISO 4577–1983 Plastics—Polypropylene and Propylene
priate safety and health practices and determine the applica-
Copolymers—Determination of Thermal Oxidative Sta-
bility of regulatory limitations prior to use.
bility in Air-Oven Method
NOTE 2—This test method and ISO 4577–1983 are technically similar
ISO 1873 Plastics—Polypropylene and Propylene-
but different in preparation of test specimens, thickness of test specimen,
Copolymer Thermoplastics:
measurement of the number of air flow changes in the ovens, and the
Part 1: Designation
number of air changes per hour required.
Part 2: Determination of Properties
2. Referenced Documents
3. Terminology
2
2.1 ASTM Standards:
3.1 Definitions—The definitions of plastics used in this test
D 618 Practice for Conditioning Plastics and Electrical
method are in accordance with Terminology D 883 unless
Insulating Materials for Testing
otherwise indicated.
D 883 Terminology Relating to Plastics
D 3641 Practice for Injection Molding Test Specimens of
4. Summary of Test Method
Thermoplastic Molding and Extrusion Materials
4.1 Aging is accelerated by exposing the specimens to an
elevated temperature in a forced draft oven equipped with a
1 biaxial or uniaxial rotating specimen holder.
This test method is under the jurisdiction ofASTM Committee D20 on Plastics
and is the direct responsibility of Subcommittee D20.15 on Thermoplastic Materi- 4.2 Visual examination is used to determine the time to
als.
failure. The time to failure of the material is taken as the
Current edition approved March 1, 2004. Published April 2004. Originally
approved in 1972. Last previous edition approved in 2000 as D 3012 - 00.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
the ASTM website. 4th Floor, New York, NY 10036.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D3012–04
number of days after which the specimen shows localized 6.2.3 Thermocouples shall comply with the requirements of
crazing, crumbling, or discoloration, or a combination thereof. Specification E 608 and shall be calibrated in accordance with
Method E 220.
5. Significance and Use 6.2.4 Resistance thermometers shall comply with the re-
quirements of Test Methods E 644 and Specification E 1137,
5.1 U
...

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5.4 Measure the flow rate of a material using any of the conditions listed for the material in X4.1. For many materials, there are specifications that require the use of this test method, but with some procedural modifications that take precedence when adhering to the specification. Therefore, it is advisable to refer to that material specification before using this test method. Table 1 in Classification D4000 lists the ASTM materials standards that currently exist. An alternative test method for poly (vinyl chloride) (PVC) compounds is found in Test Method D3364.  
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ASTM D2561-17(2023)(Test Method)
Standard Test Method for Environmental Stress-Crack Resistance of Blow-Molded Polyethylene Containers

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5.1 When properly used, these procedures serve to isolate such factors as material, blow-molding conditions, post-treatment, and so forth, on the stress-crack resistance of the container.  
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5.3 Results can be used for estimating the shelf life of blow-molded containers in terms of their resistance to environmental stress cracking provided this is done against a rigorous background of practical field experience and reproducible test data.
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1.1 Under certain conditions of stress, and in the presence of environments such as soaps, wetting agents, oils, or detergents, blow-molded polyethylene containers exhibit mechanical failure by cracking at stresses appreciably below those that would cause cracking in the absence of these environments.  
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1.2.2 Procedure B, Stress-Crack Resistance of a Specific Container to Polyoxyethylated Nonylphenol (CAS 68412-54-4), a Stress-Cracking Agent—The conditions of test described in this procedure are designed for testing containers made from Class 3 polyethylene Specification D4976. Therefore, this procedure is recommended for containers made from Class 3 polyethylene only. This procedure is particularly useful for determining the effect of resin on the stress-crack resistance of the container.  
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1.1 This specification covers poly(ether ketone ketone) materials, commonly referred to as PEKK, which are suitable for molding, extrusion, composites, powder coating and additive manufacturing. Only materials in this Class 6-8 are covered by this specification. This classification system provides requirements for the use of regrind or reprocessed materials.  
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1.4 This classification system and subsequent line callout (specification) are intended to provide means of calling out poly(ether ketone ketone) materials used in the fabrication of end items or parts.  
1.5 Poly(ether ketone ketone) (PEKK) is a member of the poly (aryl ether ketone) or PAEK polymer family. PEKK has a broad range of repeat unit combinations of Isophthaloyl and Terephthaloyl repeat units. This standard classifies the polymer options.  
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1.4 This test method is valid for a wide range of frequencies, typically from 0.01 Hz to 100 Hz.  
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1.6 Test data obtained by this test method are relevant and appropriate for use in engineering design.  
1.7 The values stated in ...

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5.1 These procedures provide a means to assess the drop impact resistance of the group or lot of blown containers from which the test specimens were selected.  
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Note 1: There is no known ISO equivalent to this standard.  
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Standard Test Method for Volatile Matter (Including Water) of Vinyl Chloride Resins

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5.1 The quantity of volatile components in a vinyl chloride resin can be established by this test method. This test method does not identify the components.
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1.1 This test method covers the quantitative determination of the volatile matter (including water) present in vinyl chloride resins.  
1.2 The values stated in SI units are to be regarded as standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method is identical ISO 1269.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3275-18(2023)(Classification)
Standard Classification System for E-CTFE-Fluoroplastic Molding, Extrusion, and Coating Materials

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This classification system covers melt processible molding, extrusion, and coating materials of ethylene-chlorotrifluoroethylene (E-CTFE) fluoroplastics. The resin is a copolymer of ethylene and chlorotrifluoroethylene. The classification of ECTFE materials into groups in accordance with their physical appearance, and further into classes based on melt flow rate, is provided. The test specimens shall be subjected to tests to determine their melt flow rate, melting endotherm peak, specific gravity, tensile property, dielectric constant and dissipation factor, and oxygen index.
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1.2 The values stated in SI units, as detailed in IEEE/ASTM SI-10, are to be regarded as standard.  
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4.1 These test methods are suitable for research or as quality control or specification tests.  
4.2 Viscosity measures the resistance of a fluid to uniformly continuous flow without turbulence or other forces.
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1.1 These test methods (A and B) determine the viscosity of polyols in the range from 10 to 100 000 mPa·s(cP) at 25°C. Test Method A is a rotational procedure for determining dynamic viscosity. Test Method B is a general procedure for kinematic viscosity of transparent polyols. (See Note 1.)  
1.2 The values stated in SI units are to be regarded as the standard. Other equivalent units are provided because of current common usage.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Test Method A is equivalent to ISO 3219. Test Method B is equivalent to ISO 3104.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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