Standard Specification for Industrial Grade Aniline (Withdrawn 2003)

SCOPE
1.1 This specification covers industrial grade aniline.
1.2 Consult current OSHA regulations and suppliers' Material Safety Data Sheets for all materials used in this specification.  Note 1-The properties included in this specification are those required to characterize the above material. If additions are deemed necessary, these will be added when their inclusion becomes desirable and the necessary methods become available.

General Information

Status
Withdrawn
Publication Date
09-Dec-1997
Withdrawal Date
09-Jan-2003
Current Stage
Ref Project

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Technical specification
ASTM D3264-97 - Standard Specification for Industrial Grade Aniline (Withdrawn 2003)
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 3264 – 97
Standard Specification for
Industrial Grade Aniline
This standard is issued under the fixed designation D 3264; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope Determine Conformance with Specifications
E 203 Test Method for Water Using Karl Fischer Reagent
1.1 This specification covers industrial grade aniline.
2.2 Other Document:
1.2 The following applies to all specified limits in this
OSHA Regulations, 29 CFR, paragraphs 1910.1000 and
specification: for purposes of determining conformance with
1920.1200
this specification, an observed value or a calculated value shall
be rounded off “to the nearest unit” in the last right-hand digit
3. Properties
used in expressing the specification limit in accordance with
3.1 Industrial grade aniline shall conform to the following
the rounding-off method of Practice E 29.
requirements:
1.3 Consult current OSHA regulations, suppliers’ Material
ASTM
Safety Data Sheets, and local regulations for all materials used
Property Specification Test
in this specification.
Method
NOTE 1—The properties included in this specification are those re-
Nitrobenzene, max, weight % 0.0002 D 4589
quired to characterize the above material. If additions are deemed
Water, max, weight % 0.05 E 203
A
necessary, these will be added when their inclusion becomes desirable and
Appearance
Color, max, PT/Co scale 100 D 1209
the necessary methods become available.
Distillation range, including the temperature,
184.2°C, at 101.3 kPa (760 mm Hg)
2. Referenced Documents
pressure, max° C
2.1 ASTM Standards: Total 1.0 D 1078
95 % (2.0 mL to 97.0 mL) 0.5
D 1078 Test Method for Distillation Range of Volatile
Relative density, 20/4°C 1.020 to 1.024 D 3505
Organic Liquids
Solidification point, anhydrous basis, min, °C −6.20 D 1493
D 1209 Test Method for Color of Clear Liquids (Platinum- _______________
Cobalt Scale)
A
Clear liquid free of sediment and haze when observed at 18.3 to 25.6°C (65 to
D 1493 Test Method for Solidification Point of Industrial
78°F).
Organic Chemicals
2 NOTE 2—Aniline is light sensitive and will darken on exposure to light
D 3436 Practice for Sampling and Handling Aniline
and air.
D 3505 Test Method for Density or R
...

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