Standard Test Methods for Polymer-Modified Mortar and Concrete

SIGNIFICANCE AND USE
These test methods are used to develop data for comparison with the requirements of Specification C 1438. Standardized procedures are used to compare the properties of specimens made from test mixtures of polymer-modified concrete or mortar with the properties of specimens made from reference mixtures. These test methods are not intended to simulate job conditions.
SCOPE
1.1 Most sections of ASTM test methods and practices for hydraulic cement, mortar and concrete apply to the preparation and testing of specimens made with polymer-modifiers. However, there are some exceptions, most notably curing, that need special procedures in order to develop the properties inherent with polymer-modification. These test methods cover these exceptions.
1.2 For testing polymer-modified mortar and concrete specimens, the procedures in this standard supersede those in the referenced ASTM test methods and practices. These test methods are not applicable to dry, packaged mortar and concrete.
1.4 The values stated in SI units are to be regarded as standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
26-Sep-1999
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
e1
Designation: C 1439 – 99
Standard Test Methods for
Polymer-Modified Mortar and Concrete
This standard is issued under the fixed designation C 1439; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
e NOTE—Editorial corrections were made throughout in October 1999.
1. Scope Concrete by the Volumetric Method
C 185 Test Method for Air Content of Hydraulic Cement
1.1 Most sections of ASTM test methods and practices for
Mortar
hydraulic cement mortar and concrete apply to the preparation
C 192 Practice for Making and Curing ConcreteTest Speci-
and testing of specimens made with polymer-modifiers. How-
mens in the Laboratory
ever, there are some exceptions, most notably curing, that need
C 231 Test Method for Air Content of Freshly Mixed
special procedures in order to develop the properties inherent
Concrete by the Pressure Method
with polymer-modification. These test methods cover these
C 260 Specification forAir-EntrainingAdmixtures for Con-
exceptions.
crete
1.2 Fortestingpolymer-modifiedmortarandconcretespeci-
C 305 PracticeforMechanicalMixingofHydraulicCement
mens, the procedures in this standard supersede those in the
Pastes and Mortars of Plastic Consistency
referenced ASTM test methods and practices. These test
C 403 Test Method for Time of Setting of Concrete Mix-
methods are not applicable to dry, packaged mortar and
tures by Penetration Resistance
concrete.
C 494 Specification for ChemicalAdmixtures for Concrete
1.3 The values stated in SI units are to be regarded as
C 778 Specification for Standard Sand
standard.
C 1202 Test Method for Electrical Indication of Concrete’s
1.4 This standard does not purport to address all of the
Ability to Resist Chloride Ion Penetration
safety concerns, if any, associated with its use. It is the
C 1404 Test Method for Bond Strength of Adhesive Sys-
responsibility of the user of this standard to establish appro-
temsUsedwithConcretesMeasuredbyDirectionTension
priate safety and health practices and determine the applica-
C 1438 Specification for Latex and Powder Polymer Modi-
bility of regulatory limitations prior to use.
fiers for Hydraulic Cement Concrete and Mortar
2. Referenced Documents
3. Significance and Use
2.1 ASTM Standards:
2 3.1 These test methods are used to develop data for com-
C 33 Specification for Concrete Aggregates
parison with the requirements of Specification C 1438. Stan-
C 39 Test Method for Compressive Strength of Cylindrical
2 dardized procedures are used to compare the properties of
Concrete Specimens
specimens made from test mixtures of polymer-modified con-
C 109 Test Method for Compressive Strength of Hydraulic
2 crete or mortar with the properties of specimens made from
Cement Mortar (using 2-inch or 50 mm Cube)
reference mixtures. These test methods are not intended to
C 127 Test Method for Specific Gravity and Absorption of
2 simulate job conditions.
Coarse Aggregate
C 128 Test Method for Specific Gravity and Absorption of
4. Materials
Fine Aggregate
4.1 polymer modifier—the polymer modifier of the required
C 138 Test Method for Unit Weight, Yield, andAir Content
type as furnished by the supplier.
(Gravimetric) of Concrete
4.2 antifoam agent—antifoam agent of the type recom-
C 143 Test Method for Slump of Portland Cement Concrete
mended by the manufacturer, if one is not incorporated in the
C 150 Specification for Portland Cement
polymer modifier.
C 173 Test Method for Air Content of Freshly Mixed
4.3 cement—portland cement conforming to Specification
C 150; if necessary, blend into a single lot prior to test. Use
ThistestmethodisunderthejurisdictionofASTMCommitteeC-9onConcrete same lot for both test and reference mixtures.
andConcreteAggregatesandisthedirectresponsibilityofSubcommitteeC09.44on
Polymer Modified Concrete and Mortars.
Current edition approved July 10, 1999. Published September 1999.
2 3
Annual Book of ASTM Standards, Vol 04.02. Annual Book of ASTM Standards, Vol 04.01.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
C 1439
4.4 aggregates—fine and coarse aggregates for concrete 6. Procedure
conforming to Specification C 33; if necessary, blend each into
6.1 General—Mix concretes and mortars in mechanical
a single lot prior to test. Use same lot for both test and
mixers in batches of such size as to leave about 10 % excess
reference mixtures.
after molding test specimens and testing the unhardened
4.5 graded sand—sand for mortar mixtures conforming to
mixtures.
Specification C 778; if necessary, blend into a single lot prior
6.2 Temperature—Before mixing the concrete or mortar,
to test. Use same lot for both test and reference mixtures.
bring the materials to a uniform temperature, as described in
Practice C 192 for concrete and Test Method C 109 for mortar.
5. Proportioning of Concrete and Mortar Mixtures
6.3 Polymer Modifier—Store the polymer modifier in a dry
5.1 Concrete Mixture Proportioning—Make the test and
place, in moisture-proof containers. Mix the polymer modifier
reference concrete with proportions similar to those shown for
thoroughly before use to ensure uniformity.
a nominal cubic-meter batch.
6.4 Reference Concrete and Mortar—Prepare reference
5.1.1 Test Concrete—Make the test concrete conforming to
concrete or mortar in compliance with Practice C 192 or Test
the following requirements:
Method C 109, respectively.
Parts by Mass, kg
NOTE 1—For trial batches to establish the amounts of water and
Portland cement 390 6 3
A
Fine aggregate 975 6 6 air-entraining admixture to achieve the specified fresh properties, it is
A
Coarse aggregate #8 780 6 6
permissible to add these ingredients in increments and remix the batches.
B
Polymer Modifier
With the first increment of water and air-entraining admixture, if appli-
C
Antifoam agent
cable, follow the mixing procedures specified in the previous section. If
D
Potable water
theslump,orflow,oraircontentislessthanrequired,addadditionalwater
A
Saturated-surface-dry basis as described in Test Methods C 127 and C 128.
or air-entraining admixture and remix the batch. For mortar mixtures,
B
The level recommended by the manufacturer.
remix at slow speed for 30 s. For concrete, remix the batch for 1 min.
C
If the polymer modifier does not contain an antifoam agent, add the type and
Remixing is permitted as often as necessary, provided the elapsed time
dosagerecommendedbythemanufacturer,tothepolymermodifierpriortomixing
from the start of initial mixing to the completion of mixing does not
the concrete.
D
exceed 30 min. Cover the mixer to minimize evaporation when tests of
The amount of water to give a slump of 90 6 15 mm.
fresh properties are being performed. These are trial batches only and are
5.1.2 Reference Concrete—Make the reference concrete
not to be used for testing.
conforming to the following requirements:
Parts by Mass, kg 6.5 Test Mortar—For mixing test mortar, follow Practice
Portland cement 390 6 3
C 305, with the following changes:
A
Fine aggregate 975 6 6
A 6.5.1 For Latex Polymer Modifiers:
Coarse aggregate #8 780 6 6
B
Air-entraining admixture
6.5.1.1 Place all the polymer modifier (with antifoam agent,
C
Potable water
as required) and mixing water in the bowl.
A
Saturated-surface-dry basis as described in Test Methods C 127 and C 128.
6.5.1.2 Add the cement to the bowl; start the mixer and mix
B
The amount of air-entraining admixture, meeting Specification C 260, to give
at the slow speed (140 6 5 r/min) for 30 s.
an air content within 2 % of the test concrete and not exceeding 7.0 %.
C 6.5.2 For Powder Polymer Modifiers:
The amount of water to give a slump of 90 6 15 mm.
6.5.2.1 Blendallthepolymermodifier(withantifoamagent,
5.2 Mortar Mixture Proportioning:
as required) and cement, within1hof mixing the mortar.
5.2.1 Test Mortar—Make the test mortar conforming to the
6.5.2.2 Place the water in the bowl.
following proportions:
6.5.2.3 Add the cement/polymer modifier blend to the
Parts by Mass, kg
Portland cement 100 6 2
water; start the mixer and mix at the slow speed (140 6 5
A
Graded sand 275 6 10
r/min) for 30 s
B
Polymer modifier
C
6.6 Test Concrete—For mixing test concrete, follow Prac-
Antifoam agent
D
Potable water
tice C 192, with the following changes:
A
6.6.1 For Latex Polymer Modifiers—Prior to starting rota-
Saturated-surface-dry basis as described in Test Methods C 128.
B
The level recommended by the manufacturer.
tion of the mixer, add the coarse aggregate, polymer modifier,
C
If the polymer modifier does not contain an antifoam agent, add the type and
and approximately half of the water. Rotate the mixer a few
dosagerecommendedbythemanufacturer,tothepolymermodifierpriortomixing
revolutions, then add the fine aggregate, cement and remaining
the mortar.
D
The amount of water that produces a flow of 105 to 115 % when tested
water. Mix the concrete for 3 min, followed by a 1 minute rest,
according to Test Method C 109.
followed by 1 min final mixing. Cover the open end of the
5.2.2 Reference Mortar—Make the reference mortar con-
mixer during the rest period to prevent evaporation. Take
forming to the following proportions:
precautions to compensate for mortar retained by the mixer so
Parts by Mass, kg
that the discharged batch, as used, will be correctly propor-
Portland cement 100 6 2
A tioned (see Note 2).
Graded sand 275 6 10
B
Air-entraining admixture
6.6.2 For Powder Polymer Modifiers—Blend all the poly-
C
Potable water
mer modifier (with antifoam agent, as required) and cement,
A
Saturated-surface-dry basis as described in Test Methods C 128.
within1hof mixing the concrete. Prior to starting rotation of
B
The amount of air-entraining admixture, meeting Specification C 260, to give
the mixer, add the coarse aggregate and approximately half of
an air content that is within 2 % of the test mortar and not exceeding 12.0 %.
C the water. Rotate the mixer a few revolutions, then add the fine
Amount of water that produces a flow of 105 to 115 % when tested according
to Test Method C 109. aggregate, cement/polymer modifier blend, and
...

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