Standard Test Method for Flexural Strength of Advanced Ceramics at Ambient Temperature—Cylindrical Rod Strength

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ASTM C1684-13 - Standard Test Method for Flexural Strength of Advanced Ceramics at Ambient Temperature—Cylindrical Rod Strength
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1684 − 13
StandardTest Method for
Flexural Strength of Advanced Ceramics at Ambient
1
Temperature—Cylindrical Rod Strength
This standard is issued under the fixed designation C1684; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Estimating Weibull Distribution Parameters forAdvanced
Ceramics
1.1 This test method is for the determination of flexural
C1322Practice for Fractography and Characterization of
strengthofrodshapespecimensofadvancedceramicmaterials
Fracture Origins in Advanced Ceramics
at ambient temperature. In many instances it is preferable to
C1368 Test Method for Determination of Slow Crack
test round specimens rather than rectangular bend specimens,
Growth Parameters of Advanced Ceramics by Constant
especiallyifthematerialisfabricatedinrodform.Thismethod
Stress-Rate Strength Testing at Ambient Temperature
permits testing of machined, drawn, or as-fired rod shaped
E4Practices for Force Verification of Testing Machines
specimens. It allows some latitude in the rod sizes and cross
E337Test Method for Measuring Humidity with a Psy-
sectionshapeuniformity.Roddiametersbetween1.5and8mm
chrometer (the Measurement of Wet- and Dry-Bulb Tem-
and lengths from 25 to 85 mm are recommended, but other
peratures)
1
sizes are permitted. Four-point- ⁄4 point as shown in Fig. 1 is
the preferred testing configuration. Three-point loading is
3. Terminology
permitted. This method describes the apparatus, specimen
requirements, test procedure, calculations, and reporting re- 3.1 Definitions:
quirements. The method is applicable to monolithic or 3.1.1 complete gage section, n—theportionofthespecimen
particulate- or whisker-reinforced ceramics. It may also be between the two outer loading points in four-point flexure and
used for glasses. It is not applicable to continuous fiber- three-point flexure fixtures. C1161
reinforced ceramic composites.
3.1.2 flaw, n—a structural discontinuity in an advanced
1.2 This standard does not purport to address all of the ceramic body that acts as a highly localized stress raiser.
safety concerns, if any, associated with its use. It is the 3.1.2.1 Discussion—The presence of such discontinuities
responsibility of the user of this standard to establish appro-
does not necessarily imply that the ceramic has been prepared
priate safety and health practices and determine the applica- improperly or is faulty. C1322
bility of regulatory limitations prior to use.
3.1.3 flexural strength, n—a measure of the ultimate
strength of a specified beam in bending. C1145, C1161
2. Referenced Documents
1
3.1.4 four-point- ⁄4 point flexure, n—configuration of flex-
2
2.1 ASTM Standards:
uralstrengthtestingwhereaspecimenissymmetricallyloaded
C158Test Methods for Strength of Glass by Flexure (De-
attwolocationsthataresituatedonequarteroftheoverallspan
termination of Modulus of Rupture)
away from the outer two support loading points (see Fig. 1).
C1145Terminology of Advanced Ceramics
C1145, C1161
C1161Test Method for Flexural Strength of Advanced
3.1.5 fracture origin, n—the source from which brittle
Ceramics at Ambient Temperature
fracture commences. C1145, C1322
C1239Practice for Reporting Uniaxial Strength Data and
3.1.6 inert flexural strength, n—ameasureofthestrengthof
specifiedbeaminbendingasdeterminedinanappropriateinert
1 condition whereby no slow crack growth occurs.
This test method is under the jurisdiction of ASTM Committee C28 on
Advanced Ceramics and is the direct responsibility of Subcommittee C28.01 on 3.1.6.1 Discussion—An inert condition may be obtained by
Mechanical Properties and Performance.
using vacuum, low temperatures, very fast test rates, or any
Current edition approved Aug. 1, 2013. Published September 2013. Originally
inert media. C1161
approved in 2008. Last previous edition approved in 2008 as C1684 – 08. DOI:
10.1520/C1684-13.
3.1.7 inherent flexural strength, n—theflexuralstrengthofa
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
material in the absence of any effect of surface grinding or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
other surface finishing process, or of extraneous damage that
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. may be present.The measured inherent strength is in general a
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1684 − 13
1
FIG. 1 Four-Point- ⁄4 Point Flexure Loading Configuration
function of the fle
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1684 − 08 C1684 − 13
Standard Test Method for
Flexural Strength of Advanced Ceramics at Ambient
1
Temperature—Cylindrical Rod Strength
This standard is issued under the fixed designation C1684; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method is for the determination of flexural strength of rod shape specimens of advanced ceramic materials at
ambient temperature. In many instances it is preferable to test round specimens rather than rectangular bend specimens, especially
if the material is fabricated in rod form. This method permits testing of machined, drawn, or as-fired rod shaped specimens. It
allows some latitude in the rod sizes and cross section shape uniformity. Rod diameters between 1.5 and 8 mm and lengths from
1
25 to 85 mm are recommended, but other sizes are permitted. Four-point- ⁄4 point as shown in Fig. 1 is the preferred testing
configuration. Three-point loading is permitted. This method describes the apparatus, specimen requirements, test procedure,
calculations, and reporting requirements. The method is applicable to monolithic or particulate- or whisker-reinforced ceramics.
It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
3
2.1 ASTM Standards:
C158 Test Methods for Strength of Glass by Flexure (Determination of Modulus of Rupture)
C1145 Terminology of Advanced Ceramics
C1161 Test Method for Flexural Strength of Advanced Ceramics at Ambient Temperature
C1239 Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Ceramics
C1322 Practice for Fractography and Characterization of Fracture Origins in Advanced Ceramics
C1368 Test Method for Determination of Slow Crack Growth Parameters of Advanced Ceramics by Constant Stress-Rate
Strength Testing at Ambient Temperature
E4 Practices for Force Verification of Testing Machines
E337 Test Method for Measuring Humidity with a Psychrometer (the Measurement of Wet- and Dry-Bulb Temperatures)
3. Terminology
3.1 Definitions:
3.1.1 complete gage section, n—the portion of the specimen between the two outer loading points in four-point flexure and
three-point flexure fixtures. C1161
3.1.2 flaw, n—a structural discontinuity in an advanced ceramic body that acts as a highly localized stress raiser.
1
This test method is under the jurisdiction of ASTM Committee C28 on Advanced Ceramics and is the direct responsibility of Subcommittee C28.01 on Mechanical
Properties and Performance.
Current edition approved Jan. 1, 2008Aug. 1, 2013. Published January 2008September 2013. Originally approved in 2008. Last previous edition approved in 2008 as C1684
– 08. DOI: 10.1520/C1684-08.10.1520/C1684-13.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3.1.2.1 Discussion—
The presence of such discontinuities does not necessarily imply that the ceramic has been prepared improperly or is faulty. C1322
3.1.3 flexural strength, n—a measure of the ultimate strength of a specified beam in bending. C1145, C1161
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1684 − 13
1
FIG. 1 Four-Point- ⁄4 Point Flexure Loading Configuration
1
3.1.4 four-point- ⁄4 point flexure,n—configuration of flexural strength testing where a specimen is symmetrically loaded at two
locations that are situated one quarter of the overall span away from the outer two support loading points (see Fig. 1). C1145,
C1161
3.1.5 fracture origin, n—the source from which brittle fracture commences. C1145, C1322
3.1.6 inert flexural strength, n—a measure of the strength of specified beam in bending as determined in an appropriate inert
condition whereby no slow crack growth occurs.
3.1.
...

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