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ASTM G30-22

(Practice)

Standard Practice for Making and Using U-Bend Stress-Corrosion Test Specimens

Standard Practice for Making and Using U-Bend Stress-Corrosion Test Specimens

SIGNIFICANCE AND USE
5.1 The U-bend specimen may be used for any metal alloy sufficiently ductile to be formed into the U-shape without mechanically cracking. The specimen is most easily made from strip or sheet but can be machined from plate, bar, castings, or weldments; wire specimens may be used also.  
5.2 Since the U-bend usually contains large amounts of elastic and plastic strain, it provides one of the most severe tests available for smooth (as opposed to notched or precracked) stress-corrosion test specimens. The stress conditions are not usually known and a wide range of stresses exist in a single stressed specimen. The specimen is therefore unsuitable for studying the effects of different applied stresses on stress-corrosion cracking or for studying variables that have only a minor effect on cracking. The advantage of the U-bend specimen is that it is simple and economical to make and use. It is most useful for detecting large differences between the stress-corrosion cracking resistance of (a) different metals in the same environment, (b) one metal in different metallurgical conditions in the same environment, or (c) one metal in several environments.
SCOPE
1.1 This practice covers procedures for making and using U-bend specimens for the evaluation of stress-corrosion cracking in metals. The U-bend specimen is generally a rectangular strip that is bent 180° around a predetermined radius and maintained in this constant strain condition during the stress-corrosion test. Bends slightly less than or greater than 180° are sometimes used. Typical U-bend configurations showing several different methods of maintaining the applied stress are shown in Fig. 1.  
FIG. 1 Typical Stressed U-bends  
1.2 U-bend specimens usually contain both elastic and plastic strain. In some cases (for example, very thin sheet or small diameter wire) it is possible to form a U-bend and produce only elastic strain. However, bent-beam (Practice G39 or direct tension (Practice G49)) specimens are normally used to study stress-corrosion cracking of strip or sheet under elastic strain only.  
1.3 This practice is concerned only with the test specimen and not the environmental aspects of stress-corrosion testing, which are discussed elsewhere (1)2 and in Practices G35, G36, G37, G41, G44, G103 and Test Method G123.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Apr-2022
ICS
77.060 - Corrosion of metals
Technical Committee
G01 - Corrosion of Metals
Drafting Committee
G01.06 - Environmentally Assisted Cracking
Current Stage
Ref Project

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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: G30 − 22
Standard Practice for
Making and Using U-Bend Stress-Corrosion Test
1
Specimens
ThisstandardisissuedunderthefixeddesignationG30;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
1.1 This practice covers procedures for making and using
U-bendspecimensfortheevaluationofstress-corrosioncrack-
2. Referenced Documents
ing in metals. The U-bend specimen is generally a rectangular
3
strip that is bent 180° around a predetermined radius and
2.1 ASTM Standards:
maintained in this constant strain condition during the stress-
E3Guide for Preparation of Metallographic Specimens
corrosiontest.Bendsslightlylessthanorgreaterthan180°are
G1Practice for Preparing, Cleaning, and Evaluating Corro-
sometimes used. Typical U-bend configurations showing sev-
sion Test Specimens
eral different methods of maintaining the applied stress are
G35Practice for Determining the Susceptibility of Stainless
shown in Fig. 1.
Steels and Related Nickel-Chromium-Iron Alloys to
Stress-Corrosion Cracking in Polythionic Acids
1.2 U-bend specimens usually contain both elastic and
G36Practice for Evaluating Stress-Corrosion-Cracking Re-
plastic strain. In some cases (for example, very thin sheet or
sistance of Metals and Alloys in a Boiling Magnesium
small diameter wire) it is possible to form a U-bend and
Chloride Solution
produceonlyelasticstrain.However,bent-beam(PracticeG39
G37Practice for Use of Mattsson’s Solution of pH 7.2 to
or direct tension (Practice G49)) specimens are normally used
Evaluate the Stress-Corrosion Cracking Susceptibility of
tostudystress-corrosioncrackingofstriporsheetunderelastic
Copper-Zinc Alloys
strain only.
G39Practice for Preparation and Use of Bent-Beam Stress-
1.3 This practice is concerned only with the test specimen
Corrosion Test Specimens
and not the environmental aspects of stress-corrosion testing,
G41Practice for Determining Cracking Susceptibility of
2
which are discussed elsewhere (1) and in Practices G35, G36,
Metals Exposed Under Stress to a Hot Salt Environment
G37, G41, G44, G103 and Test Method G123.
G44PracticeforExposureofMetalsandAlloysbyAlternate
1.4 The values stated in SI units are to be regarded as
Immersion in Neutral 3.5% Sodium Chloride Solution
standard. The values given in parentheses after SI units are
G49Practice for Preparation and Use of Direct Tension
providedforinformationonlyandarenotconsideredstandard.
Stress-Corrosion Test Specimens
1.5 This standard does not purport to address all of the G103PracticeforEvaluatingStress-CorrosionCrackingRe-
safety concerns, if any, associated with its use. It is the sistance of Low Copper 7XXX Series Al-Zn-Mg-Cu
responsibility of the user of this standard to establish appro- Alloys in Boiling 6% Sodium Chloride Solution
priate safety, health, and environmental practices and deter- G123TestMethodforEvaluatingStress-CorrosionCracking
mine the applicability of regulatory limitations prior to use. of Stainless Alloys with Different Nickel Content in
Boiling Acidified Sodium Chloride Solution
1.6 This international standard was developed in accor-
dance with internationally recognized principles on standard- G193Terminology and Acronyms Relating to Corrosion
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom- 3. Terminology
3.1 For definitions of corrosion-related terms used in this
practice, see Terminology G193.
1
This practice is under the jurisdiction ofASTM Committee G01 on Corrosion
of Metals and is the direct responsibility of Subcommittee G01.06 on Environmen-
tally Assisted Cracking.
Current edition approved May 1, 2022. Published May 2022. Originally
3
approvedin1972.Lastpreviouseditionapprovedin2016asG30–97(2016).DOI: For referenced ASTM standards, visit the ASTM website, www.astm.org, or
10.1520/G0030-22. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
The boldface numbers in parentheses refer to a list of references at the end of Standards volume information, refer to the standard’s Document Summary page on
this standard. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
G30−22
FIG. 1 Typical Stressed U-bends
4. Summary of Practice 6. Hazards
4.1 This practic
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: G30 − 97 (Reapproved 2016) G30 − 22
Standard Practice for
Making and Using U-Bend Stress-Corrosion Test
1
Specimens
This standard is issued under the fixed designation G30; the number immediately following the designation indicates the year of original
adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A superscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers procedures for making and using U-bend specimens for the evaluation of stress-corrosion cracking in
metals. The U-bend specimen is generally a rectangular strip whichthat is bent 180° around a predetermined radius and maintained
in this constant strain condition during the stress-corrosion test. Bends slightly less than or greater than 180° are sometimes used.
Typical U-bend configurations showing several different methods of maintaining the applied stress are shown in Fig. 1.
1.2 U-bend specimens usually contain both elastic and plastic strain. In some cases (for example, very thin sheet or small diameter
wire) it is possible to form a U-bend and produce only elastic strain. However, bent-beam (Practice G39 or direct tension (Practice
G49)) specimens are normally used to study stress-corrosion cracking of strip or sheet under elastic strain only.
1.3 This practice is concerned only with the test specimen and not the environmental aspects of stress-corrosion testing, which
2
are discussed elsewhere (1) and in Practices G35, G36, G37, G41, G44, G103 and Test Method G123.
1.4 The values stated in SI units are to be regarded as standard. The inch-pound unitsvalues given in parentheses after SI units
are provided for information. information only and are not considered standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
3
2.1 ASTM Standards:
E3 Guide for Preparation of Metallographic Specimens
G1 Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens
4
G15 Terminology Relating to Corrosion and Corrosion Testing (Withdrawn 2010)
1
This practice is under the jurisdiction of ASTM Committee G01 on Corrosion of Metals and is the direct responsibility of Subcommittee G01.06 on Environmentally
Assisted Cracking.
Current edition approved May 1, 2016May 1, 2022. Published June 2016May 2022. Originally approved in 1972. Last previous edition approved in 20152016 as G30 – 97
(2015).(2016). DOI: 10.1520/G0030-97R16.10.1520/G0030-22.
2
The boldface numbers in parentheses refer to a list of references at the end of this standard.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’sstandard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
G30 − 22
FIG. 1 Typical Stressed U-bends
G35 Practice for Determining the Susceptibility of Stainless Steels and Related Nickel-Chromium-Iron Alloys to Stress-
Corrosion Cracking in Polythionic Acids
G36 Practice for Evaluating Stress-Corrosion-Cracking Resistance of Metals and Alloys in a Boiling Magnesium Chloride
Solution
G37 Practice for Use of Mattsson’s Solution of pH 7.2 to Evaluate the Stress-Corrosion Cracking Susceptibility of Copper-Zinc
Alloys
G39 Practice for Preparation and Use of Bent-Beam Stress-Corrosion Test Specimens
G41 Practice for Determining Cracking Susceptibility of Metals Exposed Under Stress to a Hot Salt Environment
G44 Practice for Exposure of Metals and Alloys by Alternate Immersion in Neutral 3.5 % Sodium Chloride Solution
G49 Practice for Preparation and Use of Direct Tension Stress-Corrosion Test Specimens
G103 Practice for Evaluating Stress-Corrosion Cracking Resistance o
...

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SIGNIFICANCE AND USE
3.1 Moist air containing sulfur dioxide quickly produces easily visible corrosion on many metals in a form resembling that occurring in industrial environments. It is therefore a test medium well suited to detect pores or other sources of weakness in protective coatings and deficiencies in corrosion resistance associated with unsuitable alloy composition or treatments.  
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4.1 Polythionic acids are chemically described as H2SxO6, where x is usually 3, 4, or 5 (1)3 though can be more than 50 (2). These acid environments provide a way of evaluating the resistance of stainless steels and related alloys to intergranular stress corrosion cracking. Failure is accelerated by the presence of increasing amounts of intergranular precipitate. Results for the polythionic acid test have not been correlated exactly with those of intergranular corrosion tests (Test Methods G28). Also, this test may not be relevant to stress corrosion cracking in chlorides or caustic environments.  
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4.1 This test environment is believed to give an accelerated ranking of the relative or absolute degree of stress-corrosion cracking susceptibility for different brasses. It has been found to correlate well with the corresponding service ranking in environments that cause stress-corrosion cracking which is thought to be due to the combined presence of traces of moisture and ammonia vapor. The extent to which the accelerated ranking correlates with the ranking obtained after long-term exposure to environments containing corrodents other than ammonia is not at present known. Examples of such environments may be severe marine atmospheres (Cl−), severe industrial atmospheres (predominantly SO2), and super-heated ammonia-free steam.  
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1.1 This practice covers the preparation and use of Mattsson’s solution of pH 7.2 as an accelerated stress-corrosion cracking test environment for brasses (copper-zinc base alloys). The variables (to the extent that these are known at present) that require control are described together with possible means for controlling and standardizing these variables.  
1.2 This practice is recommended only for brasses (copper-zinc base alloys). The use of this test environment is not recommended for other copper alloys since the results may be erroneous, providing completely misleading rankings. This is particularly true of alloys containing aluminum or nickel as deliberate alloying additions.  
1.3 This practice is intended primarily where the test objective is to determine the relative stress-corrosion cracking susceptibility of different brasses under the same or different stress conditions or to determine the absolute degree of stress corrosion cracking susceptibility, if any, of a particular brass or brass component under one or more specific stress conditions. Other legitimate test objectives for which this test solution may be used do, of course, exist. The tensile stresses present may be known or unknown, applied or residual. The practice may be applied to wrought brass products or components, brass castings, brass weldments, and so forth, and to all brasses. Strict environmental test conditions are stipulated for maximum assurance that apparent variations in stress-corrosion susceptibility are attributable to real variations in the material being tested or in the tensile stress level and not to environmental variations.  
1.4 This practice relates solely to the preparation and control of the test environment. No attempt is made to recommend surface preparation or finish, or both, as this may vary with the test objectives. Similarly, no attempt is made to recommend particular stress-corrosion test specimen configurations or methods of applying the stress. Test specimen configurations that may be used are referenced in Practice G30 and STP 425.2  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included ...

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ASTM G186-05(2021)(Test Method)
Standard Test Method for Determining Whether Gas-Leak-Detector Fluid Solutions Can Cause Stress Corrosion Cracking of Brass Alloys

SIGNIFICANCE AND USE
5.1 Brass components are routinely used in compressed gas service for valves, pressure regulators, connectors and many other components. Although soft brass is not susceptible to ammonia SCC, work-hardened brass is susceptible if its hardness exceeds about 54 HR 30T (55HRB) (Rockwell scale). Normal assembly of brass components should not induce sufficient work hardening to cause susceptibility to ammonia SCC. However, it is has been observed that over-tightening of the components will render them susceptible to SCC, and the problem becomes more severe in older components that have been tightened many times. In this test, the specimens are obtained in the hardened condition and are strained beyond the elastic limit to accelerate the tendency towards SCC.  
5.2 It is normal practice to use LDFs to check pressurized systems to assure that leaking is not occurring. LDFs are usually aqueous solutions containing surfactants that will form bubbles at the site of a leak. If the LDF contains ammonia or other agent that can cause SCC in brass, serious damage can occur to the system that will compromise its safety and integrity.  
5.3 It is important to test LDFs to assure that they do not cause SCC of brass and to assure that the use of these products does not compromise the integrity of the pressure containing system.  
5.4 It has been found that corrosion of brass is necessary before SCC can occur. The reason for this is that the corrosion process results in cupric and cuprous ions accumulating in the electrolyte. Therefore, adding copper metal and cuprous oxide (Cu2O) to the aqueous solution accelerates the SCC process if agents that cause SCC are present. However, adding these components to a solution that does not cause SCC will not make stressed brass crack.  
5.5 Repeated application of the solution to the specimen followed by a drying period causes the components in the solution to concentrate thereby further increasing the rate of cracking. This also simulates se...
SCOPE
1.1 This test method covers an accelerated test method for evaluating the tendency of gas leak detection fluids (LDFs) to cause stress corrosion cracking (SCC) of brass components in compressed gas service.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM G39-99(2021)(Practice)
Standard Practice for Preparation and Use of Bent-Beam Stress-Corrosion Test Specimens

SIGNIFICANCE AND USE
5.1 The bent-beam specimen is designed for determining the stress-corrosion behavior of alloy sheets and plates in a variety of environments. The bent-beam specimens are designed for testing at stress levels below the elastic limit of the alloy. For testing in the plastic range, U-bend specimens should be employed (see Practice G30). Although it is possible to stress bent-beam specimens into the plastic range, the stress level cannot be calculated for plastically-stressed three- and four-point loaded specimens as well as the double-beam specimens. Therefore, the use of bent-beam specimens in the plastic range is not recommended for general use.
SCOPE
1.1 This practice covers procedures for designing, preparing, and using bent-beam stress-corrosion specimens.  
1.2 Different specimen configurations are given for use with different product forms, such as sheet or plate. This practice is applicable to specimens of any metal that are stressed to levels less than the elastic limit of the material, and therefore, the applied stress can be accurately calculated or measured (see Note 1). Stress calculations by this practice are not applicable to plastically stressed specimens.  
Note 1: It is the nature of these practices that only the applied stress can be calculated. Since stress-corrosion cracking is a function of the total stress, for critical applications and proper interpretation of results, the residual stress (before applying external stress) or the total elastic stress (after applying external stress) should be determined by appropriate nondestructive methods, such as X-ray diffraction (1).2  
1.3 Test procedures are given for stress-corrosion testing by exposure to gaseous and liquid environments.  
1.4 The bent-beam test is best suited for flat product forms, such as sheet, strip, and plate. For plate material the bent-beam specimen is more difficult to use because more rugged specimen holders must be built to accommodate the specimens. A double-beam modification of a four-point loaded specimen to utilize heavier materials is described in 10.5.  
1.5 The exposure of specimens in a corrosive environment is treated only briefly since other practices deal with this aspect, for example, Practices D1141, G30, G36, G44, G50, and G85. The experimenter is referred to ASTM Special Technical Publication 425 (2).  
1.6 The bent-beam practice generally constitutes a constant strain (deflection) test. Once cracking has initiated, the state of stress at the tip of the crack as well as in uncracked areas has changed, and therefore, the known or calculated stress or strain values discussed in this practice apply only to the state of stress existing before initiation of cracks.  
1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.8  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (For more specific safety hazard information see Section 7 and 12.1.)  
1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM G82-98(2021)e1(Guide)
Standard Guide for Development and Use of a Galvanic Series for Predicting Galvanic Corrosion Performance

SIGNIFICANCE AND USE
4.1 When two dissimilar metals in electrical contact are exposed to a common electrolyte, one of the metals can undergo increased corrosion while the other can show decreased corrosion. This type of accelerated corrosion is referred to as galvanic corrosion. Because galvanic corrosion can occur at a high rate, it is important that a means be available to alert the user of products or equipment that involve the use of dissimilar metal combinations in an electrolyte of the possible effects of galvanic corrosion.  
4.2 One method that is used to predict the effects of galvanic corrosion is to develop a galvanic series by arranging a list of the materials of interest in order of observed corrosion potentials in the environment and conditions of interest. The metal that will suffer increased corrosion in a galvanic couple in that environment can then be predicted from the relative position of the two metals in the series.  
4.3 Types of Galvanic Series:  
4.3.1 One type of Galvanic Series lists the metals of interest in order of their corrosion potentials, starting with the most active (electronegative) and proceeding in order to the most noble (electropositive). The potentials themselves (versus an appropriate reference half-cell) are listed so that the potential difference between metals in the series can be determined. This type of Galvanic Series has been put in graphical form as a series of bars displaying the range of potentials exhibited by the metal listed opposite each bar. Such a series is illustrated in Fig. 1.    
4.4 Use of a Galvanic Series:  
4.4.1 Generally, upon coupling two metals in the Galvanic Series, the more active (electronegative) metal will have a tendency to undergo increased corrosion while the more noble (electropositive) metal will have a tendency to undergo reduced corrosion.  
4.4.2 Usually, the further apart two metals are in the series, and thus the greater the potential difference between them, the greater is the driving force f...
SCOPE
1.1 This guide covers the development of a galvanic series and its subsequent use as a method of predicting the effect that one metal can have upon another metal can when they are in electrical contact while immersed in an electrolyte. Suggestions for avoiding known pitfalls are included.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 5.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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