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ASTM D6463/D6463M-06

(Test Method)

Standard Test Method for Time to Failure of Pressure Sensitive Articles Under Sustained Shear Loading

Standard Test Method for Time to Failure of Pressure Sensitive Articles Under Sustained Shear Loading

SIGNIFICANCE AND USE
This test method measures the cohesive strength of the adhesive on a pressure sensitive article. The time to failure can predict end use properties of pressure sensitive articles such as edge ooze from cold flow; trimming, slitting and die cutting quality; telescoping in tapes; ability to seal packages; and vertical holding power.
This test method is suitable for quality control, development and applications testing.
If the adhesive is not already coated, the adhesive can be coated on smooth, clear polyester (PET) film backing 0.05 mm [0.002 in.] thick. The recommended dry adhesive thickness is 0.025 mm [0.001 in.].
Humidity has a strong effect on time to failure for many pressure sensitive articles. Therefore, humidity should be controlled in accordance with 8.1.2.
SCOPE
1.1 This test method covers the ability of a pressure sensitive article (for example, tape, label, sticker, etc.) to remain adhered to a stainless steel panel under a constant load applied parallel to the bonding surface of the pressure sensitive article.
1.2 Values stated in either SI or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents, therefore, each system must be used independently without combining values in any way.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
28-Feb-2006
ICS
83.180 - Adhesives
Technical Committee
D10 - Packaging
Drafting Committee
D10.14 - Tape and Labels
Current Stage
Ref Project

Relations

Replaces
ASTM D6463-99 - Standard Test Method for Time to Failure of Pressure Sensitive Articles Under Sustained Shear Loading
Effective Date
01-Mar-2006

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ASTM D6463/D6463M-06 - Standard Test Method for Time to Failure of Pressure Sensitive Articles Under Sustained Shear LoadingASTM D6463/D6463M-06 - Standard Test Method for Time to Failure of Pressure Sensitive Articles Under Sustained Shear Loading
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ASTM D6463/D6463M-06 - Standard Test Method for Time to Failure of Pressure Sensitive Articles Under Sustained Shear Loading
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Please contact ASTM International (www.astm.org) for the latest information.
Designation:D6463/D6463M–06
Standard Test Method for
Time to Failure of Pressure Sensitive Articles Under
1
Sustained Shear Loading
This standard is issued under the fixed designation D6463/D6463M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope ASTM Test Methods
E691 Practice for Conducting an Interlaboratory Study to
1.1 This test method covers the ability of a pressure sensi-
Determine the Precision of a Test Method
tive article (for example, tape, label, sticker, etc.) to remain
adhered to a stainless steel panel under a constant load applied
3. Terminology
parallel to the bonding surface of the pressure sensitive article.
3.1 Many of the terms found in this test method are defined
1.2 Values stated in either SI or inch-pound units are to be
in Terminology D907.
regarded separately as standard. The values stated in each
system may not be exact equivalents, therefore, each system
4. Summary of Test Method
must be used independently without combining values in any
4.1 This test method consists of bonding a standard area of
way.
a pressure sensitive article to a stainless steel panel. The
1.3 This standard does not purport to address all of the
bonded construction is allowed to dwell in a constant tempera-
safety concerns, if any, associated with its use. It is the
ture and humidity environment for 30 min. The construction is
responsibility of the user of this standard to establish appro-
then mounted vertically. A standard mass of 500 g [1.1 lb] is
priate safety and health practices and determine the applica-
attached to the pressure sensitive article and allowed to act
bility of regulatory limitations prior to use.
until the construction separates or until 3000 min elapse. If
2. Referenced Documents there is no separation after 3000 min, the test is repeated on a
2 fresh specimen with a mass of 1000 g [2.2 lb] and allowed to
2.1 ASTM Standards:
act until separation occurs or until 3000 min elapse. If no
A666 Specification for Annealed or Cold-Worked Austen-
separation occurs, perform Procedure C of Test Method
itic Stainless Steel Sheet, Strip, Plate, and Flat Bar
D3654/D3654M for shear holding power to stainless steel at
D907 Terminology of Adhesives
49°C [120°F]. The test result is the time in minutes to
D3654/D3654M Test Methods for Shear Adhesion of
separation.
Pressure-Sensitive Tapes
D5750/D5750M Guide for Width and Length of Pressure-
5. Significance and Use
Sensitive Tape
5.1 This test method measures the cohesive strength of the
E171 Specification for Atmospheres for Conditioning and
adhesive on a pressure sensitive article. The time to failure can
Testing Flexible Barrier Materials
predict end use properties of pressure sensitive articles such as
E177 Practice for Use of the Terms Precision and Bias in
edge ooze from cold flow; trimming, slitting and die cutting
quality; telescoping in tapes; ability to seal packages; and
vertical holding power.
1
This test method is under the jurisdiction of ASTM Committee D14 on
5.2 This test method is suitable for quality control, devel-
Adhesives and is the direct responsibility of Subcommittee D14.50 on Hot Melts,
opment and applications testing.
Pressure Sensitives, and Archival Adhesives.
Current edition approved March 1, 2006. Published April 2006. Originally
5.3 Iftheadhesiveisnotalreadycoated,theadhesivecanbe
approved in 1999. Last previous edition approved in 1999 as D6463 – 99. DOI:
coated on smooth, clear polyester (PET) film backing 0.05 mm
10.1520/D6463_D6463M-06.
2 [0.002 in.] thick. The recommended dry adhesive thickness is
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM 0.025 mm [0.001 in.].
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Please contact ASTM International (www.astm.org) for the latest information.
D6463/D6463M–06
FIG. 1 Test Panel with Specimen and Mass (Side View)
5.4 Humidity has a strong effect on time to failure for many fromameanline.Oneorbothofthepanelendsshallbeground
pressure sensitive articles. Therefore, humidity should be to form a 90° angle with the panel surface. Panels showing
controlled in accordance with 8.1.2. stains, discolorations, or numerous scratches are not accept-
able. New
...

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5.1 These test methods provide a quantitative measure of the pressure-sensitive tack property of an adhesive.
FIG. 1 Loop Tack Test Fixture 1  
FIG. 2 Loop Tack Test Fixture 2  
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SCOPE
1.1 These test methods cover the determination of properties of a pressure-sensitive adhesive. These test methods are applicable to those adhesives that form a bond of measurable strength rapidly upon contact with another surface. Tack force may be measured as the force required to separate the adhesive from the adherend at the interface shortly after they have been brought into contact under a load equal only to the weight of the pressure-sensitive article (for example, tape, label, sticker, etc.) on a 1 in.2 contact area.  
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5.1 When a box becomes wet, the performance of the box and its closure are reduced. It is desirable to have box closure methods that retain an ability to keep the box closed when wet. Sealing or reinforcing methods sometimes are useful to improve performance of wet boxes and closures. Water resistance is sometimes a regulatory or contractual requirement.  
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SIGNIFICANCE AND USE
5.1 This test method measures the cohesive strength of the adhesive on a pressure sensitive article. The time to failure can predict end use properties of pressure sensitive articles such as edge ooze from cold flow; trimming, slitting and die cutting quality; telescoping in tapes; ability to seal packages; and vertical holding power.  
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SCOPE
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1.2 Values stated in either SI or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents, therefore, each system must be used independently without combining values in any way.  
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SCOPE
1.1 This specification covers film, paper, and cloth pressure-sensitive tapes used for box closure and sealing.  
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1.1 This specification covers paper-backed pressure-sensitive tapes used for light-duty packaging and masking.  
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Standard Guide for Width and Length of Pressure-Sensitive Tape

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4.1 Conformance to this guide will reduce chances of misunderstanding between suppliers and users of pressure-sensitive tapes.  
4.2 It is recommended that this guide be referenced where widths and lengths of pressure-sensitive tapes are stated, such as in contracts, orders, advertisements, and labeling.
SCOPE
1.1 This guide provides guidelines for widths and lengths of pressure-sensitive tape, including tolerances and labeling in the inch-pound and SI systems. It is not intended for tapes used for medical, surgical, or label stock purposes.  
1.2 Units stated in the inch-pound system followed by a calculated unit in the SI system are to be regarded separately as standard and should not be interchangeable with units stated in the SI system. The units stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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