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ASTM D95-13e1

(Test Method)

Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation

Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation

SIGNIFICANCE AND USE
5.1 A knowledge of the water content of petroleum products is important in the refining, purchase, sale, and transfer of products.  
5.2 The amount of water as determined by this test method (to the nearest 0.05 or 0.1 volume %, depending on the trap size used) may be used to correct the volume involved in the custody transfer of petroleum products and bituminous materials.  
5.3 The allowable amount of water may be specified in contracts.
SCOPE
1.1 This test method covers the determination of water in the range from 0 to 25 % volume in petroleum products, tars, and other bituminous materials by the distillation method. Note 1—Volatile water-soluble material, if present, may be measured as water.  
1.2 The specific products considered during the development of this test method are listed in Table 1. For bituminous emulsions refer to Test Method D244. For crude oils, refer to Test Method D4006 (API MPMS Chapter 10.2).Note 2—With some types of oil, satisfactory results may be obtained from Test Method D1796 (API MPMS Chapter 10.6).  
1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 6.

General Information

Status
Historical
Publication Date
30-Apr-2013
ICS
75.140 - Waxes, bituminous materials and other petroleum products
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.02 - Hydrocarbon Measurement for Custody Transfer (Joint ASTM-API)
Current Stage
Ref Project

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ASTM D95-13e1 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by DistillationASTM D95-13e1 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
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ASTM D95-13e1 - Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation: D95 − 13
Manual of Petroleum Measurement Standards (MPMS), Chapter 10.5
Standard Test Method for
Water in Petroleum Products and Bituminous Materials by
1
Distillation
ThisstandardisissuedunderthefixeddesignationD95;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1
ε NOTE—IP information was removed editorially in September 2013.
1. Scope* D244 Test Methods and Practices for Emulsified Asphalts
D1796 Test Method for Water and Sediment in Fuel Oils by
1.1 This test method covers the determination of water in
the Centrifuge Method (Laboratory Procedure) (API
the range from 0 to 25 % volume in petroleum products, tars,
MPMS Chapter 10.6)
and other bituminous materials by the distillation method.
D4006 Test Method for Water in Crude Oil by Distillation
NOTE 1—Volatile water-soluble material, if present, may be measured
(API MPMS Chapter 10.2)
as water.
D4057 Practice for Manual Sampling of Petroleum and
1.2 The specific products considered during the develop-
Petroleum Products (API MPMS Chapter 8.1)
ment of this test method are listed in Table 1. For bituminous
D4177 Practice for Automatic Sampling of Petroleum and
emulsions refer to Test Method D244. For crude oils, refer to
Petroleum Products (API MPMS Chapter 8.2)
Test Method D4006 (API MPMS Chapter 10.2).
D5854 Practice for Mixing and Handling of Liquid Samples
of Petroleum and Petroleum Products (API MPMS Chap-
NOTE 2—With some types of oil, satisfactory results may be obtained
ter 8.3)
from Test Method D1796 (API MPMS Chapter 10.6).
E123 SpecificationforApparatusforDeterminationofWater
1.3 The values stated in SI units are to be regarded as the
by Distillation
standard. The values in parentheses are for information only.
3
2.2 API Standards:
1.4 This standard does not purport to address all of the
MPMS Chapter 8.1 Manual Sampling of Petroleum and
safety concerns, if any, associated with its use. It is the
Petroleum Products (ASTM Practice D4057)
responsibility of the user of this standard to establish appro-
MPMS Chapter 8.2 Automatic Sampling of Petroleum and
priate safety and health practices and determine the applica-
Petroleum Products (ASTM Practice D4177)
bility of regulatory limitations prior to use. For specific hazard
MPMS Chapter 8.3 Mixing and Handling of Liquid Samples
statements, see Section 6.
of Petroleum and Petroleum Products (ASTM Practice
D5854)
2. Referenced Documents
MPMSChapter10.2 DeterminationofWaterinCrudeOilby
2
2.1 ASTM Standards:
the Distillation Method (ASTM Test Method D4006)
D235 Specification for Mineral Spirits (Petroleum Spirits)
MPMS Chapter 10.6 Test Method forWater and Sediment in
(Hydrocarbon Dry Cleaning Solvent)
Fuel Oils by the Centrifuge Method (Laboratory Proce-
dure) (ASTM Test Method D1796)
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products, Liquid Fuels, and Lubricants and the API Committee on
Petroleum Measurement, and is the direct responsibility of Subcommittee D02.02
/COMQ, the joint ASTM-API Committee on Hydrocarbon Measurement for
Custody Transfer (Joint ASTM-API).
CurrenteditionapprovedMay1,2013.PublishedJuly2013.Originallyapproved
in 1921. Last previous edition approved in 2010 as D95 – 05 (2010). DOI:
10.1520/D0095-13E01.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
3
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Published as Manual of Petroleum Measurement Standards. Available from
Standards volume information, refer to the standard’s Document Summary page on AmericanPetroleumInstitute(API),1220L.St.,NW,Washington,DC20005-4070,
the ASTM website. http://www.api.org.
*A Summary of Changes section appears at the end of this standard
© Jointly copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, USA and the American Petroleum Institute (API), 1220 L Street NW, Washington DC 20005, USA
1

---------------------- Page: 1 ----------------------
´1
D95−13
NOTE 4—It is recommended to use a wide boiling range solvent with
3. Terminology
10% boiling below 100°C to help to ensure an even distillation rate.
3.1 Definitions:
6.1.3 Volatile Spirits Solvent—The following volatile spirits
3.1.1 bituminous material, n—in petroleum technology,a
solvents are acceptable:
black or dark-colored very viscous liquid or semi-solid com-
6.1.3.1 Petroleum Spirit, with a boiling range from 100 to
posed principally of high molecular weight condensed
120°C (212 to 248°F). (Warning—Flammable.
...

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