ASTM D1514-15

Standard Test Method for Carbon Black—Sieve Residue

SIGNIFICANCE AND USE
4.1 The quantity of sieve residue of carbon black is important in some molded or extruded products as it may relate to the surface appearance of those products. The maximum residue in each application is normally determined and agreed to between the user and the producer.
SCOPE
1.1 This test method covers the determination of the water wash sieve residue in regular untreated carbon blacks. It may not be applicable to oil-treated carbon blacks because the oil would prevent proper wetting of the black by water.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 6.

General Information

• Status: Historical
• Publication Date: 14-Jun-2015
• ICS: 83.040.20 - Rubber compounding ingredients
• Technical Committee: D24 - Carbon Black
• Drafting Committee: D24.31 - Non-Carbon Black Components of Carbon Black

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1514 − 15
Standard Test Method for
1
Carbon Black—Sieve Residue
This standard is issued under the fixed designation D1514; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Significance and Use
1.1 This test method covers the determination of the water 4.1 The quantity of sieve residue of carbon black is impor-
wash sieve residue in regular untreated carbon blacks. It may tantinsomemoldedorextrudedproductsasitmayrelatetothe
surfaceappearanceofthoseproducts.Themaximumresiduein
not be applicable to oil-treated carbon blacks because the oil
would prevent proper wetting of the black by water. each application is normally determined and agreed to between
the user and the producer.
1.2 The values stated in SI units are to be regarded as the
standard. The values in parentheses are for information only.
5. Apparatus
3, 4
1.3 This standard does not purport to address all of the
5.1 Sieve and Filtering Apparatus, as shown in Fig. 1.
safety concerns, if any, associated with its use. It is the
5.2 Balance, with a sensitivity of 0.01 g.
responsibility of the user of this standard to establish appro-
5.3 Analytical Balance, with a sensitivity of 0.1 mg.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. For specific
5.4 Oven, gravity-convection type, capable of temperature
precautionary statements, see Section 6.
regulation within 61°C at 125°C and temperature uniformity
within 65°C.
2. Referenced Documents
5.5 Sieves, of either phosphor bronze or stainless steel. The
2
2.1 ASTM Standards:
sieve shall be in accordance with Specification E11. The sieve
D1799 Practice for Carbon Black—Sampling Packaged
to be used shall be agreed upon between the purchaser and the
Shipments
seller.
D1900 Practice for Carbon Black—Sampling Bulk Ship-
5.6 Weighing Dishes.
ments
D4483 Practice for Evaluating Precision for Test Method
6. Precautions
Standards in the Rubber and Carbon Black Manufacturing
6.1 Keep the apparatus clean at all times to prevent con-
Industries
tamination.
E11 Specification for Woven Wire Test Sieve Cloth and Test
6.2 Examinethesieveseachtimetheyareusedtomakesure
Sieves
that no cracks or holes have developed.
3. Summary of Test Method
6.3 Examine the strainer periodically to ascertain that the
filter screen is in good condition.
3.1 Asample of carbon black is washed with water through
a wire-mesh screen of a specified size until all that remains is
7. Sampling
a non-carbon black residue.This residue is dried, weighed, and
7.1 Samples shall be taken in accordance with Practice
the amount of residue is expressed as mg/kg (ppm) of the
D1799 or Practice D1900.
original sample.
3
Sieve and filtering apparatus, available from Titan Specialties, Inc., P.O. Box
2316, Pampa, TX 70066-2316, has been found suitable. The A2000 Test Set from
1
This test method is under the jurisdiction ofASTM Committee D24 on Carbon Krahnen IQS, GmbH, Paffrather Str. 13–15, D-51069 Koeln, Germany, has been
Black and is the direct responsibility of Subcommittee D24.31 on Non-Carbon found suitable.AnASTM specified apparatus modified with an enlarged funnel leg
Black Components of Carbon Black. ID (5.080 cm or 2.0 in.) and sieve screen OD (6.032 cm or 2.375 in.) has also been
Current edition approved June 15, 2015. Published August 2015. Originally found suitable.
4
approved in 1957. Last previous edition approved in 2011 as D1514 – 04 (2011). The sole source of supply of housing No. 20 and cartridge No. 30 known to the
DOI: 10.1520/D1514-15. committee at this time is Amtek, Plymouth Products Division, 562 Indiana Ave.,
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Sheboygan, WI 53081. If you are aware of alternative suppliers, please provide this
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM information to ASTM International Headquarters. Your comments will receive
1
Standards volume information, refer to the standard’s Document Summary page on careful consideration at a meeting of the responsible technical committee, which
the ASTM website. you may attend.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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D1514 − 15
NOTE1—Ifdesireditispermissibletoutilizewettingagentstofacilitate
dispersion. Care must be taken to ensure that all of the solid material is
transferred from the vessel used for dispersing the black into the funnel of
the washing apparatus.
9.7 Use a gentle stream of water from
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1514 − 04 (Reapproved 2011) D1514 − 15
Standard Test Method for
1
Carbon Black—Sieve Residue
This standard is issued under the fixed designation D1514; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the determination of the water wash sieve residue in regular untreated carbon blacks. It may not
be applicable to oil-treated carbon blacks because the oil would prevent proper wetting of the black by water.
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. For specific precautionary statements, see Section 6.
2. Referenced Documents
2
2.1 ASTM Standards:
D1799 Practice for Carbon Black—Sampling Packaged Shipments
D1900 Practice for Carbon Black—Sampling Bulk Shipments
D4483 Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
3. Summary of Test Method
3.1 A sample of carbon black is washed with water through a wire-mesh screen of a specified size until all that remains is a
non-carbon black residue. This residue is dried, weighed, and the amount of residue is expressed as mg/kg (ppm) of the original
sample.
4. Significance and Use
4.1 The quantity of sieve residue of carbon black is important in some molded or extruded products as it may relate to the
surface appearance of those products. The maximum residue in each application is normally determined and agreed to between
the user and the producer.
5. Apparatus
3, 4
5.1 Sieve and Filtering Apparatus, as shown in Fig. 1.
5.2 Balance, with a sensitivity of 0.01 g.
5.3 Analytical Balance, with a sensitivity of 0.1 mg.
5.4 Oven, gravity-convection type, capable of temperature regulation within 61°C at 125°C and temperature uniformity within
65°C.
1
This test method is under the jurisdiction of ASTM Committee D24 on Carbon Black and is the direct responsibility of Subcommittee D24.31 on Non-Carbon Black
Components of Carbon Black.
Current edition approved May 1, 2011June 15, 2015. Published July 2011August 2015. Originally approved in 1957. Last previous edition approved in 20042011 as
D1514 – 04.D1514 – 04 (2011). DOI: 10.1520/D1514-04R11.10.1520/D1514-15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Sieve and filtering apparatus, available from Titan Specialties, Inc., P.O. Box 2316, Pampa, TX 70066-2316, has been found suitable. The A2000 Test Set from Krahnen
IQS, GmbH, Paffrather Str. 13–15, D-51069 Koeln, Germany, has been found suitable. An ASTM specified apparatus modified with an enlarged funnel leg ID (5.080 cm or
2.0 in.) and sieve screen OD (6.032 cm or 2.375 in.) has also been found suitable.
4
The sole source of supply of housing No. 20 and cartridge No. 30 known to the committee at this time is Amtek, Plymouth Products Division, 562 Indiana Ave.,
Sheboygan, WI 53081. If you are aware of alternative suppliers, please provide this information to ASTM International Headquarters. Your comments will receive careful
1
consideration at a meeting of the responsible technical committee, which you may attend.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1514 − 15
4
NOTE 1—Industrial/O.E.M. filter and pleated polyester fabric reusable cartridges have been found to be a satisfactory strainer.
NOTE 2—Corrosion-free piping must be used.
NOTE 3—Detailed drawings can be obtained from Test Method D1514 – 88a.
NOTE 4—Spray nozzle: Part No. 460.746.30 BE available from Lechler Inc., 445 Kautz Rd., St. Charles, IL 60174, or Titan Specialties Inc., P.O. Box
2316, Pampa, TX 70066-2316.
FIG. 1 Schematic Diagram of Apparatus for Sieve Residue
...