ASTM D3042-09
(Test Method)Standard Test Method for Insoluble Residue in Carbonate Aggregates
Standard Test Method for Insoluble Residue in Carbonate Aggregates
SIGNIFICANCE AND USE
The amount and size distribution of noncarbonate (insoluble) material in carbonate aggregates is of interest to those conducting research on the polish susceptibility of stone used in pavements or on the friction properties of pavement surfaces. In addition, some agencies utilize the test for acceptance purposes to delineate carbonate aggregates that polish excessively and become slippery and those that will not.
Note 1—The quality of the results produced by this standard are dependent upon the competence of the personnel performing the procedure and the capability, calibration, and the maintenance of the equipment used. Agencies that meet the criteria of Practice D 3666 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D 3666 alone does not completely assure reliable results. Reliable results depend on many factors: following the suggestions of Practice D 3666 or similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers determination of the percentage of insoluble residue in carbonate aggregates using hydrochloric acid solution to react the carbonates.
1.2 The values stated in SI units are to be regarded as standard. Regarding sieves, per Specification E 11, “The values stated in SI units shall be considered standard for the dimensions of the wire cloth openings and the diameter of the wires used in the wire cloth. The values stated in inch-pound units shall be considered standard with regard to the sieve frames.” When sieve mesh sizes are referenced, the alternate inch-pound designations are provided for information purposes and enclosed in parentheses.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precaution statements are given in Section 7.
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Designation: D3042 − 09
StandardTest Method for
1
Insoluble Residue in Carbonate Aggregates
This standard is issued under the fixed designation D3042; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope E11 Specification for Woven Wire Test Sieve Cloth and Test
Sieves
1.1 This test method covers determination of the percentage
ofinsolubleresidueincarbonateaggregatesusinghydrochloric
3. Significance and Use
acid solution to react the carbonates.
3.1 The amount and size distribution of noncarbonate (in-
1.2 The values stated in SI units are to be regarded as
soluble) material in carbonate aggregates is of interest to those
standard. Regarding sieves, per Specification E11, “The values
conducting research on the polish susceptibility of stone used
stated in SI units shall be considered standard for the dimen-
in pavements or on the friction properties of pavement sur-
sions of the wire cloth openings and the diameter of the wires
faces. In addition, some agencies utilize the test for acceptance
used in the wire cloth. The values stated in inch-pound units
purposes to delineate carbonate aggregates that polish exces-
shall be considered standard with regard to the sieve frames.”
sively and become slippery and those that will not.
Whensievemeshsizesarereferenced,thealternateinch-pound
NOTE 1—The quality of the results produced by this standard are
designations are provided for information purposes and en-
dependent upon the competence of the personnel performing the proce-
closed in parentheses.
dure and the capability, calibration, and the maintenance of the equipment
used. Agencies that meet the criteria of Practice D3666 are generally
1.3 This standard does not purport to address all of the
considered capable of competent and objective testing/sampling/
safety concerns, if any, associated with its use. It is the
inspection/etc. Users of this standard are cautioned that compliance with
responsibility of the user of this standard to establish appro-
Practice D3666 alone does not completely assure reliable results. Reliable
priate safety and health practices and determine the applica-
results depend on many factors: following the suggestions of Practice
bility of regulatory limitations prior to use. Specific precaution D3666 or similar acceptable guideline provides a means of evaluating and
controlling some of those factors.
statements are given in Section 7.
4. Apparatus
2. Referenced Documents
4.1 Sieves, U.S. standard 8-in. diameter, conforming to
2
2.1 ASTM Standards:
Specification E11 in the following sizes:
C136 Test Method for Sieve Analysis of Fine and Coarse
3
9.5-mm ( ⁄8-in.)
Aggregates
4.75-mm (No. 4)
C294 Descriptive Nomenclature for Constituents of Con-
2.36-mm (No. 8)
1.18-mm (No. 16)
crete Aggregates
600-µm (No. 30)
C670 Practice for Preparing Precision and Bias Statements
300-µm (No. 50)
for Test Methods for Construction Materials
150-µm (No. 100)
75-µm (No. 200)
D3666 Specification for Minimum Requirements for Agen-
cies Testing and Inspecting Road and Paving Materials 4.2 Balance—A balance having a minimum capacity of 15
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
kgandmeetingtherequirementsofSpecificationD4753,Class
ances and Standard Masses for Use in Soil, Rock, and GP5.
Construction Materials Testing
4.3 Oven, of appropriate size capable of being maintained at
110 6 5°C.
4.4 Agitation Equipment, such as a jar mill or a magnetic
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
stirrer.
and Paving Materials and is the direct responsibility of Subcommittee D04.51 on
Aggregate Tests.
4.5 Bunsen Burner or Hot Plate.
Current edition approved June 1, 2009. Published June 2009. Originally
approved in 1972. Last previous edition approved in 2003 as D3042 – 03. DOI:
4.6 Receiving Tank, of nonreactive material to receive wash
10.1520/D3042-09.
water and residue washed through the 8-in. diameter sieves.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.7 Rapid Filter Paper, acid-resistant.
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. 4.8 Safety Eyeglasses, Rubber Gloves, Aprons, and so forth.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
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D3042 − 09
4.9 Borosilicate Glass Containers, for performing acid 7.4 Place an aggregate sample weighing a minimum of 500
leaching test. g in
...
This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D3042–03 Designation:D3042–09
Standard Test Method for
1
Insoluble Residue in Carbonate Aggregates
This standard is issued under the fixed designation D 3042; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 Thistestmethodcoversdeterminationofthepercentageofinsolubleresidueincarbonateaggregatesusinghydrochloricacid
solution to react the carbonates.
1.2The values stated in SI units are to be regarded as standard.
1.2 The values stated in SI units are to be regarded as standard. Regarding sieves, per Specification E 11, “The values stated
in SI units shall be considered standard for the dimensions of the wire cloth openings and the diameter of the wires used in the
wire cloth. The values stated in inch-pound units shall be considered standard with regard to the sieve frames.” When sieve mesh
sizes are referenced, the alternate inch-pound designations are provided for information purposes and enclosed in parentheses.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. Specific precaution statements are given in Section 7.
2. Referenced Documents
2
2.1 ASTM Standards:
C 136 Test Method for Sieve Analysis of Fine and Coarse Aggregates
C 294 Descriptive Nomenclature for Constituents of Natural Mineral Concrete Aggregates
2
C 670 Practice for Preparing Precision and Bias Statements for Test Methods of Construction Materials Practice for Preparing
Precision and Bias Statements for Test Methods for Construction Materials
D 3666 Specification for Minimum Requirements for Agencies Testing and Inspecting Road and Paving Materials
D 4753 SpecificationGuide for Evaluating, Selecting, and Specifying Balances and Scales Standard Masses for Use in Soil,
Rock, and Construction Materials Testing
E11 Specification for Wire-Wire Cloth and Sieves for Testing Purposes
3. Significance and Use
3.1 The amount and size distribution of noncarbonate (insoluble) material in carbonate aggregates is of interest to those
conducting research on the polish susceptibility of stone used in pavements or on the friction properties of pavement surfaces. In
addition, some agencies utilize the test for acceptance purposes to delineate carbonate aggregates that polish excessively and
become slippery and those that will not.
NOTE 1—The quality of the results produced by this standard are dependent upon the competence of the personnel performing the procedure and the
capability, calibration, and the maintenance of the equipment used. Agencies that meet the criteria of Practice D 3666 are generally considered capable
of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D 3666 alone does not
completely assure reliable results. Reliable results depend on many factors: following the suggestions of Practice D 3666 or similar acceptable guideline
provides a means of evaluating and controlling some of those factors.
4. Apparatus
4.1 Sieves, U.S. standard 203.2-mm (8-in.) 8-in. diameter, conforming to Specification E 11in the following sizes:
3
9.5-mm ( ⁄8-in.)
4.75-mm (No. 4)
2.36-mm (No. 8)
1.18-mm (No. 16)
1
This test method is under the jurisdiction ofASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.51 onAggregate
Tests.
Current edition approved July 10, 2003. Published September 2003. Originally approved in 1972. Last previous edition approved in 1997 as D3042–97.
Current edition approved June 1, 2009. Published June 2009. Originally approved in 1972. Last previous edition approved in 2003 as D 3042 – 03.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. ForAnnualBookofASTMStandards
, Vol 04.02.volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
D3042–09
600-µm (No. 30)
300-µm (No. 50)
150-µm (No. 100)
75-µm (No. 200)
4.2 Bal
...
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