ASTM D5755-02
(Test Method)Standard Test Method for Microvacuum Sampling and Indirect Analysis of Dust by Transmission Electron Microscopy for Asbestos Structure Number Concentrations
Standard Test Method for Microvacuum Sampling and Indirect Analysis of Dust by Transmission Electron Microscopy for Asbestos Structure Number Concentrations
SCOPE
1.1 This test method covers a procedure to ( a) identify asbestos in dust and (b) provide an estimate of the surface loading of asbestos in the sampled dust reported as the number of asbestos structures per unit area of sampled surface.
1.1.1 If an estimate of the asbestos mass is to be determined, the user is referred to Test Method D 5756.
1.2 This test method describes the equipment and procedures necessary for sampling, by a microvacuum technique, non-airborne dust for levels of asbestos structures. The non-airborne sample is collected inside a standard filter membrane cassette from the sampling of a surface area for dust which may contain asbestos.
1.2.1 This procedure uses a microvacuuming sampling technique. The collection efficiency of this technique is unknown and will vary among substrates. Properties influencing collection efficiency include surface texture, adhesiveness, electrostatic properties and other factors.
1.3 Asbestos identified by transmission electron microscopy (TEM) is based on morphology, selected area electron diffraction (SAED), and energy dispersive X-ray analysis (EDXA). Some information about structure size is also determined.
1.4 This test method is generally applicable for an estimate of the surface loading of asbestos structures starting from approximately 1000 asbestos structures per square centimetre.
1.4.1 The procedure outlined in this test method employs an indirect sample preparation technique. It is intended to disperse aggregated asbestos into fundamental fibrils, fiber bundles, clusters, or matrices that can be more accurately quantified by transmission electron microscopy. However, as with all indirect sample preparation techniques, the asbestos observed for quantification may not represent the physical form of the asbestos as sampled. More specifically, the procedure described neither creates nor destroys asbestos, but it may alter the physical form of the mineral fibers.
1.5 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
General Information
Relations
Standards Content (Sample)
NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 5755 – 02
Standard Test Method for
Microvacuum Sampling and Indirect Analysis of Dust by
Transmission Electron Microscopy for Asbestos Structure
1
Number Surface Loading
This standard is issued under the fixed designation D 5755; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 1.5 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
1.1 This test method covers a procedure to (a) identify
only.
asbestos in dust and (b) provide an estimate of the surface
1.6 This standard does not purport to address all of the
loading of asbestos in the sampled dust reported as the number
safety concerns, if any, associated with its use. It is the
of asbestos structures per unit area of sampled surface.
responsibility of the user of this standard to establish appro-
1.1.1 If an estimate of the asbestos mass is to be determined,
priate safety and health practices and determine the applica-
the user is referred to Test Method D 5756.
bility of regulatory limitations prior to use.
1.2 This test method describes the equipment and proce-
dures necessary for sampling, by a microvacuum technique,
2. Referenced Documents
non-airborne dust for levels of asbestos structures. The non-
2.1 ASTM Standards:
airborne sample is collected inside a standard filter membrane
2
D 1193 Specification for Reagent Water
cassette from the sampling of a surface area for dust which may
3
D 3195 Practice for Rotameter Calibration
contain asbestos.
D 3670 Guide for Determination of Precision and Bias of
1.2.1 This procedure uses a microvacuuming sampling tech-
3
Methods of Committee D-22
nique. The collection efficiency of this technique is unknown
D 5756 Test Method for Microvacuum Sampling and Indi-
and will vary among substrates. Properties influencing collec-
rect Analysis of Dust by Transmission Electron Micros-
tion efficiency include surface texture, adhesiveness, electro-
3
copy for Asbestos Mass Surface Loading
static properties and other factors.
D 6620 Practice for Determining a Detection Limit for
1.3 Asbestos identified by transmission electron microscopy
3
Asbestos Measurements Based on Counts
(TEM) is based on morphology, selected area electron diffrac-
tion (SAED), and energy dispersive X-ray analysis (EDXA).
3. Terminology
Some information about structure size is also determined.
3.1 Definitions:
1.4 This test method is generally applicable for an estimate
3.1.1 asbestiform—a special type of fibrous habit in which
of the surface loading of asbestos structures starting from
the fibers are separable into thinner fibers and ultimately into
approximately 1000 asbestos structures per square centimetre.
fibrils. This habit accounts for greater flexibility and higher
1.4.1 The procedure outlined in this test method employs an
tensile strength than other habits of the same mineral. For more
indirect sample preparation technique. It is intended to disperse
4
information on asbestiform mineralogy, see Refs (1), (2) and
aggregated asbestos into fundamental fibrils, fiber bundles,
(3).
clusters, or matrices that can be more accurately quantified by
3.1.2 asbestos—a collective term that describes a group of
transmission electron microscopy. However, as with all indi-
naturally occurring, inorganic, highly fibrous, silicate domi-
rect sample preparation techniques, the asbestos observed for
nated minerals, which are easily separated into long, thin,
quantification may not represent the physical form of the
flexible fibers when crushed or processed.
asbestos as sampled. More specifically, the procedure de-
scribed neither creates nor destroys asbestos, but it may alter
the physical form of the mineral fibers.
1
This test method is under the jurisdiction of ASTM Committee D22 on
2
Sampling and Analysis of Atmospheres and is the direct responsibility of Subcom- Annual Book of ASTM Standards, Vol 11.01.
3
mittee D22.07 on Sampling and Analysis of Asbestos. Annual Book of ASTM Standards, Vol 11.03.
4
Current edition approved November 10, 2002. Published January 2002. Origi- The boldface numbers in parentheses refer to the list of references at the end of
nally approved in 1995. Last previous edition approved in 1995 as D 5755 - 95. this test method.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.