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ASTM C341-96

(Test Method)

Standard Test Method for Length Change of Drilled or Sawed Specimens of Hydraulic-Cement Mortar and Concrete

Standard Test Method for Length Change of Drilled or Sawed Specimens of Hydraulic-Cement Mortar and Concrete

SCOPE
1.1 This test method covers the determination of the length changes of drilled or sawed specimens of hydraulic-cement mortar and concrete due to causes other than externally applied forces and temperature changes. It can be readily adapted, if desired, to studies of length change involving different schedules or environmental treatment than the standard procedures prescribed by this test method.  
1.2 The values stated in inch-pound units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Nov-1996
ICS
91.100.10 - Cement. Gypsum. Lime. Mortar
Technical Committee
C09 - Concrete and Concrete Aggregates
Drafting Committee
C09.68 - Volume Change
Current Stage
Ref Project

Relations

Replaced By
ASTM C341/C341M-03 - Standard Practice for Length Change of Cast, Drilled, or Sawed Specimens of Hydraulic-Cement Mortar and Concrete
Effective Date
10-Jul-2003

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ASTM C341-96 - Standard Test Method for Length Change of Drilled or Sawed Specimens of Hydraulic-Cement Mortar and ConcreteASTM C341-96 - Standard Test Method for Length Change of Drilled or Sawed Specimens of Hydraulic-Cement Mortar and Concrete
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ASTM C341-96 - Standard Test Method for Length Change of Drilled or Sawed Specimens of Hydraulic-Cement Mortar and Concrete
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: C 341 – 96
Standard Test Method for
Length Change of Drilled or Sawed Specimens of Hydraulic-
1
Cement Mortar and Concrete
This standard is issued under the fixed designation C 341; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Significance and Use
1.1 This test method covers the determination of the length 4.1 Measurements of length change permit assessment of
changes of drilled or sawed specimens of hydraulic-cement the potential for volumetric expansion or contraction of drilled
mortar and concrete due to causes other than externally applied or sawed specimens of hydraulic-cement mortar, and concrete
forces and temperature changes. It can be readily adapted, if due to various causes other than externally applied forces and
desired, to studies of length change involving different sched- temperature changes. This test method is particularly useful for
ules or environmental treatment than the standard procedures comparative evaluation of this potential in different mortar or
prescribed by this test method. concrete specimens.
1.2 The values stated in inch-pound units are to be regarded
5. Apparatus
as the standard.
1.3 This standard does not purport to address all of the 5.1 Length Comparator—The length comparator shall gen-
erally conform to the requirements of Specification C 490,
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro- except that it should be constructed to accommodate the
specimens to be tested under this test method, which may have
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. gage lengths of 3 in. (75 mm) or more.
5.1.1 Gage Studs in Ends of Specimens—When the com-
2. Referenced Documents
parator is to be used to measure between gage studs in the ends
2.1 ASTM Standards: of specimens, the gage length for computing percentage length
2
A 276 Specification for Stainless Steel Bars and Shapes change shall be considered to be the distance between the
C 42 Test Method for Obtaining and Testing Drilled Cores innermost ends of the gage studs, and the contact terminals of
3
and Sawed Beams of Concrete the comparator shall be plane, polished, heat-treated surfaces
C 157 Test Method for Length Change of Hardened as described in Specification C 490. Fig. 3 of Specification
3
Hydraulic-Cement Mortar and Concrete C 490 shows one type of comparator which has been found
C 490 Practice for Use of Apparatus for the Determination suitable for such specimens. A horizontal comparator may be
of Length Change of Hardened Cement Paste, Mortar, and desirable for specimens that are considered too large to be
4
Concrete handled by the type of comparator illustrated in Fig. 3 of
Specification C 490.
3. Terminology
5.1.2 Gage Studs on Sides of Specimen—When the com-
3.1 Definition of Term—The term “length change,” as used parator is to be used to measure between gage studs on the
here, is defined as an increase or decrease in a linear dimension
sides of specimens, the contact terminals shall be conical,
of a test specimen which has been caused to change by any heat-treated surfaces as shown in Fig. 1, which illustrates a
factor other than externally applied forces and temperature
type of comparator that has been found satisfactory for this
changes. type of specimen. In this case, the gage length shall be the
distance between the reference points located in the exposed
ends of the gage studs (see 5.2).
1
This test method is under the jurisdiction of ASTM Committee C-9 on Concrete
5.2 Gage Studs—Gage studs shall be Type 316 stainless
and Concrete Aggregates and is the direct responsibility of Subcommittee C09.68 on
steel, meeting Specification A 276.
Volume Change.
Current edition approved Nov. 10, 1996. Published January 1997. Originally 5.2.1 For Ends of Specimens—Gage studs that are to be
published as C 341 – 54 T. Last previous edition C 341 – 89.
located in the ends of specimens shall have a rounded surface
2
Annual Book of ASTM Standards, Vol 01.05.
to provide point contact with the terminals of the comparator.
3
Annual Book of ASTM Standards, Vol 04.02.
4
The types of studs described in Specification C 490 are suitable
Annual Book of ASTM Standards, Vol 04.01.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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4.1 The results of mortar mixture tests can be suitable for comparing the relative performance of combinations of concrete-making materials such as fine aggregate, chemical admixtures, supplementary cementitious materials (SCMs), water, and hydraulic cement. Furthermore, this guide can be useful to identify unexpected performances due to combination of various materials. The relative trends in performance observed with the mortar method may suggest relative performance in concrete mixtures batched with the same materials and relative mixture proportions.  
4.2 While there are a number of ways to proportion and mix mortar mixtures, four procedures described in this guide have been used extensively for evaluating the performance of admixtures. Method A enables evaluation of materials using mixture proportions that correspond to specific job conditions. Method B can be used as a general mixture using fixed amounts of a standard sand, cement, and supplementary cementitious materials. Method C is a modified version of Test Method C359 to evaluate the impact of chemical admixtures on the early stiffening of a mortar prepared with specified amounts of job cement, a standard sand, and an amount of water that will produce a mortar with a specified initial penetration measured in accordance with Test Method C359. The measurements of penetration over time can be related to the early stiffening processes associated with false and flash set. Method D is a modified version of Test Method C185 whereby the mortar mixture can be prepared with various combinations of chemical admixtures, supplementary cementitious materials, and job water. Methods A and B would be most applicable for investigating material incompatibility issues associated with ready mixed concrete, while Method C would be applicable for concrete mixed for a short period of time in stationary mixers and transported to the forms in non-agitating equipment. Method D is suitable for all concrete mixing processes and is...
SCOPE
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1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with this guide. Some values only have SI units because the inch-pound equivalents are not used in guide.  
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Standard Test Method for Measuring Changes in Height of Cylindrical Specimens of Hydraulic-Cement Grout

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4.1 This test method is intended to provide a means of assessing the ability of a hydraulic-cement grout to retain a stable volume during the stipulated testing period of 28 days, provided that the tendency to change height does not include the effects of drying caused by evaporation, uptake of moisture, carbonation, or exposure to temperatures outside the range 23.0 °C ± 2.0 °C [73 °F ± 3.5 °F] (Note 2). An exception is made when the options described in the section on test conditions are exercised.  
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SCOPE
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1.1 This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and high strength mortar. The classifications of concrete and mortar covered are defined in Section 3.
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SCOPE
1.1 This test method covers the determination of the effect on mortar strength of the organic impurities in fine aggregate, whose presence is indicated using Test Method C40/C40M. Comparison is made between compressive strengths of mortar made with washed and unwashed fine aggregate.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in the practice.
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Standard Practice for Measuring Hydration Kinetics of Hydraulic Cementitious Mixtures Using Isothermal Calorimetry

SIGNIFICANCE AND USE
5.1 Thermal power curves are used to evaluate the isothermal hydration kinetics of the combined mixture of different materials during the early period after being mixed with water. These isothermal power curves, or hydration profiles, may provide indications relative to setting characteristics, compatibility of different materials, sulfate balance and early strength development. The isothermal hydration profiles can also be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as curing temperature. Special care must be used in evaluating extended retardation with paste specimens, which have been shown to overestimate the retardation of some mixtures containing cement, SCM, and admixtures.  
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5.3 Although this technique has been used historically to understand issues related to setting and slump loss, it must be emphasized that isothermal calorimetry results cannot predict concrete performance definitely, either positively or negatively. Extensive verification in concrete at planned dosages and temperatures, and at higher dosages, is needed. Isothermal calorimetry is an effective tool to identify sensitivities, so that concrete testing can be efficiently planned and performed.  
5.4 This practice provides a means of assessing the relative hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.5 The procedure and apparatus can be used to monitor the thermal power from pastes and mortars alone or in combination with chemical admixtures.  
5.6 The isothermal calorimeter described here can be used to measure the thermal power and heat of hydration of mortars prepared independently or obtained by wet sieving from concrete in accordance with Practice C172/C1...
SCOPE
1.1 This practice describes the apparatus and procedure for measuring relative differences in hydration kinetics of hydraulic cementitious mixtures, either in paste or mortar (see Note 1), including those containing admixtures, various supplementary cementitious materials (SCM), and other fine materials by measuring the thermal power using an isothermal calorimeter.
Note 1: Paste specimens are often preferred for mechanistic research when details of individual reaction peaks are important or for particular calorimetry configurations. Mortar specimens may give results that have better correlation with concrete setting and early strength development and are often preferred to evaluate different mixture proportions for concrete. Both paste and mortar studies have been found to be effective in evaluating concrete field problems due to incompatibility of materials used in concrete mixtures.  
1.2 This practice does not cover the measurement of heat of hydration. Heat of hydration can be determined according to Test Method C1702.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)  
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4.1 Supplementary cementitious materials (SCM) covered under existing ASTM specifications are fly ash, slag cement, raw and calcined natural pozzolans including calcined clays, silica fume, and ground-glass pozzolan. The use of these materials, and limits established in existing specifications, are based on data obtained from research programs, field testing, and long term performance monitoring. Performance of SCM in specific concrete mixtures is commonly verified through preconstruction testing. This guide provides an approach to assessing the properties of materials that are not covered under existing specifications, and for assessing the performance of those materials in concrete.  
4.2 If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.  
4.3 In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
SCOPE
1.1 This guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989/C989M, C1240, and C1866/C1866M. This guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989/C989M, C1240, and C1866/C1866M. These materials should not be represented as such and each specific source is to be evaluated separately.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Practice for Evaluating Early Hydration of Hydraulic Cementitious Mixtures Using Thermal Measurements

SIGNIFICANCE AND USE
5.1 This practice provides a means of assessing the relative early hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.2 Thermal profiles are used to evaluate the hydration behavior of hydraulic cementitious mixtures after the addition of water. They may provide indications concerning setting characteristics, compatibility of different materials, sulfate balance, relative heat of hydration, and early strength development. They can be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as the initial mixture and test temperatures. Thermal profile testing is an effective tool for identifying performance sensitivities or trends, and may help to reduce the number of concrete test mixtures required to develop and qualify mixtures, especially those to be subject to variable ambient environments. It may be used by concrete producers, materials suppliers, and other practitioners to support mixture development, selection of material types or sources, optimization of proportions, or troubleshooting of field problems.  
5.3 This practice can be used to understand concrete problems related to slump loss, setting, and early strength, but results may not predict field concrete performance. Performance verification with concrete is needed to quantify the trends identified using thermal testing.  
5.4 This practice can be used to evaluate the effects of chemical admixtures on the thermal profiles of cementitious mixtures. This can be especially useful in selecting dosages appropriate for different ambient conditions.  
5.5 Thermal measurement testing as described in this practice may have similar significance and use as isothermal calorimetry described by Practice C1679 or some types of near-adiabatic calorimetry. The selection of which practice or methods to use may depend on specific applications and circumstances. The thermal profiles obtained by this practic...
SCOPE
1.1 This practice describes the apparatus and procedure for evaluating relative differences in early hydration of hydraulic cementitious mixtures such as paste, mortar, or concrete, including those containing chemical admixtures, various supplementary cementitious materials (SCMs), and other finely divided materials, by measuring the temperature history of a specimen.  
1.2 Calorimetry is the measurement of heat lost or gained during a chemical reaction such as cement hydration; calorimetric measurements as a function of time can be used to describe and evaluate hydration and related early-age property development. Calorimetry may be performed under isothermal conditions (as described in Practice C1679) or under adiabatic or semi-adiabatic conditions. This practice cannot be described as calorimetry because no attempt is made to measure or compute the heat evolved from test specimens due to hydration, but it can in many cases be used for similar evaluations. Variables that should be considered in the application of this practice are discussed in the Appendix.  
1.3 Units—The values stated in either SI units or inch-pound units shall be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in practice.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Warning: Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2  
1.5 This...

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ASTM
ASTM C1697-21(Specification)
Standard Specification for Blended Supplementary Cementitious Materials

SCOPE
1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989/C989M, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice2 for information and guidelines. Specific reference is made to:    
ACI 232.1R  
Use of Natural Pozzolans in Concrete  
ACI 232.2R  
Use of Fly Ash in Concrete  
ACI 233R  
Slag Cement in Concrete and Mortar  
ACI 234R  
Guide for the Use of Silica Fume in Concrete  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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