ASTM D7175-15
(Test Method)Standard Test Method for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer
Standard Test Method for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer
SIGNIFICANCE AND USE
5.1 The test temperature for this test is related to the temperature experienced by the pavement in the geographical area for which the asphalt binder is intended to be used.
5.2 The complex shear modulus is an indicator of the stiffness or resistance of asphalt binder to deformation under load. The complex shear modulus and the phase angle define the resistance to shear deformation of the asphalt binder in the linear viscoelastic region. The complex modulus and the phase angle are used to calculate performance-related criteria in accordance with Specification D6373 or AASHTO Standard M320.
SCOPE
1.1 This test method covers the determination of the dynamic shear modulus and phase angle of asphalt binders when tested in dynamic (oscillatory) shear using parallel plate geometry. It is applicable to asphalt binders having dynamic shear modulus values in the range from 100 Pa to 10 MPa. This range in modulus is typically obtained between 4 and 88°C at 10 rad/s. This test method is intended for determining the linear viscoelastic properties of asphalt binders as required for specification testing and is not intended as a comprehensive procedure for the full characterization of the viscoelastic properties of asphalt binders.
1.2 This standard is appropriate for unaged materials, material aged in accordance with Test Method D2872, material aged in accordance with Practice D6521, or material aged in accordance with both Test Method D2872 and Practice D6521. This procedure is limited to asphalt binders that contain particles with largest dimension less than 250 μm.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D7175 − 15
Standard Test Method for
Determining the Rheological Properties of Asphalt Binder
1
Using a Dynamic Shear Rheometer
This standard is issued under the fixed designation D7175; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This test method covers the determination of the dy-
C670 Practice for Preparing Precision and Bias Statements
namic shear modulus and phase angle of asphalt binders when
for Test Methods for Construction Materials
tested in dynamic (oscillatory) shear using parallel plate
D140 Practice for Sampling Bituminous Materials
geometry. It is applicable to asphalt binders having dynamic
D2170 Test Method for Kinematic Viscosity of Asphalts
shearmodulusvaluesintherangefrom100Pato10MPa.This
(Bitumens)
range in modulus is typically obtained between 4 and 88°C at
D2171 Test Method for Viscosity of Asphalts by Vacuum
10rad/s.Thistestmethodisintendedfordeterminingthelinear
Capillary Viscometer
viscoelastic properties of asphalt binders as required for
D2872 Test Method for Effect of Heat andAir on a Moving
specification testing and is not intended as a comprehensive
Film of Asphalt (Rolling Thin-Film Oven Test)
procedure for the full characterization of the viscoelastic
D6373 Specification for Performance Graded Asphalt
properties of asphalt binders.
Binder
1.2 This standard is appropriate for unaged materials, ma-
D6521 Practice for Accelerated Aging of Asphalt Binder
terial aged in accordance with Test Method D2872, material
Using a Pressurized Aging Vessel (PAV)
aged in accordance with Practice D6521, or material aged in
E77 Test Method for Inspection and Verification of Ther-
accordance with bothTest Method D2872 and Practice D6521.
mometers
This procedure is limited to asphalt binders that contain E563 Practice for Preparation and Use of an Ice-Point Bath
particles with largest dimension less than 250 µm.
as a Reference Temperature
E644 Test Methods for Testing Industrial Resistance Ther-
1.3 The values stated in SI units are to be regarded as
mometers
standard. No other units of measurement are included in this
E882 Guide for Accountability and Quality Control in the
standard.
Chemical Analysis Laboratory
3
1.4 This standard may involve hazardous materials, 2.2 AASHTO Standards:
operations, and equipment. This standard does not purport to M320 Standard Specification for Performance-Graded As-
address all of the safety concerns, if any, associated with its phalt Binder
use. It is the responsibility of the user of this standard to R29 Practice for Grading or Verifying the Performance
establish appropriate safety and health practices and deter- Grade of an Asphalt Binder
mine the applicability of regulatory limitations prior to use. T315 Standard Test Method for Determining the Rheologi-
cal Properties of Asphalt Binder Using a Dynamic Shear
1.5 This international standard was developed in accor-
Rheometer
dance with internationally recognized principles on standard-
4
2.3 Deutsche Industrie Norm (DIN) Standard:
ization established in the Decision on Principles for the
43760 Standard for Calibration of Thermocouples
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
1 3
This test method is under the jurisdiction of ASTM Committee D04 on Road Available from American Association of State Highway and Transportation
and Paving Materials and is the direct responsibility of Subcommittee D04.44 on Officials (AASHTO), 444 N. Capitol St., NW, Suite 249, Washington, DC 20001,
Rheological Tests. http://www.transportation.org.
4
Current edition approved July 1, 2015. Published August 2015. Originally Available from Beuth Verlag GmbH (DIN-- DIN Deutsches Institut fur
approved in 2005. Last previous edition approved in 2008 as D7175 – 08. DOI: Normunge.V.),Burggrafenstrasse6,10787,Berlin,Germany,http://www.en.din.de.
10.1520/D7175-15.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7175 − 15
3. Terminolo
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D7175 − 08 D7175 − 15
Standard Test Method for
Determining the Rheological Properties of Asphalt Binder
1
Using a Dynamic Shear Rheometer
This standard is issued under the fixed designation D7175; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the determination of the dynamic shear modulus and phase angle of asphalt binders when tested
in dynamic (oscillatory) shear using parallel plate geometry. It is applicable to asphalt binders having dynamic shear modulus
values in the range from 100 Pa to 10 MPa. This range in modulus is typically obtained between 4 and 88°C at 10 rad/s. This test
method is intended for determining the linear viscoelastic properties of asphalt binders as required for specification testing and is
not intended as a comprehensive procedure for the full characterization of the viscoelastic properties of asphalt binders.
1.2 This standard is appropriate for unaged materials, material aged in accordance with Test Method D2872, material aged in
accordance with Practice D6521, or material aged in accordance with both Test Method D2872 and Practice D6521. This procedure
is limited to asphalt binders that contain particles with largest dimension less than 250 μm.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all
of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate
safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C670 Practice for Preparing Precision and Bias Statements for Test Methods for Construction Materials
D140 Practice for Sampling Bituminous Materials
D2170 Test Method for Kinematic Viscosity of Asphalts (Bitumens)
D2171 Test Method for Viscosity of Asphalts by Vacuum Capillary Viscometer
D2872 Test Method for Effect of Heat and Air on a Moving Film of Asphalt (Rolling Thin-Film Oven Test)
D6373 Specification for Performance Graded Asphalt Binder
D6521 Practice for Accelerated Aging of Asphalt Binder Using a Pressurized Aging Vessel (PAV)
E77 Test Method for Inspection and Verification of Thermometers
E563 Practice for Preparation and Use of an Ice-Point Bath as a Reference Temperature
E644 Test Methods for Testing Industrial Resistance Thermometers
E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory
3
2.2 AASHTO Standards:
M320 Standard Specification for Performance-Graded Asphalt Binder
R29 Practice for Grading or Verifying the Performance Grade of an Asphalt Binder
T315 Standard Test Method for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer
4
2.3 Deutsche Industrie Norm (DIN) Standard:
43760 Standard for Calibration of Thermocouples
1
This test method is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.44 on Rheological
Tests.
Current edition approved July 15, 2008July 1, 2015. Published August 2008August 2015. Originally approved in 2005. Last previous edition approved in 20072008 as
D7175 – 07.D7175 – 08. DOI: 10.1520/D7175-08.10.1520/D7175-15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from American Association of State Highway and Transportation Officials (AASHTO), 444 N. Capitol St., NW, Suite 249, Washington, DC 20001,
http://www.transportation.org.
4
Available from Beuth Verlag GmbH (DIN-- DIN Deutsches Institut fur Normung e.V.), Burggrafenstrasse 6, 10787, Berlin, Germany, http://www.en.din.de.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7175 − 15
3. Terminology
3.1 Definitions of Terms Specific to This Standard:
3.1.1 annealing, n—the process of removing the effects of steric harde
...
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D7175 − 15
Standard Test Method for
Determining the Rheological Properties of Asphalt Binder
1
Using a Dynamic Shear Rheometer
This standard is issued under the fixed designation D7175; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This test method covers the determination of the dy-
C670 Practice for Preparing Precision and Bias Statements
namic shear modulus and phase angle of asphalt binders when
for Test Methods for Construction Materials
tested in dynamic (oscillatory) shear using parallel plate
D140 Practice for Sampling Bituminous Materials
geometry. It is applicable to asphalt binders having dynamic
D2170 Test Method for Kinematic Viscosity of Asphalts
shear modulus values in the range from 100 Pa to 10 MPa. This
(Bitumens)
range in modulus is typically obtained between 4 and 88°C at
D2171 Test Method for Viscosity of Asphalts by Vacuum
10 rad/s. This test method is intended for determining the linear
Capillary Viscometer
viscoelastic properties of asphalt binders as required for
D2872 Test Method for Effect of Heat and Air on a Moving
specification testing and is not intended as a comprehensive
Film of Asphalt (Rolling Thin-Film Oven Test)
procedure for the full characterization of the viscoelastic
D6373 Specification for Performance Graded Asphalt
properties of asphalt binders.
Binder
1.2 This standard is appropriate for unaged materials, ma-
D6521 Practice for Accelerated Aging of Asphalt Binder
terial aged in accordance with Test Method D2872, material
Using a Pressurized Aging Vessel (PAV)
aged in accordance with Practice D6521, or material aged in
E77 Test Method for Inspection and Verification of Ther-
accordance with both Test Method D2872 and Practice D6521. mometers
This procedure is limited to asphalt binders that contain
E563 Practice for Preparation and Use of an Ice-Point Bath
particles with largest dimension less than 250 µm. as a Reference Temperature
E644 Test Methods for Testing Industrial Resistance Ther-
1.3 The values stated in SI units are to be regarded as
mometers
standard. No other units of measurement are included in this
E882 Guide for Accountability and Quality Control in the
standard.
Chemical Analysis Laboratory
3
1.4 This standard may involve hazardous materials, 2.2 AASHTO Standards:
operations, and equipment. This standard does not purport to M320 Standard Specification for Performance-Graded As-
address all of the safety concerns, if any, associated with its phalt Binder
use. It is the responsibility of the user of this standard to R29 Practice for Grading or Verifying the Performance
establish appropriate safety and health practices and deter- Grade of an Asphalt Binder
T315 Standard Test Method for Determining the Rheologi-
mine the applicability of regulatory limitations prior to use.
cal Properties of Asphalt Binder Using a Dynamic Shear
1.5 This international standard was developed in accor-
Rheometer
dance with internationally recognized principles on standard-
4
2.3 Deutsche Industrie Norm (DIN) Standard:
ization established in the Decision on Principles for the
43760 Standard for Calibration of Thermocouples
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee. 2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
1 3
This test method is under the jurisdiction of ASTM Committee D04 on Road Available from American Association of State Highway and Transportation
and Paving Materials and is the direct responsibility of Subcommittee D04.44 on Officials (AASHTO), 444 N. Capitol St., NW, Suite 249, Washington, DC 20001,
Rheological Tests. http://www.transportation.org.
4
Current edition approved July 1, 2015. Published August 2015. Originally Available from Beuth Verlag GmbH (DIN-- DIN Deutsches Institut fur
approved in 2005. Last previous edition approved in 2008 as D7175 – 08. DOI: Normung e.V.), Burggrafenstrasse 6, 10787, Berlin, Germany, http://www.en.din.de.
10.1520/D7175-15.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7175 − 15
3. Terminology 4.2 The standard is suitable for use when the dynamic shear
modulus varies between 100 Pa and 10 MPa. This range in
3.
...
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