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ASTM D3013-99

(Specification)

Standard Specification for Epoxy Molding Compounds

Standard Specification for Epoxy Molding Compounds

SCOPE
1.1 This specification covers requirements for epoxy thermosetting molding compounds. It provides for their identification, quality control, and purchase in such a manner that the purchaser and the seller can agree on the substantial similarity of different commercial lots or shipments.
1.2 The compounds covered under this specification consist of mixtures or blends of epoxy resins and curing agents intimately combined, in an unreacted or partially reacted condition, with fillers, reinforcements, colorants, and other chemical agents.
Note 1-The properties included in this specification are those required to identify the kinds of molding compounds covered. There may be other requirements necessary to define particular characteristics. These will be added to the specification as their inclusion becomes generally desirable and the necessary test data and methods become available. Note 2-There is no similar or equivalent ISO standard.

General Information

Status
Historical
Publication Date
09-Nov-1999
ICS
83.140.99 - Other rubber and plastics products
Technical Committee
D20 - Plastics
Drafting Committee
D20.16 - Thermosetting Materials
Current Stage
Ref Project

Relations

Replaced By
ASTM D3013-99(2004)e1 - Standard Specification for Epoxy Molding Compounds
Effective Date
01-Oct-2004

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ASTM D3013-99 - Standard Specification for Epoxy Molding CompoundsASTM D3013-99 - Standard Specification for Epoxy Molding Compounds
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ASTM D3013-99 - Standard Specification for Epoxy Molding Compounds
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 3013 – 99
Standard Specification for
Epoxy Molding Compounds
This standard is issued under the fixed designation D 3013; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope* Insulating Materials for Testing
D 638 Test Method for Tensile Properties of Plastics
1.1 This specification covers requirements for epoxy ther-
D 648 Test Method for Deflection Temperature of Plastics
mosetting molding compounds. It provides for their identifica-
Under Flexural Load
tion, quality control, and purchase in such a manner that the
D 790 TestMethodsforFlexuralPropertiesofUnreinforced
purchaser and the seller can agree on the substantial similarity
and Reinforced Plastics and Electrical Insulating Materials
of different commercial lots or shipments.
D 883 Terminology Relating to Plastics
1.2 The compounds covered under this specification consist
D 1896 Practice for Transfer Molding Specimens of Ther-
of mixtures or blends of epoxy resins and curing agents
mosetting Compounds
intimately combined, in an unreacted or partially reacted
D 2863 Test Method for Measuring the Minimum Oxygen
condition, with fillers, reinforcements, colorants, and other
Concentration to Support Candle-Like Combustion of
chemical agents.
Plastics (Oxygen Index)
1.3 The values stated in SI units are to be regarded as the
D 3892 Practice for Packaging/Packing of Plastics
standard.
2.2 Military Standard:
NOTE 1—The properties included in this specification are those re-
MIL-STD-105 Sampling Procedures and Tables for Inspec-
quired to identify the kinds of molding compounds covered.There may be
tion by Attributes
other requirements necessary to define particular characteristics. These
will be added to the specification as their inclusion becomes generally
3. Terminology
desirable and the necessary test data and methods become available.
3.1 Definitions—Definitions of terms used in this specifica-
NOTE 2—There is no similar or equivalent ISO standard.
tion are in accordance with Terminology D 883.
2. Referenced Documents
2 4. Classification
2.1 ASTM Standards:
4.1 Grades—This specification is subdivided into various
D 149 Test Method for Dielectric Breakdown Voltage and
Dielectric Strength of Solid Electrical Insulating Materials grades of epoxy molding compounds based on physical prop-
erties. This specification provides for a system of characteriza-
at Commercial Power Frequencies
D 150 Test Methods for A-C Loss Characteristics and tion and identification which enables coverage for all commer-
ciallyavailablegradeshavingpropertieswithintherangeofthe
Permittivity (Dielectric Constant) of Solid Electrical Insu-
lating Materials possible combinations as may be selected from Table 1. A
gradeisdesignatedbythecellnumbersforeachpropertyinthe
D 256 Test Method for Determining the Pendulum Impact
Resistance of Notched Specimens of Plastics orderinwhichtheyarelistedinTable1.Whenapropertyisnot
specified, a “0” is entered as the cell number.
D 495 Test Method for High-Voltage, Low-Current, Dry
Arc Resistance of Solid Electrical Insulation 4.2 Classes—Each of the grades of epoxy molding com-
pound may be further subdivided into classes according to
D 570 Test Method for Water Absorption of Plastics
D 618 Practice for Conditioning Plastics and Electrical special requirements. A class is designated by a capital letter
followedbycelldesignationcorrespondingtotherequirements
detailed in Table 2. Where no special requirements, in addition
to grade properties, are needed, no class designation is shown.
This specification is under the jurisdiction of ASTM Committee D-20 on
Plastics and is the direct responsibility of Subcommittee D20.16 on Thermosetting
NOTE 3—An example of this classification system would be grade
Materials.
12324-D-00200-F-3 an epoxy molding compound having the following
Current edition approved Nov. 10, 1999. Published February 2000. Originally
requirements (see Table 1 and Table 2):
published as D 3013 – 72. Last previous edition D 3013 – 94.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on AvailablefromStandardizationDocumentsOrderDesk,Bldg.4SectionD,700
the ASTM website. Robbins Ave., Philadelphia, PA 19111-5094, Attn: NPODS.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D3013–99
TABLE 1 Detail Grade Requirements for Epoxy Molding Compounds
Desig-
Grades (Cell Limits)
nation
Property and Unit
Order
01 2 3 4 5
No.
1 Water absorption, % in 24 h unspecified <0.16 0.16 to 0.30 0.31 to 1.0 1.1 to 3.0 >3.0
2 Flexural strength, MPa unspecified <42 42 to 69 70 to 103 104 to 207 >207
3 Impact resistance, unspecified
J/m of notch <22 22 to 53 54 to 267 268 to 534 >534
4 Tensile strength, unspecified
MPa <35 35 to 55 56 to 103 104 to 138 >138
5 Deflection temperature unspecified
under load,
°C 70 to 100 101 to 150 151 to 200 201 to 250 >250
TABLE 2 Detail Class Requirements for Epoxy Molding Compounds
Designa-
Classes (Cell Limits)
Class
Class tion Order Property and Unit
Designation
01 2 3 4 5
No.
Dielectric D 1 permittivity unspecified <3.81 3.81 to 4.50 4.51 to 5.00 5.01 to 6.00 >6.00
2 dissipation factor unspecified <0.016 0.016 to 0.03 0.04 to 0.10 0.11 to 0.20 >0.20
dielectric strength, V/mil
(short-time):
3 dry unspecified <301 301 to 325 326 to 350 351 to 400 >400
4 wet unspecified min 80 % of dry value using same test
5 arc resistance, s unspecified <61 61 to 110 111 to 140 141 to 180 >180
Flame-retardant F 1 flammability unspecified <25 25 to 40 >40 . .
5. General Requirements
5.1 The molding compounds shall be of uniform composi-
tionandsoformulatedastoconformtotherequirementsofthis
specification.
5.2 The apparent density, bulk factor, flow, particle size, and
color of the compounds shall be as agreed upon between the
purchaser and the seller in the order or contract. Properties
other than those specified in this specification may also be
agree
...

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Standard Specification for Polymeric Piles

ABSTRACT
This specification establishes the physical and performance requirements for round and rectangular cross-section polymeric piles in axial and lateral load-bearing applications including, by not limited to, marine, waterfront, and corrosive environments. It does not apply to individual polymeric pile products, sheet piles, and other mechanically connected polymeric pile products using inter-locking systems. Covered here are six types of polymeric piles that are fabricated from materials that may be virgin, recycled, or both, as long as the finished product meets all of the criteria specified herein. These types are: Type I, polymeric only; Type II, polymeric with reinforcement in the form of chopped, milled or continuous fiber or mineral; Type III, polymeric with reinforcement in the form of metallic bars, cages, or shapes; Type IV, polymeric with reinforcement in the form of non-metallic bars or cages; Type V, polymeric composite tube with a concrete core; and Type VI, any other polymeric piling meeting the requirements stated herein and not otherwise described by Types I through V. The polymeric tiles shall adhere to specified physical attributes such as size, cross-sectional shape, length, straightness, placement of reinforcement, and surface conditions. The performance requirements which pile specimens shall conform to include creep rupture, serviceability, flexural properties, shear strength, bearing strength, design flexural stiffness, energy absorption, compressive strength, combined stresses, dimensional stability (thermal expansion), hygrothermal cycling, and flame spread index.
SCOPE
1.1 This specification addresses the use of round and rectangular cross-section polymeric piles in axial and lateral load-bearing applications, including but not limited to marine, waterfront, and corrosive environments.  
1.2 This specification is only applicable to individual polymeric pile products. Sheet pile and other mechanically connected polymeric pile products using inter-locking systems, are not part of this specification.  
1.3 The piling products considered herein are characterized by the use of polymers, whereby (1) the pile strength or stiffness requires the inclusion of the polymer, or (2) a minimum of fifty percent (50 %) of the weight or volume is derived from the polymer. The type classifications of polymeric piles described in Section 4 show how they can be reinforced by composite design for increased stiffness or strength.  
1.4 This specification covers polymeric piles fabricated from materials that are virgin, recycled, or both, as long as the finished product meets all of the criteria specified herein. Diverse types and combinations of inorganic filler systems are permitted in the manufacturing of polymeric piling products. Inorganic fillers include such materials as talc, mica, silica, wollastonite, calcium carbonate, etc. Pilings are often placed in service where they will be subjected to continuous damp or wet exposure conditions. Due to concerns of water sensitivity and possible affects on mechanical properties in such service conditions, organic fillers, including lignocellulosic materials such as those made or derived from wood, wood flour, flax shive, rice hulls, wheat straw, and combinations thereof, are not permitted in the manufacturing of polymeric piling products.  
1.5 The values are stated in inch-pound units as these are currently the most common units used by the construction industry.  
1.6 Polymeric piles under this specification are designed using design stresses determined in accordance with Test Methods D6108, D6109, and D6112 and procedures contained within this specification unless otherwise specified.  
1.7 Although in some instances it will be an important component of the pile design, frictional properties are currently beyond the scope of this document.  
1.8 Criteria for design are included as part of this specification for polymeric piles. Certain Types and...

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ASTM
ASTM D7486-22(Test Method)
Standard Test Method for Measurement of Fines and Dust Particles on Plastic Pellets by Wet Analysis

SIGNIFICANCE AND USE
5.1 Molding and extruding plastic pellets require dust free, dry pellets to prevent processing problems. Plastic producers try to remove the dust and streamers with dust removal systems prior to packaging and loading. How to accurately measure dust and streamer content in plastic pellets is an important quality control issue.  
5.2 Particle size analysis is used to determine a percentage of particle size distribution from a representative sample of the whole. In terms of size analysis concerning plastic pellets, sieving is used to determine the dust content in the range of 500 to 2000 micron. Test Method D1921, Test Method B, is used to determine this type of particle sizing.  
5.3 After dry sieve analysis, particles smaller than 500 microns need to be analyzed by wet method. A fresh sample shall be used for wet analysis. This test method allows washing down the fines attached to the pellets by electrostatic forces.  
5.4 The wet analysis provides accurate quantification of small to large amounts of fines, negating static effects, and eliminating detrimental effects of mechanical agitation. A wet analysis must be employed to accurately quantify lower PPM dust levels in plastic pellets.
SCOPE
1.1 This test method measures the amount of fine particles adhered on plastic pellets or granules in which they are commonly produced and supplied. The lower limit of this test method is restricted only by the porosity of the filter disc used to capture the particle size being quantified.  
1.2 The wet analysis technique allows for separation and collection of statically charged particles by liquid wash and filtration methods. This must be performed under standard laboratory conditions.  
1.3 The values stated in SI units are to be regarded as standard.  
1.4 This test method describes an essential practice to check the quality of plastics once the production cycle is terminated and to evaluate the performance of pellet cleaning systems or of the special pneumatic conveying systems for the distinct size fractions below 500 micron only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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