Standard Guide for Recovered Carbon Black—Carbon Black Test Methods for Testing rCB

SIGNIFICANCE AND USE
3.1 Committee D36 has concluded that typical carbon black characterization methods based on structure level and surface area measurements do not seem to correlate to in-rubber performance in an equal manner for Recovered Carbon Black products. Therefore, the committee does not recommend such test methods for predicting the applications performance of recovered carbon black products. The committee is open to new research that can contradict above statement.  
3.2 Committee D36 approved to recognize the standards in 2.1 as acceptable for use in the rCB industry until rCB statistical data is available that may suggest otherwise.
SCOPE
1.1 This guide includes a list of standards under jurisdiction of ASTM Committee D24 on Carbon Black; however, they can be applied for use in the rCB industry.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
31-May-2022
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ASTM D8466-22 - Standard Guide for Recovered Carbon Black—Carbon Black Test Methods for Testing rCB
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8466 − 22
Standard Guide for
Recovered Carbon Black—Carbon Black Test Methods for
1
Testing rCB
This standard is issued under the fixed designation D8466; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D1900 Practice for Carbon Black—Sampling Bulk Ship-
ments
1.1 This guide includes a list of standards under jurisdiction
D1937 Test Method for Carbon Black, Pelleted—Mass
ofASTM Committee D24 on Carbon Black; however, they can
Strength
be applied for use in the rCB industry.
D2663 Test Methods for Carbon Black—Dispersion in Rub-
1.2 This standard does not purport to address all of the
ber
safety concerns, if any, associated with its use. It is the
D3053 Terminology Relating to Carbon Black
responsibility of the user of this standard to establish appro-
D3191 Test Methods for Carbon Black in SBR (Styrene-
priate safety, health, and environmental practices and deter-
Butadiene Rubber)—Recipe and Evaluation Procedures
mine the applicability of regulatory limitations prior to use.
D3192 Test Methods for Carbon Black Evaluation in NR
1.3 This international standard was developed in accor-
(Natural Rubber)
dance with internationally recognized principles on standard-
D3849 Test Method for Carbon Black—Morphological
ization established in the Decision on Principles for the
Characterization of Carbon Black Using Electron Micros-
Development of International Standards, Guides and Recom-
copy
mendations issued by the World Trade Organization Technical
D4122 Practice for Carbon Black—Evaluation of an Indus-
Barriers to Trade (TBT) Committee.
try Reference Black
D4821 Guide for Carbon Black—Validation of Test Method
2. Referenced Documents
Precision and Bias
2
2.1 ASTM Standards:
D5230 Test Method for Carbon Black—Automated Indi-
D1506 Test Methods for Carbon Black—Ash Content
vidual Pellet Hardness
D1508 Test Method for Carbon Black, Pelleted Fines and
D5817 Practice for Carbon Black, Pelleted—Reduction,
Attrition
Blending, and Drying of Gross Samples for Testing
D1509 Test Methods for Carbon Black—Heating Loss
D6915 Practice for Carbon Black—Evaluation of Standard
D1511 Test Method for Carbon Black—Pellet Size Distri-
Reference Blacks
bution
D7771 Test Method for Determination of Benzo-α-Pyrene
D1512 Test Methods for Carbon Black—pH Value
(BaP) Content in Carbon Black
D1513 Test Method for Carbon Black, Pelleted—Pour Den-
3. Significance and Use
sity
D1514 Test Method for Carbon Black—Sieve Residue 3.1 Committee D36 has concluded that typical carbon black
D1618 Test Method for Carbon Black Extractables— characterization methods based on structure level and surface
Transmittance of Toluene Extract area measurements do not seem to correlate to in-rubber
D1619 Test Methods for Carbon Black—Sulfur Content performance in an equal manner for Recovered Carbon Black
D1799 Practice for Carbon Black—Sampling Packaged products. Therefore, the committee does not recommend such
Shipments test methods for predicting the applications performance of
recovered carbon black products. The committee is open to
new research that can contradict above statement.
1
This guide is under the jurisdiction of ASTM Committee D36 on Recovered
3.2 Committee D36 approved to recognize the standards in
Carbon Black (rCB) and is the direct responsibility of Subcommittee D36.10 on
2.1 as acceptable for use in the rCB industry until rCB
Recovered Carbon Black.
Current edition approved June 1, 2022. Published June 2022. DOI: 10.1520/
statistical data is available that may suggest otherwise.
D8466-22.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
4. Carbon Black Standards for Use in rCB Testing
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.1 Properties—Ash Content according to Test Methods
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. D1506, Pellet Fines and Attrition according to Test Method
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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D8466 − 22
size or aggregate size, or both, of the carbon black component of rCB.
D1508, Heating Loss according to Test Methods D1509, Pellet
Size Distribution according to Test Method D1511, pH Value
4.2 Sampling and Preparation—Sampling Packaged Ship-
according to Test Methods D1512, Pour Density accor
...

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