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ASTM D5239-98

(Practice)

Standard Practice for Characterizing Fly Ash for Use in Soil Stabilization

Standard Practice for Characterizing Fly Ash for Use in Soil Stabilization

SCOPE
1.1 This practice covers procedures for characterizing fly ash to be used in soil stabilization. This practice lists representative test methods for determining the chemical, physical, and cementitious properties of fly ash. A broad guideline is provided in X1 that explains the significance of these properties in soil stabilization.
1.2 The values stated in inch-pound units are to be regarded as the standard. The SI units given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-May-1998
ICS
93.020 - Earthworks. Excavations. Foundation construction. Underground works
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.15 - Stabilization With Admixtures
Current Stage
Ref Project

Relations

Replaced By
ASTM D5239-04 - Standard Practice for Characterizing Fly Ash for Use in Soil Stabilization
Effective Date
01-Nov-2004
Referred By
ASTM E2243-13(2019) - Standard Guide for Use of Coal Combustion Products (CCPs) for Surface Mine Reclamation: Re-contouring and Highwall Reclamation
Effective Date
10-May-1998
Referred By
ASTM D5759-12(2020) - Standard Guide for Characterization of Coal Fly Ash and Clean Coal Combustion Fly Ash for Potential Uses
Effective Date
10-May-1998
Referred By
ASTM D7762-18e1 - Standard Practice for Design of Stabilization of Soil and Soil-Like Materials with Self-Cementing Fly Ash
Effective Date
10-May-1998
Referred By
ASTM E2277-14(2019) - Standard Guide for Design and Construction of Coal Ash Structural Fills
Effective Date
10-May-1998
Referred By
ASTM E2278-13(2019) - Standard Guide for Use of Coal Combustion Products (CCPs) for Surface Mine Reclamation: Revegetation and Mitigation of Acid Mine Drainage
Effective Date
10-May-1998

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ASTM D5239-98 - Standard Practice for Characterizing Fly Ash for Use in Soil StabilizationASTM D5239-98 - Standard Practice for Characterizing Fly Ash for Use in Soil Stabilization
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ASTM D5239-98 - Standard Practice for Characterizing Fly Ash for Use in Soil Stabilization
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D 5239–98
Standard Practice for
Characterizing Fly Ash for Use in Soil Stabilization
This standard is issued under the fixed designation D 5239; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope * C 191 Test Method for Time of Setting of Hydraulic Ce-
ment by Vicat Needle
1.1 This practice covers procedures for characterizing fly
C 265 Test Method for Calcium Sulfate in Hydrated Port-
ash to be used in soil stabilization. This practice lists represen-
land Cement Mortar
tative test methods for determining the chemical, physical, and
C 305 PracticeforMechanicalMixingofHydraulicCement
cementitious properties of fly ash. A broad guideline is pro-
Pastes and Mortars of Plastic Consistency
vided in Appendix X1 that explains the significance of these
C 311 Test Methods for Sampling and Testing Fly Ash or
properties in soil stabilization.
Natural Pozzolans for Use as a Mineral Admixture in
1.2 The values stated in SI units are to be regarded as the
Portland Cement Concrete
standard. The inch-pound equivalents are shown for informa-
C 593 Specification for Fly Ash and Other Pozzolans for
tion only.
Use with Lime
1.3 This standard does not purport to address all of the
C 618 Specification for Coal Fly Ash and Raw or Calcined
safety concerns, if any, associated with its use. It is the
Natural Pozzolan for Use as a Mineral Admixture in
responsibility of the user of this standard to establish appro-
Concrete
priate safety and health practices and determine the applica-
C 821 Specification for Lime for Use with Pozzolans
bility of regulatory limitations prior to use.
C 977 Specification for Quicklime and Hydrated Lime for
1.4 This practice offers a set of instructions for performing
Soil Stabilization
one or more specific operations. This document cannot replace
D 653 Terminology Relating to Soil, Rock and Contained
education or experience and should be used in conjunction
Fluids
with professional judgment. Not all aspects of this practice may
D 1293 Test Methods for pH of Water
be applicable in all circumstances. This ASTM standard is not
D 3551 Practice for Laboratory Preparation of Soil-Lime
intended to represent or replace the standard of care by which
Mixtures Using a Mechanical Mixer
the adequacy of a given professional service must be judged,
nor should this document be applied without consideration of
3. Terminology
a project’s many unique aspects. The word “Standard” in the
3.1 Definitions—Except as follows in 3.2, all definitions are
title of this document means only that the document has been
in accordance with Terminology D 653.
approved through the ASTM consensus process.
3.2 non self-cementing fly ash—fly ash produced from the
2. Referenced Documents combustion of pulverized or crushed coal. This fly ash has
pozzolanic properties and no self-cementing properties.
2.1 ASTM Standards:
3.2.1 self-cementing fly ash—fly ash produced from the
C 25 Test Methods for Chemical Analysis of Limestone,
combustion of pulverized or crushed coal. This fly ash, in
Quicklime, and Hydrated Lime
addition to having pozzolanic properties, sets and hardens by
C 109 Test Method for Compressive Strength of Hydraulic
chemical interaction with water and is capable of doing so
Cement Mortars (Using 2-in. or 50-mm Cube Specimens)
under water.
C 114 Test Methods for Chemical Analysis of Hydraulic
3.2.2 stabilizing admixtures—admixtures used to improve
Cement
soil properties such as increased soil freeze-thaw durability,
C 150 Specification for Portland Cement
stiffness,andstrength;reductionofpermeability,plasticity,and
swelling; increased control of soil compressibility and mois-
ture.
This practice is under the jurisdiction of ASTM Committee D-18 on Soil and
Rock and is the direct responsibility of Subcommittee D18.15 on Stabilization
Admixtures.
Current edition approved May 10, 1998. Published October 1998. Originally Annual Book of ASTM Standards, Vol 04.02.
published as D 5239 – 92. Last previous edition D 5239 – 92. Annual Book of ASTM Standards, Vol 11.01.
2 5
Annual Book of ASTM Standards, Vol 04.01. Annual Book of ASTM Standards, Vol 04.08.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D 5239
4. Significance and Use 6.4 Self-Cementing Properties—Determine the self-
cementing properties of fly ash by the compressive strength
4.1 This practice is intended for use with fly ash that can be
method given in Test Method C 109 except use no sand nor
used separately or along with other stabilizing admixtures to
Portland cement and mixtures shall contain fly ash plus tap
improve soil properties.
water at water-to-fly ash weight ratio of 0.35.Test compressive
4.2 The characterization of the physical and chemical prop-
strength at one and seven days. Mix the paste in accordance
erties of the fly ash should assist in the evaluation of the fly ash
with Method C 305. Mixing time may have to be modified for
for soil stabilization.
quick-setting fly ashes.
4.3 This practice is not intended to limit the flexibility of
6.4.1 Very Self-Cementing Fly Ash—Compressive strengths
design in soil stabilization. The degree of success attained in
greater than (345 MPa) 500 psi at seven days.
soil stabilization is highly dependent on the particular combi-
6.4.2 Moderately Self-Cementing Fly Ash—Compressive
nation of soil, fly ash, and other additives and the construction
strengths greater than or equal to (70 MPa) 100 psi but less
procedure used. Demonstrated sound engineering procedures
than or equal to (345 MPa) 500 psi at seven days.
that result in appropriate physical characteristics are accept-
6.4.3 Non Self-Cementing Fly Ash—Compressive strengths
able. The selection of appropriate materials, applicable tests,
less than (70 MPa) 100 psi at seven days.
acceptancecriteria,andspecificationistheresponsibilityofthe
6.5 Lime-Pozzolanic Activity—Determine the lime-
design engineer.
pozzolan strength development in accordance with Specifica-
tion C 593. For purposes of standardization, the lime must
5. Fly Ash Quality Assurance Program
meet Specification C 821.
5.1 Pre-Qualification—A fly ash is pre-qualified if it is
6.6 Strength Activity Index with Portland Cement—
sampled in accordance wit
...

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ASTM D5102/D5102M-24(Test Method)
Standard Test Methods for Unconfined Compressive Strength of Compacted Soil-Lime Mixtures

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1.1 This test method covers procedures for preparing, curing, and testing laboratory-compacted specimens of soil-lime and other lime-treated materials (Note 1) for determining unconfined compressive strength. Depending on the diameter to height ratio, two procedures for determining the unconfined compressive strength of compacted soil-lime mixtures have been developed for specimens prepared at the maximum unit weight and optimum water content, or for specimens prepared at other target unit weight and water content levels. Other applications are given in Section 5 on Significance and Use.
Note 1: Lime-based products other than commercial quicklime and hydrated lime are also used in the lime treatment of fine-grained cohesive soils. Lime kiln dust (LKD) is collected from the kiln exhaust gases by cyclone, electrostatic, or baghouse-type collection systems. Some lime producers hydrate various blends of LKD plus quicklime to produce a lime-based product.  
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1.3.2 Procedure B describes procedures for preparing and testing compacted soil-lime specimens using Test Methods D698 compaction equipment and molds commonly available in most soil testing laboratories. Procedure B is considered to provide relative measures of individual specimens in a suite of test specimens rather than standard compressive strength values. Because of the lesser height-to-diameter ratio (1.15) of the cylinders, compressive strength determined by Procedure B will normally be greater than that by Procedure A.  
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ASTM D4648/D4648M-24(Test Method)
Standard Test Methods for Laboratory Miniature Vane Shear Test for Saturated Fine-Grained Soil

SIGNIFICANCE AND USE
5.1 The miniature vane shear test may be used to obtain estimates of the undrained shear strength of fine-grained soils. The test provides a rapid determination of the undrained shear strength on undisturbed, or remolded or reconstituted soils.
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Note 1: Vane failure conditions in higher strength clay and predominately silty soils may deviate from the assumed cylindrical failure surface, thereby causing error in the measured strength.  
1.2 These test methods include the use of both conventional calibrated torque spring units (Method A) and electrical torque transducer units (Method B) with a motorized miniature vane shear device.  
1.3 Laboratory vane is an ideal tool to investigate strength anisotropy in the vertical and horizontal directions, if suitable samples (specimens) are available.  
1.4 The values stated in either inch-pound units or SI units [presented in brackets] are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Reporting of test results in units other than inch-pound shall not be regarded as nonconformance with this standard.  
1.4.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs. The rationalized slug unit is not given, unless dynamic (F = ma) calculations are involved.  
1.5 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.  
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4.1 These test methods are used to determine the resistance of compacted soil-cement specimens to repeated wetting and drying. These test methods were developed to be used in conjunction with Test Methods D560/D560M and criteria given in the Soil-Cement Laboratory Handbook4 to determine the minimum amount of cement required in soil-cement to achieve a degree of hardness adequate to resist field weathering.
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1.2 Two test methods, depending on soil gradation, are covered for preparation of material for molding specimens and for molding specimens as follows:    
Sections  
Test Method A, using soil material passing a 4.75-mm [No. 4] sieve.
This method shall be used when 100 % of the soil sample passes the 4.75-mm [No. 4] sieve.  
7  
Test Method B, using soil material passing a 19.0 mm [0.75-in.] sieve.
This method shall be used when part of the soil sample is retained on the 4.75-mm [No. 4] sieve.
This test method may be used only on materials with 30 % or less retained on the 19.0-mm [0.75-in.] sieve.  
8  
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1.1 This practice presents a procedure for calculating the unit weights and water contents of soils containing oversize particles when the data are known for the soil fraction with the oversize particles removed.  
1.2 This practice also can be used to calculate the unit weights and water contents of soil fractions when the data are known for the total soil sample containing oversize particles.  
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5.1 By definition, the tensile strength is obtained by the direct tensile test. However, the direct tensile test is difficult and expensive for routine application. The splitting tensile test appears to offer a desirable alternative because it is much simpler and inexpensive. Furthermore, engineers involved in rock mechanics design usually deal with complex stress fields, including various combinations of compressive and tensile stress fields. Under such conditions, the tensile strength should be obtained with the presence of compressive stresses to be representative of the field conditions.  
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Note 2: The quality of the results produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 This test method covers testing apparatus, specimen preparation, and testing procedures for determining the splitting tensile strength of rock by diametral line compression of disk shaped specimens.
Note 1: The tensile strength of rock determined by tests other than the straight pull test is designated as the “indirect” tensile strength and, specifically, the value obtained in Section 9 of this test is termed the “splitting” tensile strength. This test method is also sometimes referred to as the Brazilian test method.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units, which are provided for information only and are not considered standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this test method.  
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1.3.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, the purpose for obtaining the data, special purpose studies, or any considerations for the user's objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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Standard Test Methods for Detecting Water Soluble Sulfates in Construction Soils

SIGNIFICANCE AND USE
5.1 Where sulfates are suspected, subgrade soils should be tested as an integral part of a geotechnical evaluation because the possibility that sulfate induced heave may occur if calcium containing stabilizers are used to improve the soils and sulfate reactions may also cause deterioration in concrete structures. When planning to treat a soil used in construction with lime, testing the soil for water soluble sulfates prior to treatment becomes very important (Note 2).  
5.2 When sulfate containing cohesive soils are treated with calcium-based stabilizers for foundation improvements, sulfates and free alumina in natural soils react with calcium and free hydroxide to form crystalline minerals, such as ettringite and thaumasite.4 Thaumasite forms when ettringite undergoes changes in the presence of carbonates at low temperatures.5 The sulfate minerals expand considerably when they are hydrated.
Note 2: For more information on the effect of treating soils containing water soluble sulfates, refer to the following publication: Little, D.N., Stabilization of Pavement Subgrades and Base Course with Lime, Kendal/Hunt Publishing Co., Dubuque, IA, 1995.
Note 3: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 These methods determine the water soluble sulfate content of cohesive soils used in construction by using the colorimetric technique. Two methods are presented in this standard. Method A is for use in the field and Method B is for use in the laboratory. The colorimetric technique involves measuring the scattering of a light beam through a solution that contains suspended particulate matter. Measurements of sulfate concentrations in construction soils can be used to guide professionals in the selection of appropriate stabilization methods and to assist in assessment of potential deterioration in concrete structures.
Note 1: These test methods are partially based on the research conducted by Texas A & M University.  
1.2 The field method, Method A, is used as a screening test for the presence of sulfates and their concentration. The laboratory method, Method B, provides better resolution than the field method.  
1.3 Ion chromatography is also an acceptable alternative method that can be used to evaluate results, however, it is outside the scope of this standard.  
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.  
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ASTM D2850-23(Test Method)
Standard Test Method for Unconsolidated-Undrained Triaxial Compression Test on Cohesive Soils

SIGNIFICANCE AND USE
5.1 In this test method, the compressive strength of a soil is determined in terms of the total stress, therefore, the resulting strength depends on the pressure developed in the pore fluid during loading. In this test method, fluid flow is not permitted from or into the soil specimen as the load is applied, therefore the resulting pore pressure, and hence strength, differs from that developed in the case where drainage can occur.  
5.2 If the test specimens is 100 % saturated, consolidation cannot occur when the confining pressure is applied nor during the shear portion of the test since drainage is not permitted. Therefore, if several specimens of the same material are tested, and if they are all at approximately the same water content and void ratio when they are tested, they will have approximately the same unconsolidated-undrained shear strength.  
5.3 If the test specimens are partially saturated, or compacted/reconstituted specimens, where the degree of saturation is less than 100 %, consolidation may occur when the confining pressure is applied and during application of axial load, even though drainage is not permitted. Therefore, if several partially saturated specimens of the same material are tested at different confining stresses, they will not have the same unconsolidated-undrained shear strength.  
5.4 Mohr failure envelopes may be plotted from a series of unconsolidated undrained triaxial tests. The Mohr’s circles at failure based on total stresses are constructed by plotting a half circle with a radius of half the principal stress difference (deviator stress) beginning at the axial stress (major principal stress) and ending at the confining stress (minor principal stress) on a graph with principal stresses as the abscissa and shear stress as the ordinate and equal scale in both directions. The failure envelopes will usually be a horizontal line for saturated specimens and a curved line for partially saturated specimens.  
5.5 The unconsolidated-u...
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1.1 This test method covers determination of the strength and stress-strain relationships of a cylindrical specimen of either intact, compacted, or remolded cohesive soil. Specimens are subjected to a confining fluid pressure in a triaxial chamber. No drainage of the specimen is permitted during the application of the confining fluid pressure or during the compression phase of the test. The specimen is axially loaded at a constant rate of axial deformation (strain controlled).  
1.2 This test method provides data for determining undrained strength properties and stress-strain relations for soils. This test method provides for the measurement of the total stresses applied to the specimen, that is, the stresses are not corrected for pore-water pressure.
Note 1: The determination of the unconfined compressive strength of cohesive soils is covered by Test Method D2166/D2166M.
Note 2: The determination of the consolidated, undrained strength of cohesive soils with pore pressure measurement is covered by Test Method D4767.  
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.3.1 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.4 Units—The values stated in SI units are to be regarded as the standard. The values given in parentheses are mathemat...

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ASTM
ASTM D4219-22(Test Method)
Standard Test Method for Short-Term Unconfined Compressive Strength Index of Chemically Grouted Soils

SIGNIFICANCE AND USE
5.1 The purpose of this test method is to obtain values for comparison with other test values to verify uniformity of materials or the effects of controllable variables, in grout-soil compositions.  
5.2 This test method is similar, in principle, to Test Method D2166/D2166M, but is not intended for determination of strength parameters to be used in design. Such values are more properly obtained from long-term triaxial tests.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 This test method covers the determination of the short-term unconfined compressive strength index of chemically grouted soils, using displacement-controlled application of test load.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.2.1 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This practice implicitly combines two separate systems of units; the absolute and the gravitational systems. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit of mass. However, the use of balances and scales recording pounds of mass (lbm) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.  
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.  
1.3.1 For purposes of comparing a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal of significant digits in the specified limit.  
1.3.2 The procedures used to specify how data are collected/recorded or calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4381/D4381M-22(Test Method)
Standard Test Method for Sand Content by Volume of Construction Slurries

SIGNIFICANCE AND USE
5.1 This test method is used to determine the percentage of sand by volume in construction slurry. The significance of this test method mainly relates to construction slurries used for concrete wall and drilled piers construction. The range of measurement is too limited for use in applications where the sand content is intended to be greater than 20 %, such as in the cases of cement bentonite or soil bentonite walls.  
5.2 A high sand content in the construction slurry is abrasive for construction plant such as pumps, and is furthermore adverse to the formation of a filter cake in applications where bentonite fluid is used to stabilize an excavation.
Note 1: The quality of the result produced by this standard depends on the competence of the personnel performing it and the suitability of the equipment and facilities being used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method covers the determination of the sand content of bentonitic slurries used in slurry construction techniques. This test method has been modified from API Recommended Practice 13B.  
1.2 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Except, the sieve designation is identified using the “alternative” system in accordance with Practice E11 instead of the “standard system,” such that the sieve used is referred to as a No. 200 sieve, instead of a 75 µm sieve.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4452/D4452M-22(Practice)
Standard Practice for X-Ray Radiography of Soil Samples

SIGNIFICANCE AND USE
5.1 Many geotechnical tests require the utilization of intact, representative samples of soil. The quality of these samples depends on many factors. Many of the samples obtained by intact sampling methods have inherent anomalies. Sampling procedures cause disturbances of varying types and intensities. These anomalies and disturbances, however, are not always readily detectable by visual inspection of the intact samples before or after testing. Often test results would be enhanced if the presence and the extent of these anomalies and disturbances are known before testing or before destruction of the sample by testing. Such determinations assist the user in detecting flaws in sampling methods, the presence of natural or induced shear planes, and the presence of natural intrusions, such as gravels or shells at critical regions in the samples, the presence of sand and silt seams, and the intensity of disturbances caused by sampling.  
5.2 X-ray radiography provides the user with a picture of the internal massive structure of the soil sample, regardless of whether the soil is X-rayed within or without the sampling tube. X-ray radiography assists the user in identifying the following:  
5.2.1 Appropriateness of sampling methods used.  
5.2.2 Effects of sampling in terms of the disturbances caused by the turning of the edges of various thin layers in varved soils, large disturbances caused in soft soils, shear planes induced by sampling, or extrusion, or both, effects of overdriving of samplers, the presence of cuttings in sampling tubes, or the effects of using bent, corroded, or nonstandard tubes for sampling.  
5.2.3 Naturally occurring fissures, shear planes, etc.  
5.2.4 The presence of intrusions within the sample, such as calcareous nodules, gravel, or shells.  
5.2.5 Sand and silt seams, organic matter, large voids, and channels developed by natural or artificial leaching of soil components.
Note 1: The quality of the results produced by this standard is de...
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1.1 This practice covers the determination of the quality of soil samples in thin wall tubes or of extruded soil cores by X-ray radiography.  
1.2 This practice enables the user to determine the effects of sampling and natural variations within samples as identified by the extent of the relative penetration of X-rays through soil samples.  
1.3 This practice can be used to X-ray soil cores (or observe their features on a fluoroscope) in thin wall tubes or liners ranging from approximately 50 to 150 mm [2 to 6 in.] in diameter. X-rays of samples in the larger diameter tubes provide a radiograph of major features of soils and disturbances, such as large scale bending of edges of varved clays, shear planes, the presence of large concretions, silt and sand seams thicker than 6 mm [1/4 in.], large lumps of organic matter, and voids or other types of intrusions. X-rays of the smaller diameter cores provide higher resolution of soil features and disturbances, such as small concretions (3 mm [1/8 in.] diameter or larger), solution channels, slight bending of edges of varved clays, thin silt or sand seams, narrow solution channels, plant root structures, and organic matter. The X-raying of samples in thin wall tubes or liners requires minimal preparation.  
1.4 Greater detail and resolution of various features of the soil can be obtained by X-raying extruded soil cores, as compared to samples in metal tubes. The method used for X-raying soil cores is the same as that for tubes and liners, except that extruded cores have to be handled with extreme care and have to be placed in sample troughs (similar to Fig. 2) before X-raying. This practice should be used only when natural water content or other intact soil characteristics are irrelevant to the end use of the sample.  
1.4.1 Often it is necessary to obtain greater resolution of features to determine the propriety of sampling methods, the representative nature of soil samples,...

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