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ASTM D5220-02

(Test Method)

Standard Test Method for Water Content of Soil and Rock In-Place by the Neutron Depth Probe Method

Standard Test Method for Water Content of Soil and Rock In-Place by the Neutron Depth Probe Method

SIGNIFICANCE AND USE
This test method is useful as a rapid, nondestructive technique for the calculation of the in-place water content of soil and rock at desired depths below the surface.  
This test method is useful for informational and research purposes. It should only be used for quality control and acceptance testing when correlated to actual water contents using procedures and methods described in A1.2.3.
The non-destructive nature of this test method allows repetitive measurements to be made at a single test location for statistical analysis and to monitor changes over time.  
The fundamental assumptions inherent in this test method are that the material under test is homogeneous and hydrogen present is in the form of water as defined by Test Method D 2216.
SCOPE
1.1 This test method covers the calculation of the water content of soil and rock by thermalization or slowing of fast neutrons where the neutron source and the thermal neutron detector are placed at the desired depth in the bored hole lined by an access tube (see Note 1).
1.2 The water content, in mass per unit volume of the material under test, is calculated by comparing the thermal neutron count rate with previously established calibration data (see Annex A1).
1.3 A precision statement has not been developed for this standard at this time. Therefore, this standard should not be used for acceptance or rejection of a material for purchasing purposes unless correlated to other accepted ASTM methods.
1.4 The values expressed in SI units are regarded as the standard. The inch-pound units given in parentheses may be approximate and are provided for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards are given in Section 7.

General Information

Status
Historical
Publication Date
09-Feb-2002
ICS
13.080.40 - Hydrological properties of soils
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.08 - Special and Construction Control Tests
Current Stage
Ref Project

Relations

Replaces
ASTM D5220-92(1997) - Standard Test Method for Water Content of Soil and Rock In-Place by the Neutron Depth Probe Method
Effective Date
10-Feb-2002
Replaced By
ASTM D5220-08 - Standard Test Method for Water Mass per Unit Volume of Soil and Rock In-Place by the Neutron Depth Probe Method
Effective Date
01-Oct-2008
Referred By
ASTM D6031/D6031M-96(2015) - Standard Test Method for Logging In Situ Moisture Content and Density of Soil and Rock by the Nuclear Method in Horizontal, Slanted, and Vertical Access Tubes
Effective Date
10-Feb-2002

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ASTM D5220-02 - Standard Test Method for Water Content of Soil and Rock In-Place by the Neutron Depth Probe MethodASTM D5220-02 - Standard Test Method for Water Content of Soil and Rock In-Place by the Neutron Depth Probe Method
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ASTM D5220-02 - Standard Test Method for Water Content of Soil and Rock In-Place by the Neutron Depth Probe Method
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D 5220–02
Standard Test Method for
Water Content of Soil and Rock In-Place by the Neutron
1
Depth Probe Method
This standard is issued under the fixed designation D 5220; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D 2937 Test Method for Density of Soil in Place by the
2
Drive-Cylinder Method
1.1 This test method covers the calculation of the water
D 3017 Test Method for Moisture Content of Soil and
content of soil and rock by thermalization or slowing of fast
Soil-Aggregate in Place by Nuclear Methods (Shallow
neutrons where the neutron source and the thermal neutron
2
Depth)
detector are placed at the desired depth in the bored hole lined
2
D 3550 Practice for Ring-Lined Barrel Sampling of Soils
by an access tube (see Note 1).
D 4428/D 4228M Test Method for Crosshole Seismic Test-
1.2 The water content, in mass per unit volume of the
2
ing
material under test, is calculated by comparing the thermal
D 5195 Test Method for Density of Soil and Rock in Place
neutron count rate with previously established calibration data
3
at Depths Below the Surface by Nuclear Methods
(see Annex A1).
1.3 A precision statement has not been developed for this
3. Summary of Test Method
standard at this time. Therefore, this standard should not be
3.1 This test method uses thermalization of neutron radia-
used for acceptance or rejection of a material for purchasing
tion to calculate the in-place water content of soil and rock at
purposes unless correlated to other accepted ASTM methods.
various depths by placing a probe containing a neutron source
1.4 The values expressed in SI units are regarded as the
andathermalneutrondetectoratdesireddepthsinaboredhole
standard. The inch-pound units given in parentheses may be
lined by an access tube as opposed to surface measurements in
approximate and are provided for information only.
accordance with Test Method D 3017.
1.5 This standard does not purport to address all of the
3.2 Neutronsemittedbythesourcearethermalized(slowed)
safety concerns, if any, associated with its use. It is the
by collisions with materials of low atomic numbers. Hydrog-
responsibility of the user of this standard to establish appro-
enous materials, such as water and other compounds contain-
priate safety and health practices and determine the applica-
ing hydrogen, are most effective in thermalizing neutrons. In
bilityofregulatorylimitationspriortouse.Specifichazardsare
this apparatus the neutrons thermalized by the material under
given in Section 7.
test are detected by the thermal neutron detector.
2. Referenced Documents 3.3 In the absence of interference elements as discussed in
Section 5, the number of thermalized neutrons is a function of
2.1 ASTM Standards:
the hydrogen content of the material under test and the water
D 1452 Practice for Soil Investigation and Sampling by
2 content is proportional to the hydrogen content.
Auger Borings
3.4 By the use of a calibration process the water content is
D 1586 Method for Penetration Test and Split-Barrel Sam-
2 calculated by correlating the count rate to known water
pling of Soils
2
contents.
D 1587 Practice for Thin Walled Tube Sampling of Soils
D2113 Practice for Diamond Core Drilling for Site Inves-
4. Significance and Use
2
tigation
4.1 This test method is useful as a rapid, nondestructive
D 2216 Test Method for Laboratory Determination ofWater
technique for the calculation of the in-place water content of
(Moisture) Content of Soil, Rock, and Soil-Aggregate
2
soil and rock at desired depths below the surface.
Mixtures
4.2 Thistestmethodisusefulforinformationalandresearch
purposes. It should only be used for quality control and
1
This test method is under the jurisdiction ofASTM Committee D18 on Soil and
acceptance testing when correlated to actual water contents
Rock and is the direct responsibility of Subcommittee D18.08 on Special and
using procedures and methods described in A1.2.3.
Construction Control Tests.
Current edition approved Feb. 10, 2002. Published May 2002. Originally
published as D 5220–92. Last previous edition D 5220–92(1997)
2 3
Annual Book of ASTM Standards, Vol 04.08. Annual Book of ASTM Standards, Vol 04.09.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D 5220–02
4.3 The non-destructive nature of this test method allows
repetitive measurements to be made at a single test location for
statistical analysis and to monitor changes over time.
4.4 The fundamental assumptions inhere
...

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1.1 This test method describes the procedures for measuring the water mass per unit volume of soil and soil-aggregate by use of an in situ permittivity probe. Measurements are taken at a depth beneath the surface of the soil determined by the design of the probe.  
1.1.1 For limitations see Section 6 on Interferences.  
1.2 The permittivity probe is inserted into a hole drilled or punched into the soil being measured. As its name indicates, the probe measures the dielectric permittivity of the soil into which it is placed. Two electrodes, connected to an oscillating circuit, are mounted a predetermined distance apart. These electrodes act as the plates of a capacitor, with the soil between the plates forming the capacitor dielectric.  
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ASTM D5220/D5220M-21(Test Method)
Standard Test Method for Water Mass per Unit Volume of Soil and Rock In-Place by the Neutron Depth Probe Method

SIGNIFICANCE AND USE
5.1 This test method is useful as a rapid, nondestructive technique for the measurement of the in-place water mass per unit volume of soil and rock at desired depths below the surface.  
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5.1 Understanding the mechanical properties of frozen soils is of primary importance to permafrost engineering. Data from creep tests are necessary for the design of most foundation elements embedded in, or bearing on frozen ground. They make it possible to predict the time-dependent settlements of piles and shallow foundations under service loads, and to estimate their short- and long-term bearing capacity. Creep tests also provide quantitative parameters for the stability analysis of underground structures that are created for permanent use.  
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1.1 This test method covers the determination of the creep behavior of cylindrical specimens of frozen soil, subjected to uniaxial compression. It specifies the apparatus, instrumentation, and procedures for determining the stress-strain-time, or strength versus strain rate relationships for frozen soils under deviatoric creep conditions.  
1.2 Although this test method is one that is most commonly used, it is recognized that creep properties of frozen soil related to certain specific applications, can also be obtained by some alternative procedures, such as stress-relaxation tests, simple shear tests, and beam flexure tests. Creep testing under triaxial test conditions will be covered in another standard.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
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1.4.2 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
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SIGNIFICANCE AND USE
5.1 The water content of soil is used throughout geotechnical engineering practice, both in the laboratory and in the field. Results are sometimes needed within a short time period and in locations where it is not practical to install an oven or to transport samples to an oven. This test method is used for these occasions.  
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1.1 This test method outlines procedures for determining the water (moisture) content of soil by chemical reaction using calcium carbide as a reagent to react with the available water in the soil producing a gas. A measurement is made of the gas pressure produced when a specified mass of wet or moist soil is placed in a testing device with an appropriate volume of reagent and mixed.  
1.2 This test method is not intended as a replacement for Test Method D2216; but as a supplement when rapid results are required, when testing is done in field locations, or where an oven is not practical for use. Test Method D2216 is to be used as the test method to compare for accuracy checks and correction.  
1.3 This test method is applicable for most soils. Calcium carbide, used as a reagent, reacts with water as it is mixed with the soil by shaking and agitating with the aid of steel balls in the apparatus. To produce accurate results, the reagent must react with all the water which is not chemically hydrated with soil minerals or compounds in the soil. Some highly plastic clay soils or other soils not friable enough to break up may not produce representative results because some of the water may be trapped inside soil clods or clumps which cannot come in contact with the reagent. There may be some soils containing certain compounds or chemicals that will react unpredictably with the reagent and give erroneous results. Any such problem will become evident as calibration or check tests with Test Method D2216 are made. Some soils containing compounds or minerals that dehydrate with heat (such as gypsum) which are to have special temperature control with Test Method D2216 may not be affected (dehydrated) in this test method.  
1.4 This test method is limited to using calcium carbide moisture test equipment made for 20 g, or larger, soil specimens and to testing soil which contains particles no larger than the 4.75 mm (No. 4) Standard sieve size.  
1.5 The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are mathematical conversions, which are provided for information purposes only and are not considered standard.  
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5.1 The water content of a soil is used throughout geotechnical engineering practice both in the laboratory and in the field. The use of Test Method D2216 for water content determination can be time consuming and there are occasions when a more expedient method is desirable. The use of a microwave oven is one such method.  
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5.4 This test method is best suited for minus 4.75-mm (No. 4) sieve sized material. Larger size particles can be tested; however, care must be taken because of the increased chance of particle shattering.  
5.5 The use of this method may not be appropriate when highly accurate results are required, or the test using the data is extremely sensitive to moisture variations.  
5.6 Due to the localized high temperatures that the specimen is exposed to in microwave heating, the physical characteristics of the soil may be altered. Degregation of individual particles may occur, along with vaporization or chemical transition. It is therefore recommended that samples used in this test method not be used for other tests subsequent to drying.
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1.1 This test method outlines procedures for determining the water content of soils by incrementally drying soil in a microwave oven.  
1.2 This test method can be used as a substitute for Test Method D2216 when more rapid results are desired to expedite other phases of testing and slightly less accurate results are acceptable.  
1.3 When questions of accuracy between this test method and Test Method D2216 arise, Test Method D2216 shall be the referee method.  
1.4 This test method is applicable for most soil types. For some soils, such as those containing significant amounts of halloysite, mica, montmorillonite, gypsum or other hydrated materials, highly organic soils, or soils in which the pore water contains significant amounts of dissolved solids (such as salt in the case of marine deposits), this test method may not yield reliable water content values due to the potential for heating above 110°C or lack of means to account for the presence of precipitated solids that were previously dissolved.  
1.5 The values stated in SI units are to be regarded as the standard. Performance of the test method utilizing another system of units shall not be considered non-conformance. The sieve designations are identified using the “standard” system in accordance with Specification E11, such as 2.0-mm and 19-mm, followed by the “alternative” system of No. 10 and 3/4-in., respectively, in parentheses.  
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ASTM
ASTM D8037/D8037M-16(Practice)
Standard Practice for Direct Push Hydraulic Logging for Profiling Variations of Permeability in Soils

SIGNIFICANCE AND USE
5.1 The injection logging system provides a rapid and efficient way to ascertain the pressure required to inject water into unconsolidated formations at the given flow rate in real time (Fig. 1) (1-4, 7).5 The measured injection pressure and flow rate are then used to assess variations in formation permeability versus depth and infer changes in formation lithology and understand the local hydrostratigraphy (1-4, 8-16). Log interpretation should be confirmed with targeted soil coring adjacent to selected log locations or running logs adjacent to one or more previously logged borings. Practice D3740 was developed for agencies engaged in the testing and/or inspection of soils and rock. As such, it is not totally applicable to agencies performing this practice. However, users of this practice should recognize that the framework of Practice D3740 is appropriate for evaluating the quality of an agency performing this practice. Currently there is no known qualifying national authority that inspects agencies that perform this practice.
SCOPE
1.1 This practice describes a method for rapid delineation of variations in formation permeability in the subsurface using an injection logging tool. Clean water is injected from a port on the side of the probe as it is advanced at approximately 2cm/s into virgin soils. Logging with the injection tool is typically performed with direct push equipment, however other drilling machines may be modified to run the logs by direct push methods (for example, addition of a suitable hammer and/or hydraulic ram systems). Injection logs exceeding 100 ft [30m] depth have been obtained. Direct push methods are not intended to penetrate consolidated rock and may encounter refusal in very dense formations or when cobbles or boulders are encountered in the subsurface. However, injection logging has been performed in some semi-consolidated or soft formations.  
1.2 This standard practice describes how to obtain a real time vertical log of injection pressure and flow rate with depth. The data obtained is indicative of the variations of permeability in the subsurface and is typically used to infer formation lithology. The person(s) responsible for review, interpretation and application of the injection logging data should be familiar with the logging technique as well as the soils, geology and hydrogeology of the area under investigation.  
1.3 The injection logging system may be operated with a built in electrical conductivity sensor to provide additional real time information on stratigraphy and is essential for targeting test zones. Other sensors, such as fluorescence detectors (Practice D6187), a membrane interface probe (Practice D7352) or a cone penetration tool (Test Method D5778) may be used in conjunction with injection logging to provide additional information. The use of the injection logging tool in concert with an electrical conductivity array or cone penetration tool is highly recommended (although not mandatory) to further define hydrostratigraphic conditions, such as migration pathways, low permeability zones (for example, aquitards) and to guide confirmation sampling. The EC log and injection pressure log may be compared in some settings to identify the presence of ionic contaminants or ionic injectates used for remediation.  
1.4 The injection logging system does not provide quantitative permeability or hydraulic conductivity information. However, injection pressure and flow data may be used to provide a qualitative indication of formation permeability. Semi-quantitative values of permeability may be obtained by correlation of injection logging data with other methods (1-4).2 Also, a log of estimated hydraulic conductivity (5) may be calculated for the saturated zone using an empirical model included in some versions of the log viewing software. The data allows for estimates of hydraulic conductivity (K) at the inch-scale using the corrected injection pressure ...

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ASTM
ASTM D6836-16(Test Method)
Standard Test Methods for Determination of the Soil Water Characteristic Curve for Desorption Using Hanging Column, Pressure Extractor, Chilled Mirror Hygrometer, or Centrifuge

SIGNIFICANCE AND USE
5.1 The soil water characteristic curve (SWCC) is fundamental to hydrological characterization of unsaturated soils and is required for most analyses of water movement in unsaturated soils. The SWCC is also used in characterizing the shear strength and compressibility of unsaturated soils. The unsaturated hydraulic conductivity of soil is often estimated using properties of the SWCC and the saturated hydraulic conductivity.  
5.2 This method applies only to soils containing two pore fluids: a gas and a liquid. The liquid is usually water and the gas is usually air. Other liquids may also be used, but caution must be exercised if the liquid being used causes excessive shrinkage or swelling of the soil matrix.  
5.3 A full investigation has not been conducted regarding the correlation between soil water characteristic curves obtained using this method and soil water characteristics curves of in-place materials. Thus, results obtained from this method should be applied to field situations with caution and by qualified personnel.
Note 1: The quality of the result produced by this standard depends on the competence of the personnel performing the test and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors. Practice D3740 provides a means of evaluating some of these factors.
SCOPE
1.1 These test methods cover the determination of soil water characteristic curves (SWCCs) for desorption (drying). SWCCs describe the relationship between suction and volumetric water content, gravimetric water content, or degree of water saturation. SWCCs are also referred to as soil water retention curves, soil water release curves, or capillary pressure curves.  
1.2 This standard describes five methods (A-E) for determining the soil water characteristic curve. Method A (hanging column) is suitable for making determinations for suctions in the range of 0 to 80 kPa. Method B (pressure chamber with volumetric measurement) and Method C (pressure chamber with gravimetric measurement) are suitable for suctions in the range of 0 to 1500 kPa. Method D (chilled mirror hygrometer) is suitable for making determinations for suctions in the range of 500 kPa to 100 MPa. Method E (centrifuge method) is suitable for making determinations in the range 0 to 120 kPa. Method A typically is used for coarse soils with little fines that drain readily. Methods B and C typically are used for finer soils, which retain water more tightly. Method D is used when suctions near saturation are not required and commonly is employed to define the dry end of the soil water characteristic curve (that is, water contents corresponding to suctions >1000 kPa). Method E is typically used for coarser soils where an appreciable amount of water can be extracted with suctions up to 120 kPa. The methods may be combined to provide a detailed description of the soil water characteristic curve. In this application, Method A or E is used to define the soil water characteristic curve at lower suctions (0 to 80 kPa for A, 0 to 120 kPa for E) near saturation and to accurately identify the air entry suction, Method B or C is used to define the soil water characteristic curve for intermediate water contents and suctions (100 to 1000 kPa), and Method D is used to define the soil water characteristic curves at low water contents and higher suctions (>1000 kPa).  
1.3 All observed and calculated values shall conform to the guide for significant digits and rounding established in Practice D6026. The procedures in Practice D6026 that are used to specify how data are collected, recorded, and calculated are regarded as the industry standard. In addition, they are represe...

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ASTM
ASTM D4959-16(Test Method)
Standard Test Method for Determination of Water Content of Soil By Direct Heating

SIGNIFICANCE AND USE
5.1 The water content of a soil is used throughout geotechnical engineering practice both in the laboratory and in the field. The use of Test Methods D2216 for water content determination can be time consuming and there are occasions when a more expedient method is desirable. Drying by direct heating is one such method. Results of this test method have been demonstrated to be of satisfactory accuracy for use in field control work, such as in the determination of water content, and in the determination of in-place dry unit weight of soils.  
5.2 The principal objection to the use of the direct heating for water content determination is the possibility of overheating the soil, thereby yielding a water content higher than would be determined by Test Methods D2216. While not eliminating this possibility, the incremental drying procedure in this test method will minimize its effects. Some heat sources have settings or controls that can also be used to reduce overheating. Loose fitting covers or enclosures can also be used to reduce overheating while assisting in uniform heat distribution.  
5.3 The behavior of a soil when subjected to direct heating is dependent on its mineralogical composition, and as a result, no one procedure is applicable for all types of soils or heat sources. The general procedure of this test method applies to all soils, but test details may need to be tailored to the soil being tested.  
5.4 When this test method is to be used repeatedly on the same or similar soil from a given site, a correction factor can usually be determined by making several comparisons between the results of this test method and Test Methods D2216. A correction factor is valid when the difference is consistent for several comparisons, and is reconfirmed on a regular specified basis.  
5.5 This test method may not be appropriate when precise results are required, or when minor variations in water content will affect the results of other test methods, such as borderline s...
SCOPE
1.1 This test method covers procedures for determining the water content of soils by drying with direct heat, such as using a hotplate, stove, blowtorch, and the like.  
1.2 This test method can be used as a substitute for Test Methods D2216 when more rapid results are desired to expedite other phases of testing and slightly less accurate results are acceptable.  
1.3 When questions of accuracy between this test method and Test Methods D2216 arise, Test Methods D2216 shall be the referee method.  
1.4 This test method is applicable for most soil types. For some soils, such as those containing significant amounts of halloysite, mica, montmorillonite, gypsum, or other hydrated materials, highly organic soils or soils that contain dissolved solids, (such as salt in the case of marine deposits), this test method may not yield reliable water content values due to the potential for heating above 110°C or lack of means to account for the presence of precipitated solids that were previously dissolved.  
1.5 The values stated in SI units are to be regarded as standard. Performance of the test method utilizing another system of units shall not be considered non-conformance. The sieve designations are identified using the “standard” system in accordance with Specification E11, such as 2.0-mm and 19-mm, followed by the “alternative” system of No. 10 and 3/4-in., respectively, in parentheses.  
1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in D6026, unless otherwise superseded by this standard.  
1.6.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any consider...

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