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ASTM D1201-99

(Specification)

Standard Specification for Thermosetting Polyester Molding Compounds

Standard Specification for Thermosetting Polyester Molding Compounds

SCOPE
1.1 This specification covers compression molding thermosetting compounds consisting of unsaturated polyester resin binders that have been combined with fillers, pigments, and other chemical agents.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are given for information only.
Note 1-The properties included in this specification are those required to identify the types of molding compounds covered. There may be other requirements necessary to identify particular characteristics. These will be added to the specification as their inclusion becomes generally desirable and the necessary test data and methods become available.
Note 2--ISO 3672-1: 1979(E) is similar but not equivalent to this specification. Product classifications and characterization are not equivalent.

General Information

Status
Historical
Publication Date
09-Nov-1999
ICS
83.140.99 - Other rubber and plastics products
Technical Committee
D20 - Plastics
Drafting Committee
D20.16 - Thermosetting Materials
Current Stage
Ref Project

Relations

Replaced By
ASTM D1201-99(2004) - Standard Specification for Thermosetting Polyester Molding Compounds
Effective Date
01-Oct-2004

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ASTM D1201-99 - Standard Specification for Thermosetting Polyester Molding CompoundsASTM D1201-99 - Standard Specification for Thermosetting Polyester Molding Compounds
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ASTM D1201-99 - Standard Specification for Thermosetting Polyester Molding Compounds
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 1201 – 99
Standard Specification for
Thermosetting Polyester Molding Compounds
This standard is issued under the fixed designation D 1201; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope * 3. Classification
1.1 This specification covers compression molding, thermo- 3.1 This specification covers the following types of polyes-
setting, unsaturated polyester molding compounds as further ter molding compounds:
defined in 3.1. 3.1.1 Type 1—General-purpose, granular material with min-
1.2 The values stated in SI units are to be regarded as the eral fillers.
standard. 3.1.2 Type 2—General-purpose, granular material with min-
eral and cellulosic fillers, and having improved mechanical
NOTE 1—The properties included in this specification are those re-
strength.
quired to identify the types of molding compounds covered.There may be
3.1.3 Type 3—General-purpose, putty-type material with
other requirements necessary to identify particular characteristics. These
mineral fillers.
will be added to the specification as their inclusion becomes generally
desirable and the necessary test data and methods become available.
3.1.4 Type 4—Putty-type material with mineral fillers hav-
NOTE 2—ISO 3672–1: 1979(E) is similar but not equivalent to this
ing superior electrical properties.
specification. Product classification and characterization are not equiva-
3.1.5 Type 5—High-impact, glass-fiber filled material in
lent.
mat form. It has good electrical properties.
3.1.6 Type 6—High-impact, glass-fiber filled material in
2. Referenced Documents
putty form.
2.1 ASTM Standards:
D 256 Test Method for Determining the Pendulum Impact
4. General Requirements
Resistance of Notched Specimens of Plastics
4.1 The molding compounds shall be of uniform composi-
D 495 Test Method for High-Voltage, Low-Current, Dry
tion, so compounded as to conform to the requirements
Arc Resistance of Solid Electrical Insulation
prescribed in this specification.
D 570 Test Method for Water Absorption of Plastics
4.2 The apparent density, bulk factor, particle size, physical
D 618 Practice for Conditioning Plastics and Electrical
form, and color of the compound shall be as agreed upon
Insulating Materials for Testing
between the purchaser and supplier.
D 790 TestMethodsforFlexuralPropertiesofUnreinforced
and Reinforced Plastics and Electrical Insulating Materi- NOTE 3—The terms “apparent density,” “bulk factor,” and “particle
size” cannot be used in the same sense with putty-type and glass-filled
als
materials as with granular materials.
D 792 TestMethodsforDensityandSpecificGravity(Rela-
tive Density) of Plastics by Displacement
5. Detail Requirements
D 3892 Practice for Packaging/Packing of Plastics
5.1 Test specimens, molded by compression under condi-
2.2 ISO Standard:
tions specified by the manufacturer, shall conform to the
ISO 3672–1: 1979(E) Plastics—Unsaturated Polyester
requirements prescribed in Table 1.
Resins—Part 1: Designation
6. Sampling
6.1 Abatchofmoldingcompoundshallbeconsideredaunit
This specification is under the jurisdiction of ASTM Committee D-20 on
Plastics and is the direct responsibility of Subcommittee D20.16 on Thermosetting
of manufacture and may consist of a blend of two or more
Materials.
production runs of the same material.
Current edition approved Nov. 10, 1999. Published February 2000. Originally
published as D 1201 – 52. Last previous edition D 1201 – 81 (1992).
Annual Book of ASTM Standards, Vol 08.01.
Annual Book of ASTM Standards, Vol 10.01.
Annual Book of ASTM Standards, Vol 08.02.
Available from American National Standards Institute, 11 W. 42nd St., 13th
Floor, New York, NY 10036.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D 1201
TABLE 1 Detail Requirements for Compression-Molded Test Specimens
Type 1 Type 2 Type 3 Type 4 Type 5 Type 6
Specific gravity, 23/23°C:
min 2.18 1.6 1.7 1.9 1.95 1.75
max 2.28 1.9 1.9 2.1 2.10 1.90
Flexural strength, min:
MPa 51.7 65.5 51.7 51.7 82.7 82.7
Modulus of elasticity in flexure, min:
MPa 13 800 8 960 8 960 12 400 13 800 11 000
Impact resistance (Izod), min, J/m of notch . . . . 320(6) 320(6)
Arc resistance, min, s 175 125 125 175 130 75
Water absorption, 24 h, max, % 0.15 1.0 0.5 0.15 0.15 0.25
6.2 Adequate statistical sampling shall
...

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4.1 This guide provides information, requirements and recommendations for design professionals, fabricators, installers and end-users of FRP chimney liners. FRP is a cost-effective and appropriate material of construction for liners operating at moderate temperatures in a corrosive chemical environment.  
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1.6 Field erection, sequence of construction, proper field-joint preparation, and alignment are reviewed.  
1.7 Quality control and assurance procedures are developed for the design, fabrication, and erection phases. The quality-assurance program defines the proper authority and responsibility, control of design, material, fabrication and erection, inspection procedures, tolerances, and conformity to standards. The quality-control procedures provide the steps required to implement the quality-assurance program.  
1.8 Appendix X1 includes research and development subjects to further support recommendations of this guide.  
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Standard Specification for Rigid Poly(Vinyl Chloride) (PVC) Exterior-Profile Extrusions Used for Assembled Windows and Doors

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This specification establishes requirements for the material properties, including dimensional stability, weatherability, and extrusion quality, of rigid poly(vinyl chloride) (PVC) exterior profile extrusions used for assembled windows and doors. Methods for testing and for identifying exterior profile extrusions that comply with this specification are also provided. The physical and performance requirements of PVC are presented in details. The dimensional stability and impact strength shall be tested to meet the requirements prescribed.
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1.1 This specification establishes requirements for the material properties, including dimensional stability, weatherability, and extrusion quality, of rigid poly(vinyl chloride) (PVC) exterior profile extrusions used for assembled windows and doors. Methods for testing and for identifying exterior profile extrusions that comply with this specification are also provided.  
1.2 The use of rigid PVC recycled plastic in this product shall be in accordance with the requirements in Section 6.
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5.1 Heat buildup in PVC exterior building products due to absorption of the energy from the sun may lead to distortion problems. Heat buildup is affected by the color, emittance, absorptance, and reflectance of a product. Generally, the darker the color of the product, the more energy is absorbed and the greater is the heat buildup. However, even with the same apparent color, the heat buildup may vary due to the specific pigment system involved. The greatest heat buildup generally occurs in the color black containing carbon black pigment. The black control sample used in this test method contains 2.5 parts of furnace black per 100 parts of PVC suspension resin. The maximum temperature rise above ambient temperature for this black is 90°F (50°C) for a 45° or horizontal surface when the sun is perpendicular to the surface and 74°F (41°C) for a vertical surface assuming that the measurements were done on a cloudless day with no wind and heavy insulation on the back of the specimen.4  
5.2 This test method allows the measurement of the temperature rise under a specific type heat lamp, relative to that of a black reference surface, thus predicting the heat buildup due to the sun's energy.  
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SCOPE
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Note 2: There are no ISO standards covering the primary subject matter of this test method.  
1.2 Rigid PVC exterior profile extrusions for assembled windows and doors are covered in Specification D4726.  
1.3 Rigid PVC exterior profiles for fencing are covered in Specification F964.  
1.4 Rigid PVC siding profiles are covered in Specification D3679.  
1.5 Rigid PVC soffit profiles are covered in Specification D4477.  
1.6 Rigid PVC and Rigid CPVC plastic building products compounds are covered in Specification D4216.  
1.7 The text of this test method references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this test method.  
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5.1 When properly used, these procedures serve to isolate such factors as material, blow-molding conditions, post-treatment, and so forth, on the stress-crack resistance of the container.  
5.2 Environmental stress cracking of blow-molded containers is governed by many factors. Since variance of any of these factors can change the environmental stress-crack resistance of the container, the test results are representative only of a given test performed under defined conditions in the laboratory. The reproducibility of results between laboratories on containers made on more than one machine from more than one mold has not been established.  
5.3 Results can be used for estimating the shelf life of blow-molded containers in terms of their resistance to environmental stress cracking provided this is done against a rigorous background of practical field experience and reproducible test data.
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1.2.2 Procedure B, Stress-Crack Resistance of a Specific Container to Polyoxyethylated Nonylphenol (CAS 68412-54-4), a Stress-Cracking Agent—The conditions of test described in this procedure are designed for testing containers made from Class 3 polyethylene Specification D4976. Therefore, this procedure is recommended for containers made from Class 3 polyethylene only. This procedure is particularly useful for determining the effect of resin on the stress-crack resistance of the container.  
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Note 2: There is no known ISO equivalent to this standard.  
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4.1 Column crush tests only provide information about the crush properties of blown thermoplastic containers when employed under conditions approximating those under which the tests are conducted.  
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1.1 This test method covers the determination of mechanical properties of blown thermoplastic containers, whether blown commercially or in the laboratory, loaded under columnar crush conditions at a constant rate of compressive deflection.
Note 1: Although this test method was developed specifically for blow-molded containers, the general procedure can also be applied to containers of suitable geometries produced by other means, for example, thermoforming, injection molding, etc.  
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5.1 These procedures provide a means to assess the drop impact resistance of the group or lot of blown containers from which the test specimens were selected.  
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1.2.2 Procedure B, Bruceton Staircase Method—This procedure is used to determine the mean failure height and the standard deviation of the distribution.  
1.3 The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are for information only.  
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This specification covers requirements and methods of test for the material, dimensions, and workmanship, and the properties of extruded, compression molded, and injection molded PAEK sheet, plate, rod, and tubular bar manufactured from PAEK. The type of PAEK extruded, compression molded, and injection molded product may be categorized by type, grade and class depending on resin and filler compositions. Every type of PAEK shape may be categorized into one of several grades as follows: Grade 1 (general purpose) which is extruded, compression molded or injection molded product made using only 100% virgin PAEK resin and Grade 2 (recycle grade) which is extruded, compression molded or injection molded product made using any amount up to 100% of recycled thermoplastic PAEK. The type, class and grade is further differentiated based on dimensional stability. Different tests shall be conducted in order to determine the following properties of PAEK: tensile stress at break, elongation at break, tensile modulus, dimensional stability, lengthwise camber and widthwise bow, squareness, flexural modulus, and Izod impact.
SCOPE
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1.2 The properties included in this specification are those required for the compositions covered. Requirements necessary to identify particular characteristics important to specialized applications are described by using the classification system given in Section 4.  
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1.4 The values are stated in inch-pound units and are regarded as the standard in all property and dimensional tables. For reference purposes, SI units are also included in Table 1.  
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SCOPE
1.1 This classification system covers requirements for plasticized cellulose acetate butyrate thermoplastic compounds suitable for injection molding and extrusion. These compounds have a butyryl content less than 38 % and an acetyl content less than 15 % and can contain dyes and pigments. This classification system does not include special materials compounded for special applications. Cellulosic plastic materials, being thermoplastic, are reprocessable and recyclable. This classification system allows for the use of those cellulosic materials, provided that all specific requirements of this classification system are met.  
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1.4 The values stated in SI units are to be regarded as standard.  
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SCOPE
1.1 This specification addresses the use of round and rectangular cross-section polymeric piles in axial and lateral load-bearing applications, including but not limited to marine, waterfront, and corrosive environments.  
1.2 This specification is only applicable to individual polymeric pile products. Sheet pile and other mechanically connected polymeric pile products using inter-locking systems, are not part of this specification.  
1.3 The piling products considered herein are characterized by the use of polymers, whereby (1) the pile strength or stiffness requires the inclusion of the polymer, or (2) a minimum of fifty percent (50 %) of the weight or volume is derived from the polymer. The type classifications of polymeric piles described in Section 4 show how they can be reinforced by composite design for increased stiffness or strength.  
1.4 This specification covers polymeric piles fabricated from materials that are virgin, recycled, or both, as long as the finished product meets all of the criteria specified herein. Diverse types and combinations of inorganic filler systems are permitted in the manufacturing of polymeric piling products. Inorganic fillers include such materials as talc, mica, silica, wollastonite, calcium carbonate, etc. Pilings are often placed in service where they will be subjected to continuous damp or wet exposure conditions. Due to concerns of water sensitivity and possible affects on mechanical properties in such service conditions, organic fillers, including lignocellulosic materials such as those made or derived from wood, wood flour, flax shive, rice hulls, wheat straw, and combinations thereof, are not permitted in the manufacturing of polymeric piling products.  
1.5 The values are stated in inch-pound units as these are currently the most common units used by the construction industry.  
1.6 Polymeric piles under this specification are designed using design stresses determined in accordance with Test Methods D6108, D6109, and D6112 and procedures contained within this specification unless otherwise specified.  
1.7 Although in some instances it will be an important component of the pile design, frictional properties are currently beyond the scope of this document.  
1.8 Criteria for design are included as part of this specification for polymeric piles. Certain Types and...

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ASTM
ASTM D7486-22(Test Method)
Standard Test Method for Measurement of Fines and Dust Particles on Plastic Pellets by Wet Analysis

SIGNIFICANCE AND USE
5.1 Molding and extruding plastic pellets require dust free, dry pellets to prevent processing problems. Plastic producers try to remove the dust and streamers with dust removal systems prior to packaging and loading. How to accurately measure dust and streamer content in plastic pellets is an important quality control issue.  
5.2 Particle size analysis is used to determine a percentage of particle size distribution from a representative sample of the whole. In terms of size analysis concerning plastic pellets, sieving is used to determine the dust content in the range of 500 to 2000 micron. Test Method D1921, Test Method B, is used to determine this type of particle sizing.  
5.3 After dry sieve analysis, particles smaller than 500 microns need to be analyzed by wet method. A fresh sample shall be used for wet analysis. This test method allows washing down the fines attached to the pellets by electrostatic forces.  
5.4 The wet analysis provides accurate quantification of small to large amounts of fines, negating static effects, and eliminating detrimental effects of mechanical agitation. A wet analysis must be employed to accurately quantify lower PPM dust levels in plastic pellets.
SCOPE
1.1 This test method measures the amount of fine particles adhered on plastic pellets or granules in which they are commonly produced and supplied. The lower limit of this test method is restricted only by the porosity of the filter disc used to capture the particle size being quantified.  
1.2 The wet analysis technique allows for separation and collection of statically charged particles by liquid wash and filtration methods. This must be performed under standard laboratory conditions.  
1.3 The values stated in SI units are to be regarded as standard.  
1.4 This test method describes an essential practice to check the quality of plastics once the production cycle is terminated and to evaluate the performance of pellet cleaning systems or of the special pneumatic conveying systems for the distinct size fractions below 500 micron only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: There is no known ISO equivalent to this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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