Bitumen and bituminous binders - Determination of the distillation characteristics of cut-back and fluxed bituminous binders made with mineral fluxes

This document specifies a method for the determination of the distillation characteristics of cut-back and fluxed bituminous binders made with mineral fluxes.
WARNING - The use of this document may involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this document to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung der Destillationseigenschaften von mit Mineralölfluxmitteln verschnittenen und gefluxten bitumenhaltigen Bindemitteln

Dieses Dokument legt ein Verfahren für die Bestimmung der Destillationseigenschaften von mit Mineralölfluxmitteln verschnittenen und gefluxten bitumenhaltigen Bindemitteln fest.
WARNUNG — Die Anwendung dieses Dokuments kann gefährliche Substanzen, Arbeitsgänge und Ausrüstung einschließen. Dieses Dokument beansprucht nicht, alle Sicherheitsprobleme zu behandeln, die mit seiner Anwendung verbunden sind. Es liegt in der Verantwortung des Anwenders dieses Dokuments, vor dessen Anwendung geeignete Sicherheits- und Gesundheitsschutzmaßnahmen vorzusehen und zu prüfen, ob einschränkende Vorschriften zu berücksichtigen sind.

Bitumes et liants bitumineux - Détermination des caractéristiques de distillation des bitumes fluidifiés et fluxés par des fluxants d'origine minérale

Le présent document spécifie une méthode de détermination des caractéristiques de distillation des liants bitumineux fluidifiés et fluxés avec des fluxants d’origine minérale.
AVERTISSEMENT — L'utilisation de ce document peut impliquer l'intervention de produits, d'opérations et d'équipements à caractère dangereux. Le présent document n'est pas censé aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de ce document de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določevanje destilacijskih značilnosti rezanih in fluksiranih bitumenskih veziv

Ta dokument določa metodo za določevanje destilacijskih značilnosti rezanih in fluksiranih bitumenskih veziv.
OPOZORILO: Pri uporabi tega evropskega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta evropski standard ne obravnava vseh varnostnih težav, ki se navezujejo na njegovo uporabo. Za vzpostavitev ustreznih varnostnih in zdravstvenih praks ter za določitev uporabnosti regulativnih omejitev pred uporabo je odgovoren uporabnik tega evropskega standarda.

General Information

Status
Published
Publication Date
16-Jul-2019
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Due Date
17-Jul-2019
Completion Date
17-Jul-2019

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SLOVENSKI STANDARD
SIST EN 13358:2019
01-november-2019
Nadomešča:
SIST EN 13358:2010
Bitumen in bitumenska veziva - Določevanje destilacijskih značilnosti rezanih in
fluksiranih bitumenskih veziv

Bitumen and bituminous binders - Determination of the distillation characteristics of cut-

back and fluxed bituminous binders made with mineral fluxes

Bitumen und bitumenhaltige Bindemittel - Bestimmung der Destillationseigenschaften

von mit Mineralölfluxmitteln verschnittenen und gefluxten bitumenhaltigen Bindemitteln

Bitumes et liants bitumineux - Détermination des caractéristiques de distillation des

bitumes fluidifiés et fluxés par des fluxants d'origine minérale
Ta slovenski standard je istoveten z: EN 13358:2019
ICS:
75.140 Voski, bitumni in drugi naftni Waxes, bituminous materials
proizvodi and other petroleum products
91.100.50 Veziva. Tesnilni materiali Binders. Sealing materials
SIST EN 13358:2019 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 13358:2019
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SIST EN 13358:2019
EN 13358
EUROPEAN STANDARD
NORME EUROPÉENNE
July 2019
EUROPÄISCHE NORM
ICS 91.100.50 Supersedes EN 13358:2010
English Version
Bitumen and bituminous binders - Determination of the
distillation characteristics of cut-back and fluxed
bituminous binders made with mineral fluxes

Bitumes et liants bitumineux - Détermination des Bitumen und bitumenhaltige Bindemittel -

caractéristiques de distillation des bitumes fluidifiés et Bestimmung der Destillationseigenschaften von mit

fluxés par des fluxants d'origine minérale Mineralölfluxmitteln verschnittenen und gefluxten

bitumenhaltigen Bindemitteln
This European Standard was approved by CEN on 19 May 2019.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this

European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references

concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN

member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by

translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management

Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2019 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 13358:2019 E

worldwide for CEN national Members.
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SIST EN 13358:2019
EN 13358:2019 (E)
Contents Page

European foreword ....................................................................................................................................................... 3

1 Scope .................................................................................................................................................................... 4

2 Normative references .................................................................................................................................... 4

3 Terms and definitions ................................................................................................................................... 4

4 Principle ............................................................................................................................................................. 4

5 Apparatus ........................................................................................................................................................... 4

6 Procedure........................................................................................................................................................... 6

6.1 General ................................................................................................................................................................ 6

6.2 Preparation of test samples ........................................................................................................................ 6

6.3 Preparation of apparatus ............................................................................................................................. 6

6.4 Test procedure ................................................................................................................................................. 7

7 Calculation ......................................................................................................................................................... 9

7.1 Bituminous residue after distillation ...................................................................................................... 9

7.2 Total distillate .................................................................................................................................................. 9

7.3 Distillate fractions .......................................................................................................................................... 9

8 Expression of results ................................................................................................................................... 10

9 Precision .......................................................................................................................................................... 10

9.1 Repeatability .................................................................................................................................................. 10

9.2 Reproducibility ............................................................................................................................................. 10

10 Test report ...................................................................................................................................................... 10

Annex A (informative) Specification of thermometer ................................................................................. 14

Bibliography ................................................................................................................................................................. 15

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SIST EN 13358:2019
EN 13358:2019 (E)
European foreword

This document (EN 13358:2019) has been prepared by Technical Committee CEN/TC 336 “Bitumen and

bituminous binders”, the secretariat of which is held by AFNOR.

This European Standard shall be given the status of a national standard, either by publication of an

identical text or by endorsement, at the latest by January 2020, and conflicting national standards shall

be withdrawn at the latest by January 2020.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. CEN shall not be held responsible for identifying any or all such patent rights.

This document supersedes EN 13358:2010.
The main technical changes in comparison to the previous edition are:

— Clause 5: an electric heating plate or heating mantle may be used as alternatives to the gas burner;

— Clause 5: mercury stem thermometers are replaced by temperature measuring devices allowing

similar temperature determinations to be made. Annex A (characteristics of mercury stem

thermometer) becomes informative;

— Subclause 6.4.2: requirements on distillation rate (drops per minute) may be replaced by a minimum

rate of temperature increase in cases where the distillation process has a very low yield;

— Subclause 6.4.3: volumes of distillate are to be recorded at least at the reference corrected

temperatures mentioned in EN 15322;

— Clauses 6.4.3 and 10: the possibility to record volumes of distillate to a precision of 0,1 ml is

abandoned.
This document is based on ASTM D 402-97.

According to the CEN-CENELEC Internal Regulations, the national standards organisations of the

following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia,

Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland,

Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of North

Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United

Kingdom.
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SIST EN 13358:2019
EN 13358:2019 (E)
1 Scope

This document specifies a method for the determination of the distillation characteristics of cut-back and

fluxed bituminous binders made with mineral fluxes.

WARNING — The use of this document may involve hazardous materials, operations and

equipment. This document does not purport to address all of the safety problems associated with

its use. It is the responsibility of the user of this document to establish appropriate safety and

health practices and to determine the applicability of regulatory limitations prior to use.

2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

EN 58, Bitumen and bituminous binders — Sampling bituminous binders
EN 12594, Bitumen and bituminous binders — Preparation of test samples
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.

ISO and IEC maintain terminological databases for use in standardization at the following addresses:

— IEC Electropedia: available at http://www.electropedia.org/
— ISO Online browsing platform: available at https://www.iso.org/obp
3.1
distillation
process of evaporation and condensation of a liquid
3.2
mineral flux
flux which may be of carbochemical or petrochemical origin or a mixture of both
4 Principle

Petroleum cut-back and fluxed bituminous binders are distilled at a controlled rate until the temperature

of the liquid reaches 360 °C. The volumes of distillate and residue obtained over specified temperature

ranges are measured. The residue from the distillation and also the distillate can be tested as required.

5 Apparatus
Usual laboratory apparatus and glassware, together with the following:

5.1 Distillation flask, 500 ml and with side-arm, of dimensions given in Figure 1.

5.2 Heating system. Equipment needed when using a gas burner or equivalent (see Figure 3).

5.2.1 Shield, of steel, lined with 3 mm of suitable thermal insulation material and fitted with

transparent mica windows of the form and dimensions shown in Figure 2, which is used to protect the

distillation flask from air currents and to reduce radiation.
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SIST EN 13358:2019
EN 13358:2019 (E)

5.2.2 Shield cover (top), consisting of two parts of fire resistant millboard of 6 mm minimum

thickness.

5.2.3 Support for shield and distillation flask, two sheets 150 mm × 150 mm of a mesh of

approximately 1 mm wire gauze on a tripod or ring.

5.2.4 Heat source, adjustable Tirrill gas burner or equivalent. It is advised to protect the gas burner

flame using a chimney, as shown in Figure 3.
5.2.5 Height adjustable platform, to support the gas burner.
5.3 Heating system. Equipment needed when using an electric heater.
5.3.1 Shield and shield cover, as described under 5.2.1 and 5.2.2.

5.3.2 Electric heater (replacing items 6, 7 and 8 in Figure 3), with a heating plate adequately surfaced

to support the distillation flask and designed so as to efficiently transfer the heat. The heating plate shall

be of sufficient dimensions to support the shield over its entire base. The heater shall be equipped with a

transformer capable of controlling from 0 W to 750 W.
5.3.3 Height adjustable platform, to support the electric heater.
5.4 Heating system. Equipment needed when using an electric heating mantle.

5.4.1 Electric heating mantle (replacing items 4, 6, 7 and 8 in Figure 3), of adequate inner size to fit

the 500 ml distillation flask and completely embed the 200 ml product sample once filled into the

distillation flask (see 6.3.1). The heating mantle shall be completed with a removable insulation collar to

cover the part of the distillation flask emerging from the heating mantle. The heating mantle shall be

equipped with a transformer capable of controlling from 0 W to 750 W.
5.4.2 Height adjustable platform, to support the electric heating mantle.

5.5 Condenser, standard glass-jacketed of nominal jacket length from 200 mm to 300 mm and overall

tube length of (450 ± 10) mm (see Figure 3).

5.6 Adapter, made with glass of approximately 1 mm thickness, with reinforced top, having an angle

of approximately 105°. The inside diameter shall be (18 ± 2) mm at the wide end and not less than 5 mm

at the narrow end. The lower surface of the adapter shall be on a smooth descending curve from the wider

end to the narrower. The inside line of the outlet end shall be vertical, and the outlet shall be cut or ground

(not
...

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