Hardmetals - Chemical analysis by flame atomic absorption spectrometry - Part 4: Determination of molybdenum, titanium and vanadium in contents from 0,01 to 0,5 % (m/m) (ISO 7627-4:1983)

General requirements concerning the field of application, principle, interfering elements,aparatus, sampling and test report are given in ISO 7627-1.

Hartmetalle - Chemische Analyse durch Flammenatomabsorptionsspektrometrie - Teil 4: Bestimmung des Molybdän-, Titan-, und Vanadiumgehaltes von 0,01 bis 0,5 % (m/m) (ISO 7627-4:1983)

Métaux-durs - Analyse chimique par spectrométrie d'absorption atomique dans la flamme - Partie 4: Dosages du molybdène, du titane et du vanadium à des teneurs comprises entre 0,01 et 0,5 % (m/m) (ISO 7627-4:1983)

La présente partie de l'ISO 7627 spécifie la méthode à utiliser pour le dosage par spectrométrie d'absorption atomique dans la flamme du molybdène, du titane et du vanadium dans les métaux-durs, à des teneurs en chacun de ces éléments comprises entre 0,01 et 0,05 % (m/m). Les prescriptions générales concernant le domaine d'application, le principe, les interférences, l'appareillage, l'échantillonnage et le procès-verbal d'essai figurent dans l'ISO 7627/1.

Hardmetals - Chemical analysis by flame atomic absorption spectrometry - Part 4: Determination of molybdenum, titanium and vanadium in contents from 0,01 to 0,5 % (m/m) (ISO 7627-4:1983)

General Information

Status
Published
Publication Date
06-Apr-1993
Withdrawal Date
30-Oct-1993
Current Stage
9093 - Decision to confirm - Review Enquiry
Start Date
13-Oct-1999
Completion Date
13-Oct-1999

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Hardmetals - Chemical analysis by flame atomic absorption spectrometry - Part 4: Determination of molybdenum, titanium and vanadium in contents from 0,01 to 0,5 % (m/m) (ISO 7627-4:1983)Hartmetalle - Chemische Analyse durch Flammenatomabsorptionsspektrometrie - Teil 4: Bestimmung des Molybdän-, Titan-, und Vanadiumgehaltes von 0,01 bis 0,5 % (m/m) (ISO 7627-4:1983)Métaux-durs - Analyse chimique par spectrométrie d'absorption atomique dans la flamme - Partie 4: Dosages du molybdene, du titane et du vanadium a des teneurs comprises entre 0,01 et 0,5 % (m/m) (ISO 7627-4:1983)Hardmetals - Chemical analysis by flame atomic absorption spectrometry - Part 4: Determination of molybdenum, titanium and vanadium in contents from 0,01 to 0,5 % (m/m) (ISO 7627-4:1983)77.160Metalurgija prahovPowder metallurgy77.040.30Kemijska analiza kovinChemical analysis of metalsICS:Ta slovenski standard je istoveten z:EN 27627-4:1993SIST EN 27627-4:2000en01-december-2000SIST EN 27627-4:2000SLOVENSKI
STANDARD



SIST EN 27627-4:2000



SIST EN 27627-4:2000



SIST EN 27627-4:2000



SIST EN 27627-4:2000



SIST EN 27627-4:2000



- International Standard 762714 INTERNATIONAL ORGANIZATION FOR STANDARDIZATION.MEX~YHAPOAHAR OPTAHM3AUMR fl0 CTAH~APTM3A~MM.ORGANlSATlON INTERNATIONALE DE NORMALISATION Hardmetals - Chemical analysis by flame’.atomic absorption spectrometry - Part 4: Determination of molybdenum, titanium and vanadium in contents from 0,Ol to 0,5 % (mlm) Mkaux-durs - Analyse cbimique par spectrometrie d’absorp tion a tomique dans Ia flamme - Partie 4: Dosage du mo/ybd&ne, du titane et du vanadium a des teneurs comprises entre Q,Ol et 0,5 % (mlm) First edition - 1983-10-15 UDC 669.018.25 : 643.422 . r .< ’ Ref. No. ISO 7627/4-1983 (EI SIST EN 27627-4:2000



Foreword ISO (the International Organization for Standardization) is a worldwide federation of national Standards bodies (ISO member bodies). The work of developing International Standards is carried out through ISO technical committees. Every member body interested in a subject for which a technical committee has been authorized has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take patt in the work. Draft International Standards adopted by the technical committees are circulated to the member bodiesfor approval before their acceptance as International Standards by the ISO Council. International Standard ISO 7627/4 was developed by Technical Committee ISO/TC 119, Powder metahrgy, and was circulated to the member bodies in August 1982. lt has been approved by the member bodies of the following countries: Austria Germany, F. R. Brazil Italy Bulgaria Korea, Rep. of China Norway Czechoslovakia Poland Egypt, Arab Rep. of Romania France South Africa, Rep. of Spain Sweden Switzerland United Kingdom USA USSR No member body expressed disapproval of the document. 0 International Organkation for Standardkation, 1983 0 Printed in Switzerland SIST EN 27627-4:2000



INTERNATIONAL STANDARD ISO 7627/4-1983 (E) Hardmetals - Chemical analysis by flame atomic absorption spectrometry - Part 4: Determination of molybdenum, titanium and vanadium in contents from 0,Ol to 0,5 % (mlm) . 1 Scope and field of application This part of ISO 7627 specifies the method to be used for the determination of molybdenum, titanium and vanadium con- tents of hardmetals within the range 0,Ol to 0,5 % (Nm) by flame atomic absorption spectrometry. General requirements concerning the fieid of application, prin- ciple, interfering elements, apparatus, sampling and test report are given in ISO 7627/1. 2 Reference ISO 762711, Hardmetals - Chemical analysis b y flame atomic absorp tion spectrometry - Part 7: General requirements. . 3 Reagents 3.1 Hydrofluoric acid, Q 1,12 g/ml. 3.2 Nitrit acid, Q 1,42 g/ml. 3.3 Ammonium fluoride, 0,l g/ml solution. 3.4 Caesium chloride, 0,Ol g/ml Solution. 3.5 High-purity stock solutions, for calibration purposes for each element to be determined, containing 1,600 g of the element per litre. NOTE - This value is understood to establish a maximum limit of 1,000 5 g and a minimum limit of 0,999 5 g. 4 Procedure 4.1 Test Portion Weigh, to the nearest 0,001 g, approximately 1 g of the test Sample. Transfer it to a 100 ml polytetrafluorethylene beaker or a beaker of other suitable material. Cover the beaker. 4.2 Dissolution of the test Portion Add 10 ml of water, 5 ml of the hydrofluoric acid (3.1). and then 5 ml of the nitric acid (3.21, drop by drop, to the beaker containing the test Portion (4.1) and heat gently until the test Portion is completely dissolved. Add 10 ml of the caesium chloride Solution (3.4) and 10 ml of the ammonium fluoride Solution (3.3). Then transfer the Solution totally to a 100 ml polypropylene one-mark volumetric flask and dilute to the mark. 4.3 Dilution volume Prepare
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