Determination of certain substances in electrotechnical products - Part 2: Disassembly, disjointment and mechanical sample preparation

IEC 62321-2:2013 provides strategies of sampling along with the mechanical preparation of samples from electrotechnical products, electronic assemblies and electronic components. These samples can be used for analytical testing to determine the levels of certain substances as described in the test methods in other parts of IEC 62321. Restrictions for substances will vary between geographic regions and from time to time. This Standard describes a generic process for obtaining and preparing samples prior to the determination of any substance which are under concern.

Verfahren zur Bestimmung von bestimmten Substanzen in Produkten der Elektrotechnik - Teil 2: Demontage, Zerlegung und mechanische Probenvorbereitung

Détermination de certaines substances dans les produits électrotechniques - Partie 2: Démontage, désassemblage et préparation mécanique de l'échantillon

La CEI 62321-2:2013 fournit des stratégies d'échantillonnage ainsi que la préparation mécanique d'échantillons de produits électrotechniques, ensembles électroniques et composants électroniques. Ces échantillons peuvent être utilisés pour un essai analytique visant à déterminer les niveaux de certaines substances, comme décrit dans les méthodes d'essai des autres parties de la CEI 62321. Les restrictions concernant les substances varient selon les régions géographiques et de temps à autres. La présente norme décrit un processus général permettant d'obtenir et de préparer des échantillons avant de déterminer toute substance posant problème.

Določevanje posameznih snovi v elektrotehničnih izdelkih - 2. del: Razstavljanje, odklop in mehanska priprava vzorca (IEC 62321-2:2013)

Standard 62321-2 določa strategije vzorčenja skupaj z mehansko pripravo vzorcev iz elektrotehničnih izdelkov, elektronskih sklopov in elektronskih komponent. Ti vzorci se lahko uporabijo za analitično testiranje za določitev vsebnosti nekaterih snovi, kot je opisano v testnih metodah v drugih delih IEC 62321. Omejitve za snovi se razlikujejo med geografskimi regijami in od časa do časa. Ta standard opisuje splošen postopek za pridobitev in pripravo vzorcev pred določitvijo katere koli zadevne snovi. Ta standard ne ponuja: - popolnih smernic za vsak izdelek, ki ga je mogoče razvrstiti kot elektrotehnično opremo. Ker hkrati z nenehnimi industrijskimi inovacijami obstaja veliko različnih elektrotehničnih komponent z različnimi zgradbami in postopki, je nerealno, da bi poskušali zagotoviti postopke za razstavljanje vsakega tipa sestavnega dela pri stikališčih; – smernice glede drugih poti za zbiranje dodatnih informacij o nekaterih snoveh v proizvodu, čeprav so zbrane informacije pomembne za strategije vzorčenja v tem standardu; – varno razstavljanje in navodila za mehansko razstavljanje pri stikališčih, povezana z elektrotehničnimi izdelki (npr. stikala, ki vsebujejo živo srebro) in reciklažno industrijo (npr. kako ravnati z zasloni CRT ali varno odstraniti baterije). Glejte standard IEC 62554 [2] za razstavljanje pri stikališčih in pripravo mehanskih vzorcev fluorescenčnih sijalk, ki vsebujejo živo srebro; – opredelitev »enote« kot vzorca; – postopke vzorčenja za embalažo in embalažne materiale; – analitične postopke za merjenje ravni določenih snovi. To je zajeto v drugih standardih (na primer drugih delih IEC 62321), ki so navedeni kot »preskusni standard« v tem standardu; – smernice za oceno skladnosti.

General Information

Status
Published
Publication Date
24-Apr-2014
Withdrawal Date
14-Nov-2016
Current Stage
6060 - Document made available - Publishing
Start Date
25-Apr-2014
Completion Date
25-Apr-2014

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SLOVENSKI STANDARD
01-junij-2014
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SIST EN 62321:2009
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Determination of certain substances in electrotechnical products - Part 2: Disassembly,
disjunction and mechanical sample preparation
Verfahren zur Bestimmung von bestimmten Substanzen in Produkten der Elektrotechnik
- Teil 2: Demontage, Zerlegung und mechanische Probenvorbereitung
Détermination de certaines substances dans les produits électrotechniques - Partie 2:
Démontage, désassemblage et préparation mécanique de l'échantillon
Ta slovenski standard je istoveten z: EN 62321-2:2014
ICS:
29.020 Elektrotehnika na splošno Electrical engineering in
general
31.020 Elektronske komponente na Electronic components in
splošno general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EUROPEAN STANDARD
EN 62321-2
NORME EUROPÉENNE
April 2014
EUROPÄISCHE NORM
ICS 13.020; 43.040.10 Supersedes EN 62321:2009 (partially)

English version
Determination of certain substances in electrotechnical products -
Part 2: Disassembly, disjointment and mechanical sample preparation
(IEC 62321-2:2013)
Détermination de certaines substances Verfahren zur Bestimmung von
dans les produits électrotechniques - bestimmten Substanzen in Produkten der
Partie 2: Démontage, désassemblage et Elektrotechnik -
préparation mécanique de l'échantillon Teil 2: Demontage, Zerlegung und
(CEI 62321-2:2013) mechanische Probenvorbereitung
(IEC 62321-2:2013)
This European Standard was approved by CENELEC on 2013-11-15. CENELEC members are bound to comply
with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard
the status of a national standard without any alteration.

Up-to-date lists and bibliographical references concerning such national standards may be obtained on
application to the CEN-CENELEC Management Centre or to any CENELEC member.

This European Standard exists in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CENELEC member into its own language and notified
to the CEN-CENELEC Management Centre has the same status as the official versions.

CENELEC members are the national electrotechnical committees of Austria, Belgium, Bulgaria, Croatia, Cyprus,
the Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany,
Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, the Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.

CENELEC
European Committee for Electrotechnical Standardization
Comité Européen de Normalisation Electrotechnique
Europäisches Komitee für Elektrotechnische Normung

CEN-CENELEC Management Centre: Avenue Marnix 17, B - 1000 Brussels

© 2014 CENELEC - All rights of exploitation in any form and by any means reserved worldwide for CENELEC members.
Ref. No. EN 62321-2:2014 E
Foreword
The text of document 111/301/FDIS, future edition 1 of IEC 62321-2, prepared by IEC/TC 111
"Environmental standardization for electrical and electronic products and systems" was submitted to the
IEC-CENELEC parallel vote and approved by CENELEC as EN 62321-2:2014.
The following dates are fixed:
(dop) 2014-10-25
• latest date by which the document has
to be implemented at national level by
publication of an identical national
standard or by endorsement
(dow) 2016-11-15
• latest date by which the national
standards conflicting with the

document have to be withdrawn
1)
replacing Clause 5 and incorporating IEC/PAS 62596:2009 [1] which will be withdrawn upon publication
of IEC 62321-2.
Future parts in the EN 62321 series will gradually replace the corresponding clauses in EN 62321:2009.
Until such time as all parts are published, however, EN 62321:2009 remains valid for those clauses not
yet re-published as a separate part.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CENELEC [and/or CEN] shall not be held responsible for identifying any or all such patent
rights.
Endorsement notice
The text of the International Standard IEC 62321-2:2013 was approved by CENELEC as a European
Standard without any modification.
In the official version, for Bibliography, the following notes have to be added for the standards indicated:
IEC 62554 NOTE Harmonised as EN 62554 (not modified).
IEC 62542 NOTE Harmonised as EN 62542 (not modified).
IEC 62321-6 NOTE Harmonised as EN 62321-6 (not modified).
IEC 62321-7-1 NOTE Harmonised as EN 62321-7-1 (not modified).
IEC 62137-1-2 NOTE Harmonised as EN 62137-1-2 (not modified).

1)
Numbers in square brackets refer to the Bibliography.

- 3 - EN 62321-2:2014
Annex ZA
(normative)
Normative references to international publications
with their corresponding European publications

The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.

NOTE  When an international publication has been modified by common modifications, indicated by (mod), the relevant EN/HD
applies.
Publication Year Title EN/HD Year

IEC 62321-1 - Determination of certain substances in EN 62321-1 -
electrotechnical products - Part 1: Introduction
and overview
IEC 62321-3-1 - Determination of certain substances in EN 62321-3-1 -
electrotechnical products - Part 3-1: Screening
electrotechnical products for lead, mercury,
cadmium, total chromium and total bromine
using X-ray Fluorescence Spectrometry

IEC 62321-3-2 - Determination of certain substances in EN 62321-3-2 -
electrotechnical products - Part 3-2: Screening
of total bromine in electric and electronic
products by combustion-ion chromatography
(C-IC)
IEC 62321-4 - Determination of certain substances in EN 62321-4 -
electrotechnical products - Part 4:
Determination of mercury in polymers, metals
and electronics by CV-AAS, CV-AFS, ICP-
OES and ICP-MS
IEC 62321-5 - Determination of certain substances in EN 62321-5 -
electrotechnical products - Part 5:
Determination of cadmium, lead and
chromium in polymers and electronics, and
cadmium and lead in metals by AAS, AFS,
ICP-OES and ICP-MS
IEC 62321-2 ®
Edition 1.0 2013-06
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
colour
inside
Determination of certain substances in electrotechnical products –

Part 2: Disassembly, disjointment and mechanical sample preparation

Détermination de certaines substances dans les produits électrotechniques –

Partie 2: Démontage, désassemblage et préparation mécanique de l'échantillon

INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
COMMISSION
ELECTROTECHNIQUE
PRICE CODE
INTERNATIONALE
CODE PRIX XB
ICS 13.020; 43.040.10 ISBN 978-2-83220-837-3

– 2 – 62321-2 © IEC:2013
CONTENTS
FOREWORD . 4
INTRODUCTION . 6
1 Scope . 7
2 Normative references . 7
3 Terms, definitions and abbreviations . 8
3.1 Terms and definitions . 8
3.2 Abbreviations . 8
4 Introduction to sampling . 9
4.1 Introductory remark . 9
4.2 Requirements and concerns for substances of concern . 9
4.3 Complexity of electrotechnical products and related challenges. 9
4.4 Strategies for sampling . 10
5 Sampling . 13
5.1 Introductory remark . 13
5.2 Complete product . 14
5.3 Partial disassembly . 14
5.4 Complete disassembly . 14
5.5 Partial disjointment . 14
5.6 Complete disjointment . 15
5.7 Considerations of sampling and disjointment . 15
5.7.1 Introductory remark . 15
5.7.2 Sample size required . 15
5.7.3 Sample size versus detection limit . 17
5.7.4 Composite testing of disjointable samples . 17
5.7.5 Non-uniform “homogeneous materials” . 18
5.7.6 Determination of sampling position of homogeneous materials . 19
6 Conclusions and recommendations for sampling . 19
7 Mechanical sample preparation . 20
7.1 Overview . 20
7.1.1 Field of application . 20
7.1.2 Quality assurance . 20
7.2 Apparatus, equipment and materials. 21
7.3 Procedure . 21
7.3.1 Manual cutting . 21
7.3.2 Coarse grinding/milling . 22
7.3.3 Homogenizing. 22
7.3.4 Fine grinding/milling . 22
7.3.5 Very fine grinding of polymers and organic materials . 22
Annex A (informative) Examples of procedures for sampling and disjointment . 23
Annex B (informative) Probability of the presence of certain substances . 32
Annex C (informative) Composite testing and sampling . 35
Annex D (informative) Tools used in sampling. 38
Annex E (informative) Examples of mobile phone disassembly and component
disjointment . 39
Bibliography . 50

62321-2 © IEC:2013 – 3 –
Figure 1 – Generic iterative procedure for sampling . 11
Figure 2 – Cross-section of a 900 µm wide lead oxide-based resistor (SMD) . 19
Figure A.1 – Methodology for sampling and disjointment . 24
Figure A.2 – Sampling of DVD player . 25
Figure A.3 – Sampling of CRT . 26
Figure A.4 – Sampling of LCD TV . 27
Figure A.5 – Sampling of PDA/phone . 28
Figure A.6 – Sampling of desk fan . 29
Figure A.7 – Sampling of components – Thick film resis
...

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