ISO 16129:2018

Surface chemical analysis — X-ray photoelectron spectroscopy — Procedures for assessing the day-to-day performance of an X-ray photoelectron spectrometer

This document is designed to allow the user to assess, on a regular basis, several key parameters of an X‑ray photoelectron spectrometer. It is not intended to provide an exhaustive performance check, but instead provides a rapid set of tests that can be conducted frequently. Aspects of instrument behaviour covered by this document include the vacuum, measurements of spectra of conductive or non-conductive test specimens and the current state of the X‑ray source. Other important aspects of the instrument performance (e.g. lateral resolution) fall outside the scope of this document. The document is intended for use with commercial X‑ray photoelectron spectrometers equipped with a monochromated Al Kα X‑ray source or with an unmonochromated Al or Mg Kα X‑ray source.

Analyse chimique des surfaces — Spectroscopie de photoélectrons X — Modes opératoires d'évaluation de la performance au jour le jour d'un spectromètre de photoélectrons X

General Information

• Status: Published
• Publication Date: 14-Nov-2018
• ICS: 71.040.40 - Chemical analysis
• Technical Committee: ISO/TC 201/SC 7 - Electron spectroscopies
• Drafting Committee: ISO/TC 201/SC 7/WG 2 - Quantification and interpretation of data in electron spectroscopy
• Current Stage: 9060 - Close of review
• Start Date: 04-Jun-2029

Relations

• Consolidated By: ISO/FDIS 26101-2 - Acoustics — Test methods for the qualification of the acoustic environment — Part 2: Determination of the environmental correction
• Effective Date: 06-Jun-2022
• Revises: ISO 16129:2012 - Surface chemical analysis — X-ray photoelectron spectroscopy — Procedures for assessing the day-to-day performance of an X-ray photoelectron spectrometer
• Effective Date: 28-Oct-2017

Standards Content (Sample)

INTERNATIONAL ISO
STANDARD 16129
Second edition
2018-11
Surface chemical analysis — X-ray
photoelectron spectroscopy —
Procedures for assessing the day-
to-day performance of an X-ray
photoelectron spectrometer
Analyse chimique des surfaces — Spectroscopie de photoélectrons X
— Modes opératoires d'évaluation de la performance au jour le jour
d'un spectromètre de photoélectrons X
Reference number
ISO 16129:2018(E)
©
ISO 2018

---------------------- Page: 1 ----------------------
ISO 16129:2018(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Website: www.iso.org
Published in Switzerland
ii © ISO 2018 – All rights reserved

---------------------- Page: 2 ----------------------
ISO 16129:2018(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms, definitions and abbreviations . 1
4 Initial approach . 1
5 Initial instrument calibration, alignment and assessment . 2
6 Test specimen selection . 2
6.1 General information . 2
6.2 The conductive specimen . 3
6.3 The non-conductive specimen . 3
6.4 Specimen for assessing the X-ray source . 4
7 Collection of reference data . 5
7.1 General information . 5
7.2 Rapid test of the instrument using a conductive specimen . 5
7.2.1 Specimen mounting and pre-treatment . 5
7.2.2 Survey spectrum . 5
7.2.3 High-resolution spectrum . 7
7.3 Rapid test of the instrument using a non-conductive specimen . 8
7.3.1 Specimen mounting and positioning .
...