ISO 15471:2016

Surface chemical analysis — Auger electron spectroscopy — Description of selected instrumental performance parameters

ISO 15471:2016 specifies the requirements for the description of specific aspects of the performance of an Auger electron spectrometer.

Analyse chimique des surfaces — Spectroscopie d'électrons Auger — Description de certains paramètres relatifs à la performance instrumentale

General Information

• Status: Published
• Publication Date: 04-Sep-2016
• ICS: 71.040.40 - Chemical analysis
• Technical Committee: ISO/TC 201/SC 7 - Electron spectroscopies
• Drafting Committee: ISO/TC 201/SC 7 - Electron spectroscopies
• Current Stage: 9093 - International Standard confirmed
• Completion Date: 10-Dec-2021

Relations

• Revises: ISO 15471:2004 - Surface chemical analysis — Auger electron spectroscopy — Description of selected instrumental performance parameters
• Effective Date: 09-Apr-2016

Standards Content (Sample)

INTERNATIONAL ISO
STANDARD 15471
Second edition
2016-09-01
Surface chemical analysis — Auger
electron spectroscopy — Description
of selected instrumental performance
parameters
Analyse chimique des surfaces — Spectroscopie d’électrons Auger
— Description de certains paramètres relatifs à la performance
instrumentale
Reference number
ISO 15471:2016(E)
©
ISO 2016

---------------------- Page: 1 ----------------------
ISO 15471:2016(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2016, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. [phone]
Fax [phone]
[e-mail]
www.iso.org
ii © ISO 2016 – All rights reserved

---------------------- Page: 2 ----------------------
ISO 15471:2016(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols and abbreviated terms . 1
5 Description of selected instrumental performance parameters . 1
5.1 Method of analysis . 1
5.2 Samples . 2
5.3 System configuration . 2
5.4 Electron gun cathode . 2
5.4.1 Cathode type . 2
5.4.2 Cathode lifetime . 2
5.5 Lateral resolution and beam current . 2
5.5.1 General. 2
5.5.2 Method 1 . 2
5.5.3 Method 2 . 3
5.5.4 Method 3 . 3
5.6 Spectrometer intensity performance and energy resolution . 3
5.6.1 General. 3
5.6.2 Method 1 . 3
5.6.3 Method 2 . 4
5.7 Spectrometer energy scale . 4
5.8 Spectrometer intensity linearity. 4
5.9 Spectrometer response function . 4
5.10 Spectrometer parameters . . 4
5.10.1 Spectrometer aberration . 4
5.10.2 Analytical area . 4
5.11 Image drift . 4
5.12 Vacuum environment . 4
Bibliography . 5
© ISO 2016 – All rights reserved iii

---------------------- Page: 3 ----------------------
ISO 15471:2016(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment,
as well as information about ISO’s adherence to the World Trade Organization (WTO) principles in the
Technical Barriers to Trade (TBT) see the following URL: www.iso.org/iso/foreword.html.
The committee responsible for this document is ISO/TC 201, Surface chemical analysis, Subcommittee
SC 7, Electron spectroscopies.
This second edition cancels and replaces the first edition (ISO 15471:2004), of which it constitutes a
minor revision with the following modifications:
— addition of a Bibliography;
— minor editorial changes to the text.
iv © ISO 2016 – All rights reserved

---------------------- Page: 4 ----------------------
ISO 15471:2016(E)

Introduction
Auger electron spectrometers (AESs) and scanning Auger electron microscopes (SAMs) are produced
by many manufacturers throughout the world. While the basic principles of the AES analytical method
in each instrument are the same, the specific designs of the instruments and the way that performance
specifications are provided differ widely. As a result, it is often difficult to compare the performance
of instruments from one manufacturer with those from another. This International Standard provides
a basic list of items devised to enable all Auger electron spectrometers to be described in a common
manner. This International Standard is not intended to replace the manufacturer’s specification,
which may extend to 30 or more pages. It is intended that, where certain items are contained in that
specification, there are agreed and defined meanings to those items.
© ISO 2016 – All rights reserved v

---------------------- Page: 5 ----------------------
INTERNATIONAL STANDARD ISO 15471:2016(E)
Surface chemical analysis — Auger electron spectroscopy
— Description of selected instrumental performance
parameters
1 Scope
This International Standard specifies the requirements for the description of specific aspects of the
performance of an Auger electron spectrometer.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
ISO 18115-1, Surface chemical analysis — Vocabulary — Part 1: General terms and terms used in
spectroscopy
3 Terms and definitions
For the purposes of this document, the terms
...

FINAL
INTERNATIONAL ISO/FDIS
DRAFT
STANDARD 15471
ISO/TC 201/SC 7
Surface chemical analysis — Auger
Secretariat: BSI
electron spectroscopy — Description
Voting begins on:
2016­05-16 of selected instrumental performance
parameters
Voting terminates on:
2016­07-11
Analyse chimique des surfaces — Spectroscopie d’électrons Auger
— Description de certains paramètres relatifs à la performance
instrumentale
RECIPIENTS OF THIS DRAFT ARE INVITED TO
SUBMIT, WITH THEIR COMMENTS, NOTIFICATION
OF ANY RELEVANT PATENT RIGHTS OF WHICH
THEY ARE AWARE AND TO PROVIDE SUPPOR TING
DOCUMENTATION.
IN ADDITION TO THEIR EVALUATION AS
Reference number
BEING ACCEPTABLE FOR INDUSTRIAL, TECHNO­
ISO/FDIS 15471:2016(E)
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN­
DARDS TO WHICH REFERENCE MAY BE MADE IN
©
NATIONAL REGULATIONS. ISO 2016

---------------------- Page: 1 ----------------------
ISO/FDIS 15471:2016(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2016, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH­1214 Vernier, Geneva, Switzerland
Tel. [phone]
Fax [phone]
[e-mail]
www.iso.org
ii © ISO 2016 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/FDIS 15471:2016(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols and abbreviated terms . 1
5 Description of selected instrumental performance parameters . 1
5.1 Method of analysis . 1
5.2 Samples . 2
5.3 System configuration . 2
5.4 Electron gun cathode . 2
5.4.1 Cathode type . 2
5.4.2 Cathode lifetime . 2
5.5 Lateral resolution and beam current . 2
5.5.1 General. 2
5.5.2 Method 1 . 2
5.5.3 Method 2 . 3
5.5.4 Method 3 . 3
5.6 Spectrometer intensity performance and energy resolution . 3
5.6.1 General. 3
5.6.2 Method 1 . 3
5.6.3 Method 2 . 4
5.7 Spectrometer energy scale . 4
5.8 Spectrometer intensity linearity. 4
5.9 Spectrometer response function . 4
5.10 Spectrometer parameters . . 4
5.10.1 Spectrometer aberration . 4
5.10.2 Analytical area . 4
5.11 Image drift . 4
5.12 Vacuum environment . 4
Bibliography . 5
© ISO 2016 – All rights reserved iii

---------------------- Page: 3 ----------------------
ISO/FDIS 15471:2016(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non­governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment,
as well as information about ISO’s adherence to the World Trade Organization (WTO) principles in the
Technical Barriers to Trade (TBT) see the following URL: www.iso.org/iso/foreword.html.
The committee responsible for this document is ISO/TC 201, Surface chemical analysis, Subcommittee
SC 7, Electron spectroscopies.
This second edition cancels and replaces the first edition (ISO 1571:2004), of which it constitutes a
minor revision with the following modifications:
— addition of a Bibliography;
— minor editorial changes to the text.
iv © ISO 2016 – All rights reserved

---------------------- Page: 4 ----------------------
ISO/FDIS 15471:2016(E)

Introduction
Auger electron spectrometers (AESs) and scanning Auger electron microscopes (SAMs) are produced
by many manufacturers throughout the world. While the basic principles of the AES analytical method
in each instrument are the same, the specific designs of the instruments and the way that performance
specifications are provided differ widely. As a result, it is often difficult to compare the performance
of instruments from one manufacturer with those from another. This International Standard provides
a basic list of items devised to enable all Auger electron spectrometers to be described in a common
manner. This International Standard is not intended to replace the manufacturer’s specification,
which may extend to 30 or more pages. It is intended that, where certain items are contained in that
specification, there are agreed and defined meanings to those items.
© ISO 2016 – All rights reserved v

---------------------- Page: 5 ----------------------
FINAL DRAFT INTERNATIONAL STANDARD ISO/FDIS 15471:2016(E)
Surface chemical analysis — Auger electron spectroscopy
— Description of selected instrumental performance
parameters
1 Scope
This International Standard specifies the requirements for the description of specific aspects of the
performance of an Auger electron spectrometer.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited ap
...