ISO/TS 13907:2012

Soil quality — Determination of nonylphenols (NP) and nonylphenol-mono- and diethoxylates — Method by gas chromatography with mass selective detection (GC-MS)

ISO/TS 13907:2012 specifies a method for the determination of nonylphenols (NP), nonylphenol-monoethoxylates (NP1EO) and nonylphenol-diethoxylates (NP2EO) in sludge, treated biowaste and soil using GC-MS. For sludge, a limit of detection of 0,1 mg/kg and for soil and treated biowaste of 0,02 mg/kg (expressed as dry matter) may be achieved.

Qualité du sol — Détermination des nonyphénols (NP) et des mono- et di-éthoxylates de nonylphénol — Méthode par chromatographie en phase gazeuse avec détection sélective de masse (CPG-SM)

General Information

• Status: Published
• Publication Date: 29-Aug-2012
• ICS: 13.080.10 - Chemical characteristics of soils
• Technical Committee: ISO/TC 190/SC 3 - Chemical and physical characterization
• Drafting Committee: ISO/TC 190/SC 3/WG 6 - Organic analysis
• Current Stage: 9093 - International Standard confirmed
• Completion Date: 16-Feb-2024

Standards Content (Sample)

TECHNICAL ISO/TS
SPECIFICATION 13907
First edition
2012-09-01
Soil quality — Determination of
nonylphenols (NP) and nonylphenol-
mono- and diethoxylates — Method
by gas chromatography with mass
selective detection (GC-MS)
Qualité du sol — Détermination des nonyphénols (NP) et des mono- et
di-éthoxylates de nonylphénol — Méthode par chromatographie en
phase gazeuse avec détection sélective de masse (CPG-SM)
Reference number
ISO/TS 13907:2012(E)
©
ISO 2012

---------------------- Page: 1 ----------------------
ISO/TS 13907:2012(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2012
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any
means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the
address below or ISO’s member body in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail [e-mail]
Web www.iso.org
Published in Switzerland
ii © ISO 2012 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/TS 13907:2012(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Principle . 1
4 Interferences . 2
4.1 Interferences from sampling. 2
4.2 Interferences by GC-MS . 2
5 Reagents . 2
6 Apparatus . 4
7 Sample storage and sample pretreatment . 5
7.1 Sample storage . 5
7.2 Sample pretreatment . 5
8 Procedure. 5
8.1 Extraction . 5
8.2 Concentration (optional). 7
8.3 Clean-up (optional) . 7
8.4 Derivatization .
...