SIST EN ISO 17402:2011
(Main)Soil quality - Requirements and guidance for the selection and application of methods for the assessment of bioavailability of contaminants in soil and soil materials (ISO 17402:2008)
Soil quality - Requirements and guidance for the selection and application of methods for the assessment of bioavailability of contaminants in soil and soil materials (ISO 17402:2008)
This International Standard provides guidance for the selection and application of methods to assess bioavailability for the characterisation of contaminated soil and soil materials. This International Standard does not give a selection of the best applicable methods, but specifies boundary conditions and principles of methods to be used and gives the minimal requirements for the development of methods. The results obtained from such methods can be used as an estimate of bioavailability in a risk-assessment approach. In this International Standard, when the term “soil” is only quoted for simplification, the broader term “soil and soil material” shall be considered. The contaminants considered in this International Standard are metals, including metalloids, and organic contaminants, including organometal compounds. This International Standard is also applicable to metals originating from natural geological and pedological processes (natural pedo-geochemical content). This International Standard can also be applied to sediments.
Bodenbeschaffenheit - Anleitung zur Auswahl und Anwendung von Verfahren für die Bewertung der Bioverfügbarkeit von Kontaminanten im Boden und in Bodenmaterialien (ISO 17402:2008)
Diese Internationale Norm gibt eine Anleitung zur Auswahl und Anwendung von Verfahren zur Bewertung der
Bioverfügbarkeit für die Charakterisierung von verunreinigtem Boden und Bodenmaterial. Diese Internationale
Norm bietet keine Auswahl der besten anwendbaren Verfahren, legt jedoch Randbedingungen und
Grundsätze von anzuwendenden Verfahren fest und führt die Mindestanforderungen an die Entwicklung von
Verfahren an. Die nach derartigen Verfahren erhaltenen Ergebnisse können als Schätzwert für die
Bioverfügbarkeit bei einem auf die Gefährdungsabschätzung bezogenen Ansatz verwendet werden.
Wenn in dieser Internationalen Norm nur der Begriff „Boden“ zur Vereinfachung der Schreibweise angegeben
wird, muss der erweiterte Begriff „Boden und Bodenmaterialien“ in Betracht kommen.
Die in dieser Internationalen Norm berücksichtigten Kontaminanten sind Metalle, einschließlich metallartiger
und organischer Kontaminanten, einschließlich metallorganischer Verbindungen. Diese Internationale Norm
gilt auch für Metalle, die aus natürlichen geologischen und pedologischen Prozessen (natürlicher
pedogeochemischer Gehalt) stammen.
Diese Internationale Norm kann auch für Sedimente angewendet werden.
ANMERKUNG 1 Ein Bewertungsverfahren auf der Grundlage des bioverfügbaren Anteils der Gesamtmenge von
Kontaminanten im Boden oder Bodenmaterial kann zur Entwicklung von gesetzlichen Anforderungen an risikobezogene
Bewertungsverfahren für Böden beitragen.
ANMERKUNG 2 In Übereinstimmung mit den angestrebten Schutzzielen werden Anwendungen bestehender Verfahren
empfohlen und deren Beschränkungen erörtert, um die Entwicklung und Einführung von ausführbaren genormten
Verfahren zu fördern, die bei der Boden- und Standortbewertung anzuwenden sind. Diese Verfahren sind notwendig, um
die quantitative Bestimmung von Faktoren zu ermöglichen, die die Bioverfügbarkeit beeinflussen.
Qualité du sol - Lignes directrices pour la sélection et l'application des méthodes d'évaluation de la biodisponibilité des contaminants dans le sol et les matériaux du sol (ISO 17402:2008)
L'ISO 17402:2008 donne des lignes directrices pour la sélection et l'application des méthodes permettant d'évaluer la biodisponibilité pour la caractérisation du sol et des matériaux du sol contaminés. L'ISO 17402:2008 ne fournit pas une sélection des meilleures méthodes applicables, mais spécifie les principes et les conditions limites des méthodes à utiliser et indique les exigences minimales relatives au développement de méthodes. Les résultats obtenus à partir de telles méthodes peuvent être utilisés en tant qu'estimation de la biodisponibilité dans une approche d'évaluation du risque.
Les contaminants considérés dans l'ISO 17402:2008 sont les métaux, y compris les métalloïdes et les contaminants organiques, notamment les composés organométalliques. La présente Norme internationale s'applique également aux métaux issus de processus géologiques et pédologiques naturels (teneur pédogéochimique naturelle).
L'ISO 17402:2008 peut également s'appliquer aux sédiments.
Kakovost tal - Zahteve in navodilo za izbiro in uporabo metod za ocenjevanje biološke razpoložljivosti onesnaževal v tleh in talnih (zemeljskih) materialih (ISO 17402:2008)
Ta mednarodni standard podaja navodilo za izbiro in uporabo metod za ocenjevanje biološke razpoložljivosti za karakterizacijo onesnaženih tal in talnih (zemeljskih) materialov. Ta mednarodni standard ne navaja izbire najboljše metode, določa pa mejne pogoje in načela uporabljenih metod ter podaja minimalne zahteve za razvoj metod. Rezultati, dobljeni s takimi metodami, se lahko uporabijo kot ocena biološke razpoložljivosti pri pristopu ocenjevanja tveganja. Kjer je v tem mednarodnem standardu zaradi nezapletenosti uporabljen izraz »tla«, je mišljen širši izraz »tla in talni (zemeljski) materiali«. Onesnaževala, obravnavana v tem mednarodnem standardu, so kovine, vključno z metaloidi, in organska onesnaževala, vključno z organokovinskimi spojinami. Ta mednarodni standard velja tudi za kovine, ki izvirajo iz naravnih geoloških in pedoloških procesov (naravna pedogeokemijska vsebnost). Ta mednarodni standard se lahko uporablja tudi za sedimente.
General Information
Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Kakovost tal - Zahteve in navodilo za izbiro in uporabo metod za ocenjevanje biološke razpoložljivosti onesnaževal v tleh in talnih (zemeljskih) materialih (ISO 17402:2008)Bodenbeschaffenheit - Anleitung zur Auswahl und Anwendung von Verfahren für die Bewertung der Bioverfügbarkeit von Kontaminanten im Boden und in Bodenmaterialien (ISO 17402:2008)Qualité du sol - Lignes directrices pour la sélection et l'application des méthodes d'évaluation de la biodisponibilité des contaminants dans le sol et les matériaux du sol (ISO 17402:2008)Soil quality - Requirements and guidance for the selection and application of methods for the assessment of bioavailability of contaminants in soil and soil materials (ISO 17402:2008)13.080.05Preiskava tal na splošnoExamination of soils in generalICS:Ta slovenski standard je istoveten z:EN ISO 17402:2011SIST EN ISO 17402:2011en,fr,de01-november-2011SIST EN ISO 17402:2011SLOVENSKI
STANDARD
SIST EN ISO 17402:2011
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN ISO 17402
June 2011 ICS 13.080.01 English Version
Soil quality - Requirements and guidance for the selection and application of methods for the assessment of bioavailability of contaminants in soil and soil materials (ISO 17402:2008)
Qualité du sol - Lignes directrices pour la sélection et l'application des méthodes d'évaluation de la biodisponibilité des contaminants dans le sol et les matériaux du sol (ISO 17402:2008)
Bodenbeschaffenheit - Anleitung zur Auswahl und Anwendung von Verfahren für die Bewertung der Bioverfügbarkeit von Kontaminanten im Boden und in Bodenmaterialien (ISO 17402:2008) This European Standard was approved by CEN on 10 June 2011.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 17402:2011: ESIST EN ISO 17402:2011
EN ISO 17402:2011 (E) 2 Contents Page Foreword .3 SIST EN ISO 17402:2011
EN ISO 17402:2011 (E) 3 Foreword The text of ISO 17402:2008 has been prepared by Technical Committee ISO/TC 190 “Soil quality” of the International Organization for Standardization (ISO) and has been taken over as EN ISO 17402:2011 by Technical Committee CEN/TC 345 “Characterization of soils” the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by December 2011, and conflicting national standards shall be withdrawn at the latest by December 2011. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 17402:2008 has been approved by CEN as a EN ISO 17402:2011 without any modification.
SIST EN ISO 17402:2011
SIST EN ISO 17402:2011
Reference numberISO 17402:2008(E)© ISO 2008
INTERNATIONAL STANDARD ISO17402First edition2008-06-15Soil quality — Requirements and guidance for the selection and application of methods for the assessment of bioavailability of contaminants in soil and soil materials Qualité du sol — Lignes directrices pour la sélection et l'application des méthodes d'évaluation de la biodisponibilité des contaminants dans le sol et les matériaux du sol
SIST EN ISO 17402:2011
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SIST EN ISO 17402:2011
ISO 17402:2008(E) © ISO 2008 – All rights reserved iii Contents Page Foreword.v Introduction.vi 1 Scope.1 2 Normative references.1 3 Terms and definitions.2 4 Bioavailability in relation to assessment of soil function.6 4.1 Soil functions and organisms to protect.6 4.2 Risk assessment.6 4.3 Protection goals.7 5 Concepts of bioavailability.8 5.1 Definitions.8 5.2 Links between bioavailability and biological effects and/or bioaccumulation.10 6 Description of methods to assess bioavailability.11 6.1 General.11 6.2 Assessment of bioavailability using chemical test methods.12 6.3 Assessment of bioavailability using ecotoxicological test methods.13 7 Pathways related to soil quality (both organism and soil).14 7.1 General.14 7.2 Human.14 7.2.1 General.14 7.2.2 Soil ingestion.14 7.2.3 Dermal contact.15 7.2.4 Inhalation of soil.15 7.2.5 Groundwater used for drinking water.15 7.3 Exposure of higher animals.15 7.4 Exposure of soil organisms.15 7.4.1 General.15 7.4.2 Exposure of soil micro-organisms.15 7.4.3 Exposure of soil invertebrates (micro-, meso- and macro-fauna).16 7.5 Exposure of plants.16 8 Available methods to measure bioavailability.17 8.1 General.17 8.2 Chemical methods to measure environmental availability.17 8.2.1 General.17 8.2.2 Methods for soil ingestion.18 8.2.3 Methods for dermal uptake.19 8.2.4 Methods for plants.19 8.2.5 Methods for leaching from the solid phase to the soil solution.19 8.2.6 Methods for biodegradation.20 8.2.7 Methods for soil organisms.20 8.2.8 Available and promising chemical methods to measure bioavailability.20 8.3 Ecotoxicological test methods to measure bioavailability.22 9 Requirements.25 9.1 General.25 9.2 Requirements for selection and application.25 9.2.1 Requirements for selection.25 9.2.2 Requirements for application.26 SIST EN ISO 17402:2011
ISO 17402:2008(E) iv © ISO 2008 – All rights reserved 9.3 Requirements for development.27 Annex A (informative)
Bioavailability in relation to biodegradability.29 Annex B (informative)
International Standards for the determination of the toxicity of chemicals on sediment organisms (laboratory tests).30 Bibliography.31
SIST EN ISO 17402:2011
ISO 17402:2008(E) © ISO 2008 – All rights reserved v Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 17402 was prepared by Technical Committee ISO/TC 190, Soil quality, Subcommittee SC 7, Soil and site assessment. SIST EN ISO 17402:2011
ISO 17402:2008(E) vi © ISO 2008 – All rights reserved Introduction Laboratory and field studies have demonstrated that biological effects are not related to the total concentration of a contaminant in the soil. Instead, an organism responds only to the fraction that is biologically available (bioavailable) for that organism. This is particularly true in soils that undergo interaction of contaminant molecules with the soil, in such a way that the contaminant is not attainable anymore by the organism or is present in a non-available form (sometimes referred to as sequestration or irreversible sorption). The bioavailable fractions of contaminants are dependent on soil properties and various processes varying with time and on the biological receptors. The conservative approach of exposure assessment, as typically described in a regulatory context, assumes that the total concentration of a contaminant present in a soil or soil material is available for uptake by organisms, including man, and as such will overestimate the risks. Therefore, a risk assessment can be optimised by using an approach that is based on estimated exposure representing the available, effective concentration of the contaminant(s) and on (existing) intrinsic toxicity data. This assumption is not new as, already in the last half of the nineteenth century, agronomists and soil scientists began to search for chemical methods to determine the concentration of individual plant-available nutrients in agricultural soils. The impetus for this search was the need for recommended nutrient additions to achieve maximum crop yield. Mulder [1] stated already in 1860: “The unnecessary full analysis of soil to learn if it is fertile or not cannot be argued enough. The long and short of it is availability, which cannot be derived beforehand. The analysis shows what there is, agriculture must draw its own conclusions from that.” Chemical methods were devised to reasonably predict the availability of inorganic ions necessary for plant development. Chemical partial extraction methods are now commonly used to evaluate available levels of nutrients in soils. Extraction methods have been optimised by correlating extraction results with response of susceptible crop species to the addition of fertilisers. The concept of availability is nowadays applied to the risk assessment of contaminants and can be tailored to the specific protection goals. Depending on the intended use of a soil or soil material, soil characterisation for different purposes (e.g. assessment of habitat and retention functions, risk assessment and compliance with regulatory values) may include chemical testing and ecotoxicological testing with selected representative test organisms. These tests will, in many cases, be soil- or site-specific at a given point in time, and cannot be extrapolated to other soils or points in time where other factors may control bioavailability. Bioavailability may be assessed in two complementary ways (see also Figure 1): ⎯ Chemical methods (e.g. extraction methods) which determine the fraction of a well-defined class of contaminants available for defined specific biotic receptors or the mobility of the contaminants in the soil. Usually these chemical methods were developed to predict the amount of contaminants taken up by the organisms. Nevertheless, these analytically determined values can also be correlated with effects. In a routine assessment of soil quality, chemical measurements may replace biological testing, if a correlation between the resulting chemical values and effect or accumulation has been demonstrated. ⎯ Biological methods which expose organisms to soil or soil eluates in order to monitor effects. If accumulation and/or effects (e.g. mortality, growth inhibition) are encountered, bioavailable contaminants are likely to be present even if they cannot be chemically identified. More knowledge on processes controlling bioavailability can close the still existing gap between chemical measurements and biological effects. SIST EN ISO 17402:2011
ISO 17402:2008(E) © ISO 2008 – All rights reserved vii
Figure 1 — Methods to assess bioavailability — Relation between chemical and biological assays and bioaccumulation Under regulatory aspects of soil protection, the risk assessment should be based upon the same common concept with regard to determination/assessment of exposure and measurement/assessment of effects. Thus, existing concepts and derived trigger values based on total concentrations of pollutants in soils or soil materials can be transferred to the proposed concept based on the prediction of the bioavailable fraction by using the more accurate description of exposure. For instance, the translation of information on bioavailability into acceptable evaluations of “how clean is clean” (e.g. site-specific limits for regulating the extent to which the remediation of soil is required) is essential for establishing realistic risk assessments and the determination of proper endpoints for remediation. A harmonised framework on bioavailability is considered in order to promote the development and introduction of workable standard methods to be used in soil and site assessment. In addition, methods for the estimation of bioavailable effective concentrations of contaminants according to the protection goals envisaged are required. These methods should preferably be described in International Standards and that standardization process should result in a limited set of established methods for the measurement of bioavailability [2]. As described in this International Standard, this process will not lead to one single method to measure bioavailability, because bioavailability depends on variables such as the contaminant, the target and the actual soil properties. Therefore, methods should not only use the word bioavailability but also refer to these variables (bioavailable for). In this International Standard, requirements and guidance are given to select methods to assess bioavailability for different target species with regard to several classes of contaminants. Methods to assess bioavailability are not described in this International Standard. Reference is made to existing International Standards and additional principles of measurement, which may need to be worked out in these International Standards. As only a few standards exist, reference is also made to measuring principles. Guidance is also provided for further standardization of a method where promising first results are reported. After a short description of methods (Clause 6), the pathways of a contaminant to the target organism are discussed (Clause 7). A summary of existing methods and promising methods that should be further developed is given in Clause 8. Clause 9 gives recommendations and includes the minimal requirements for application and further development.
SIST EN ISO 17402:2011
SIST EN ISO 17402:2011
INTERNATIONAL STANDARD ISO 17402:2008(E) © ISO 2008 – All rights reserved 1 Soil quality — Requirements and guidance for the selection and application of methods for the assessment of bioavailability of contaminants in soil and soil materials 1 Scope This International Standard provides guidance for the selection and application of methods to assess bioavailability for the characterisation of contaminated soil and soil materials. This International Standard does not give a selection of the best applicable methods, but specifies boundary conditions and principles of methods to be used and gives the minimal requirements for the development of methods. The results obtained from such methods can be used as an estimate of bioavailability in a risk-assessment approach. In this International Standard, when the term “soil” is only quoted for simplification, the broader term “soil and soil material” shall be considered. The contaminants considered in this International Standard are metals, including metalloids, and organic contaminants, including organometal compounds. This International Standard is also applicable to metals originating from natural geological and pedological processes (natural pedo-geochemical content). This International Standard can also be applied to sediments. NOTE An assessment procedure based on the bioavailable fraction of the total amount of contaminants in the soil or soil material can contribute to the development of regulatory requirements of risk-based assessment procedures for soils. According to the protection goals envisaged, applications of existing methods are recommended and their limitations discussed, with the intention of promoting the development and introduction of workable standard methods to be used in soil and site assessment. These methods are required to allow for the quantification of factors influencing bioavailability. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 11074:2005, Soil quality — Vocabulary ISO/TS 21268-1:2007, Soil quality — Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials — Part 1: Batch test using a liquid to solid ratio of 2 l/kg dry matter SIST EN ISO 17402:2011
ISO 17402:2008(E) 2 © ISO 2008 – All rights reserved 3 Terms and definitions For the purposes of this document, the terms and definitions given in ISO 11074 and the following apply. 3.1 bioavailability degree to which chemicals present in the soil may be taken up or metabolised by human or ecological receptors or are available for interaction with biological systems NOTE 1 Adapted from ISO 11074:2005. NOTE 2 The concept of bioavailability is further explained in Clause 5. NOTE 3 In ISO/TS 17924, a definition specific for human uptake through ingestion is given as the fraction of a substance present in ingested soil that reaches the systemic circulation (blood stream). 3.2 contaminant substance or agent present in the soil as a result of human activity [ISO 11074:2005] NOTE There is no assumption in this definition that harm results from the presence of the contaminant. 3.3 critical body residues CBR internal concentration accumulated in a tissue, organ or all of the body that is correlated with an adverse effect 3.4 environmental availability fraction of contaminant physico-chemically driven by desorption processes potentially available to organisms NOTE 1 See also Figure 2. NOTE 2 Environmental availability contains 1) an actual available fraction or the actual dissolved amount of pollutant at ambient conditions, or 2) a potentially available fraction, which is the maximum amount that can be released under (predefined) worst-case conditions. The potentially available fraction includes the actual available fraction. 3.5 environmental bioavailability fraction of the environmentally available compound which an organism takes up through physiologically driven processes NOTE See also Figure 2. 3.6 habitat function ability of soil/soil materials to serve as a habitat for micro-organisms, plants, soil-living animals and their interactions (biocenosis) [ISO 11074:2005] SIST EN ISO 17402:2011
ISO 17402:2008(E) © ISO 2008 – All rights reserved 3 3.7 leaching test test during which a material is put into contact with a leachant under strictly defined conditions and some constituents of the material are extracted [ISO/TS 21268-1:2007] 3.8 leachant liquid used in a leaching test [ISO/TS 21268-1:2007] 3.9 natural pedo-geochemical content concentration of a substance in soils, resulting from natural geological and pedological processes, excluding any addition of human origin [ISO 11074:2005] NOTE In the background content [concentration of a substance in soil, resulting from natural geological and pedological processes, including diffuse source inputs (ISO 19258)], the natural pedo-chemical content is combined with the content resulting from diffuse pollution. 3.10 pollutant substance or agent present in the soil (or groundwater), which due to its properties, amount or concentration causes adverse impacts on soil functions or soil use NOTE Adapted from ISO 11074:2005. 3.11 potentially harmful substance substance which, when present in a sufficient concentration or amount, may be harmful to humans or the environment NOTE It may be present as a result of human activity or naturally. 3.12 receptor potentially exposed person or part of ecosystem 3.13 retention function ability of soils/soil materials to adsorb pollutants in such a way that they cannot be mobilised via the water pathway and translocated into the terrestrial food chain [ISO 11074:2005] NOTE In this International Standard, reversible adsorption and desorption processes are also considered. 3.14 sediment or subhydric soil soil and its parent material beneath the surface water body SIST EN ISO 17402:2011
ISO 17402:2008(E) 4 © ISO 2008 – All rights reserved 3.15 soil upper layer of the Earth's crust composed of mineral particles, organic matter, water, air and living organisms NOTE 1 In a broader civil engineering sense soil includes top-soil and subsoils; deposits such as clays, silts, sands, gravels, cobbles, boulders and organic deposits such as peat; and materials of natural origin or of human origin (e.g. fills and deposited wastes). NOTE 2 Adapted from ISO 11074:2005. 3.16 soil material material coming from soil and displaced and/or modified by human activity, including excavated soil, dredged materials, manufactured soils, and treated soils and fill materials NOTE For the purposes of this International Standard, sediments are considered as soil material. 3.17 soil organisms all organisms living completely, or during specific parts of their lifetime, in the soil or on the soil surface (including the litter layer) and which contribute to soil processes (e.g. nutrient cycling), including plants (including soil algae), microflora, invertebrate and (a few) vertebrate species 3.18 toxicological bioavailability internal concentra
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