Animal and vegetable fats and oils - Determination of saponification value (ISO 3657:2023)

This document specifies a method for the determination of the saponification value of animal and vegetable fats and oils. The saponification value is a measure of the free and esterified acids present in fats and fatty acids.
The method is applicable to refined and crude vegetable and animal fats.
If mineral acids are present, the results given by this method are not interpretable unless the mineral acids are determined separately.
The saponification value can also be calculated from fatty acid data obtained by gas chromatography analysis as given in Annex B. For this calculation, it is necessary to be sure that the sample does not contain major impurities or is thermally degraded.

Tierische und pflanzliche Fette und Öle - Bestimmung der Verseifungszahl (ISO 3657:2023)

Dieses Dokument legt ein Verfahren zur Bestimmung der Verseifungszahl von tierischen und pflanzlichen Fetten und Ölen fest. Die Verseifungszahl ist ein Maß für die Menge an freien und veresterten Säuren, die in Fetten und Fettsäuren vorhanden sind.
Das Verfahren ist auf raffinierte und rohe pflanzliche und tierische Fette anwendbar.
Bei Vorhandensein von Mineralsäuren sind die nach diesem Verfahren erhaltenen Ergebnisse nicht auswertbar, es sei denn, die Mineralsäuren wurden getrennt bestimmt.
Die Verseifungszahl kann auch aus den Fettsäuredaten berechnet werden, die durch gaschromatographische Untersuchungen erhalten wurden, wie in Anhang B angegeben. Für diese Berechnung ist es notwendig, sich sicher zu sein, dass die Probe keine größeren Verunreinigungen enthält oder dass sie thermisch abgebaut wird.

Corps gras d'origines animale et végétale - Détermination de l'indice de saponification (ISO 3657:2023)

Le présent document spécifie une méthode de détermination de l'indice de saponification des corps gras d'origines animale et végétale. L'indice de saponification est une caractéristique des acides gras libres et estérifiés présents dans les corps gras et acides gras.
La méthode est applicable aux corps gras d'origines végétale et animale raffinés et bruts.
En présence d'acides minéraux, les résultats donnés par cette méthode ne sont plus interprétables si l'on ne dose pas séparément l'acidité minérale.
L'indice de saponification peut également être calculé à partir des données de composition en acides gras obtenues par chromatographie en phase gazeuse, selon l'Annexe B. Pour effectuer ce calcul, il est nécessaire de s'assurer que l'échantillon ne contient aucune impureté importante et qu'il n'est pas dégradé thermiquement.

Živalske in rastlinske maščobe ter olja - Določevanje števila umiljenja (ISO 3657:2023)

Ta dokument določa metodo za določevanje števila umiljenja živalskih in rastlinskih maščob ter olj. Umiljenje je meritev prostih in esterificiranih kislin, prisotnih v maščobah in maščobnih kislinah.
Metoda se uporablja za rafinirane in surove rastlinske in živalske maščobe.
Če so prisotne mineralne kisline, rezultatov, pridobljenih s to metodo, ni mogoče interpretirati, razen če se mineralne kisline določijo ločeno.
Umiljenje je mogoče izračunati tudi na podlagi podatkov o maščobnih kislinah, pridobljenih z analizo plinske kromatografije, kot je podana v Dodatku B. Za ta izračun je treba preveriti, da vzorec ne vsebuje večjih nečistoč in da ni termično razkrojen.

General Information

Status
Published
Public Enquiry End Date
10-Apr-2023
Publication Date
11-Sep-2023
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
01-Aug-2023
Due Date
06-Oct-2023
Completion Date
12-Sep-2023

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SLOVENSKI STANDARD
SIST EN ISO 3657:2023
01-oktober-2023
Nadomešča:
SIST EN ISO 3657:2020
Živalske in rastlinske maščobe ter olja - Določevanje števila umiljenja (ISO
3657:2023)
Animal and vegetable fats and oils - Determination of saponification value (ISO
3657:2023)
Tierische und pflanzliche Fette und Öle - Bestimmung der Verseifungszahl (ISO
3657:2023)
Corps gras d'origines animale et végétale - Détermination de l'indice de saponification
(ISO 3657:2023)
Ta slovenski standard je istoveten z: EN ISO 3657:2023
ICS:
67.200.10 Rastlinske in živalske Animal and vegetable fats
maščobe in olja and oils
SIST EN ISO 3657:2023 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 3657:2023

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SIST EN ISO 3657:2023


EN ISO 3657
EUROPEAN STANDARD

NORME EUROPÉENNE

July 2023
EUROPÄISCHE NORM
ICS 67.200.10 Supersedes EN ISO 3657:2020
English Version

Animal and vegetable fats and oils - Determination of
saponification value (ISO 3657:2023)
Corps gras d'origines animale et végétale - Tierische und pflanzliche Fette und Öle - Bestimmung
Détermination de l'indice de saponification (ISO der Verseifungszahl (ISO 3657:2023)
3657:2023)
This European Standard was approved by CEN on 12 May 2023.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3657:2023 E
worldwide for CEN national Members.

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SIST EN ISO 3657:2023
EN ISO 3657:2023 (E)
Contents Page
European foreword . 3

2

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SIST EN ISO 3657:2023
EN ISO 3657:2023 (E)
European foreword
This document (EN ISO 3657:2023) has been prepared by Technical Committee ISO/TC 34 "Food
products" in collaboration with Technical Committee CEN/TC 307 “Oilseeds, vegetable and animal fats
and oils and their by-products - Methods of sampling and analysis” the secretariat of which is held by
AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by January 2024, and conflicting national standards shall
be withdrawn at the latest by January 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 3657:2020.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 3657:2023 has been approved by CEN as EN ISO 3657:2023 without any modification.

3

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SIST EN ISO 3657:2023

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...

SLOVENSKI STANDARD
oSIST prEN ISO 3657:2023
01-april-2023
Živalske in rastlinske maščobe in olja - Določevanje števila umiljenja (ISO/DIS
3657:2023)
Animal and vegetable fats and oils - Determination of saponification value (ISO/DIS
3657:2023)
Tierische und pflanzliche Fette und Öle - Bestimmung der Verseifungszahl (ISO/DIS
3657:2023)
Corps gras d'origines animale et végétale - Détermination de l'indice de saponification
(ISO/DIS 3657:2023)
Ta slovenski standard je istoveten z: prEN ISO 3657
ICS:
67.200.10 Rastlinske in živalske Animal and vegetable fats
maščobe in olja and oils
oSIST prEN ISO 3657:2023 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN ISO 3657:2023

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oSIST prEN ISO 3657:2023
DRAFT INTERNATIONAL STANDARD
ISO/DIS 3657
ISO/TC 34/SC 11 Secretariat: BSI
Voting begins on: Voting terminates on:
2023-01-17 2023-04-11
Animal and vegetable fats and oils — Determination of
saponification value
Corps gras d'origines animale et végétale — Détermination de l'indice de saponification
ICS: 67.200.10
This document is circulated as received from the committee secretariat.
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
ISO/CEN PARALLEL PROCESSING
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 3657:2023(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION. © ISO 2023

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oSIST prEN ISO 3657:2023
ISO/DIS 3657:2023(E)
DRAFT INTERNATIONAL STANDARD
ISO/DIS 3657
ISO/TC 34/SC 11 Secretariat: BSI
Voting begins on: Voting terminates on:

Animal and vegetable fats and oils — Determination of
saponification value
Corps gras d'origines animale et végétale — Détermination de l'indice de saponification
ICS: 67.200.10
This document is circulated as received from the committee secretariat.
COPYRIGHT PROTECTED DOCUMENT
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
© ISO 2023
ISO/CEN PARALLEL PROCESSING
THEREFORE SUBJECT TO CHANGE AND MAY
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
NOT BE REFERRED TO AS AN INTERNATIONAL
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on STANDARD UNTIL PUBLISHED AS SUCH.
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
IN ADDITION TO THEIR EVALUATION AS
or ISO’s member body in the country of the requester. BEING ACCEPTABLE FOR INDUSTRIAL,
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CH-1214 Vernier, Geneva
POTENTIAL TO BECOME STANDARDS TO
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WHICH REFERENCE MAY BE MADE IN
Reference number
Email: copyright@iso.org
NATIONAL REGULATIONS.
Website: www.iso.org ISO/DIS 3657:2022(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
Published in Switzerland
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
ii
  © ISO 2023 – All rights reserved
PROVIDE SUPPORTING DOCUMENTATION. © ISO 2022

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oSIST prEN ISO 3657:2023
ISO/DIS 3657:2022(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle .
...

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