SIST ENV 14029:2002

Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix

This European Prestandard specifies methods using flame atomic absorption spectrometry (FAAS) and inductively coupled plasma emission spectrometry (ICP-ES) for the determination of elements at low content in lead for the ranges given in Table 1.
Higher contents than those listed in Table 1 should be determined according to ENV 13800.
Table 1 - Ranges of application for the determination of elements
Element   Ranges of applications (% m/m)
   FAAS   ICP-ES
Ag   0,00001   -   0,001   0,00001   -   0,001
Al   0,0001   -   0,005   0,00005   -   0,005
As   0,0002   -   0,005   0,00005   -   0,005
Bi   0,00005   -   0,0025   0,00005   -   0,0025
Ca   0,00005   -   0,001   0,00001   -   0,001
Cd   0,00005   -   0,001   0,00001   -   0,001
Co   0,00005   -   0,001   0,00005   -   0,001
Cr   0,00005   -   0,001   0,00005   -   0,001
Cu   0,00001   -   0,001   0,00001   -   0,001
Fe   0,00005   -   0,001   0,00005   -   0,001
Mg   0,00005   -   0,001   0,00005   -   0,001
Mn   0,00005   -   0,001   0,00005   -   0,001
Na   0,00005   -   0,001   0,00001   -   0,001
Ni   0,00005   -   0,001   0,00001   -   0,001
Sb   0,0002   -   0,0025   0,0002   -   0,0025
Se   0,0002   -   0,005   0,0002   -   0,005
Sn   0,0005   -   0,005   0,0002   -   0,005
Te   0,00002   -   0,0025   0,00002   -   0,0025
TI   0,00002   -   0,0025   0,00002   -   0,0025
Zn   0,00001   -   0,001   0,00001   -   0,001
These methods are intended as the definitive methods in case of dispute for the determination of elements at low content in lead. They are also recommended for the analysis of Certified Reference Materials (CRM) and Reference Materials (RM) which are used in analysis according to ENV 12908.

Blei und Bleilegierungen - Analyse durch Flammen-Atomabsorptionsspektrometrie (FAAS) oder Emissions-Spektrometrie mit induktiv gekoppeltem Plasma (ICP-ES), nach Abtrennung der Bleimatrix

Anwendungsbereich
Diese Europäische Vornorm legt ein flammen-atomabsorptionsspektrometrisches Verfahren (FAAS) und ein emissionsspektrometrisches Verfahren mit induktiv gekoppeltem Plasma (ICP-ES) für die Bestimmung der Elementgehalte in Blei fest, deren Bereiche in Tabelle 1 angegeben sind.
Höhere Gehalte als die in Tabelle 1 angegebenen, sollten nach ENV 13800 bestimmt werden.

Plomb et alliages de plomb - Analyse par spectrométrie d'absorption atomique dans la flamme (FAAS) ou spectrométrie d'émission atomique a plasma inductif couplé (ICP-ES), apres séparation de la matrice plomb

La présente Prénorme européenne spécifie des méthodes d'analyse utilisant la spectrométrie d'absorption atomique dans la flamme (FAAS) et la spectrométrie d'émission a plasma inductif couplé (ICP-ES) pour le dosage d'éléments a faible teneur dans le plomb pour les gammes de concentration données dans le Tableau 1.
Des teneurs plus élevées que celles données dans le Tableau peuvent etre déterminées par les méthodes spécifiées dans l'ENV 13800.
Tableau 1 - Gammes d'application pour le dosage des éléments
Elément   Gammes d'applications (% m/m)
   FAAS   ICP-ES
Ag   0,00001   -   0,001   0,00001   -   0,001
Al   0,0001   -   0,005   0,00005   -   0,005
As   0,0002   -   0,005   0,00005   -   0,005
Bi   0,00005   -   0,0025   0,00005   -   0,0025
Ca   0,00005   -   0,001   0,00001   -   0,001
Cd   0,00005   -   0,001   0,00001   -   0,001
Co   0,00005   -   0,001   0,00005   -   0,001
Cr   0,00005   -   0,001   0,00005   -   0,001
Cu   0,00001   -   0,001   0,00001   -   0,001
Fe   0,00005   -   0,001   0,00005   -   0,001
Mg   0,00005   -   0,001   0,00005   -   0,001
Mn   0,00005   -   0,001   0,00005   -   0,001
Na   0,00005   -   0,001   0,00001   -   0,001
Ni   0,00005   -   0,001   0,00001   -   0,001
Sb   0,0002   -   0,0025   0,0002   -   0,0025
Se   0,0002   -   0,005   0,0002   -   0,005
Sn   0,0005   -   0,005   0,0002   -   0,005
Te   0,00002   -   0,0025   0,00002   -   0,0025
TI   0,00002   -   0,0025   0,00002   -   0,0025
Zn   0,00001   -   0,001   0,00001   -   0,001
Ces méthodes sont conçues pour etre les méthodes a utiliser en cas de litige pour le dosage des éléments a faible teneur dans le plomb. Elles sont aussi recommandées pour l'analyse des Matériaux de référence certifiés (MRC) et des Matériaux de référence (MR) utilisés en analyse conformément a l'ENV 12908.

Svinec in svinčeve zlitine - Analize elementov s plamensko atomsko absorpcijsko spektrometrijo(FAAS) ali z emisijsko spektrometrijo z induktivno sklopljeno plazmo (ICP-ES) po odstranitvi svinčeve osnove

General Information

• Status: Withdrawn
• Publication Date: 31-Jan-2002
• Withdrawal Date: 13-May-2024
• ICS: 77.120.60 - Lead, zinc, tin and their alloys
• Technical Committee: INEK - Nonferrous metals
• Current Stage: 9900 - Withdrawal (Adopted Project)
• Start Date: 13-May-2024
• Due Date: 05-Jun-2024
• Completion Date: 14-May-2024
• Ref Project: ENV 14029:2001 - Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix

Standards Content (Sample)

SLOVENSKI STANDARD
SIST ENV 14029:2002
01-februar-2002
6YLQHFLQVYLQþHYH]OLWLQH$QDOL]HHOHPHQWRYVSODPHQVNRDWRPVNRDEVRUSFLMVNR
VSHNWURPHWULMR)$$6DOL]HPLVLMVNRVSHNWURPHWULMR]LQGXNWLYQRVNORSOMHQR
SOD]PR,&3(6SRRGVWUDQLWYLVYLQþHYHRVQRYH
Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or
inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead
matrix
Blei und Bleilegierungen - Analyse durch Flammen-Atomabsorptionsspektrometrie
(FAAS) oder Emissions-Spektrometrie mit induktiv gekoppeltem Plasma (ICP-ES), nach
Abtrennung der Bleimatrix
Plomb et alliages de plomb - Analyse par spectrométrie d'absorption atomique dans la
flamme (FAAS) ou spectrométrie d'émission atomique a plasma inductif couplé (ICP-
ES), apres séparation de la matrice plomb
Ta slovenski standard je istoveten z: ENV 14029:2001
ICS:
77.120.60 Svinec, cink, kositer in Lead, zinc, tin and their
njihove zlitine alloys
SIST ENV 14029:2002 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

SIST ENV 14029:2002

---------------------- Page: 2 ----------------------

SIST ENV 14029:2002
EUROPEAN PRESTANDARD
ENV 14029
PRÉNORME EUROPÉENNE
EUROPÄISCHE VORNORM
July 2001
ICS 77.040.30; 77.120.60
English version
Lead and lead alloys - Analysis by flame atomic absorption
spectrometry (FAAS) or inductively coupled plasma emission
spectrometry (ICP-ES), after separation of the lead matrix
Plomb et alliages de plomb - Analyse par spectrométrie Blei und Bleilegierungen - Analyse durch Flammen-
d'absorption atomique dans la flamme (FAAS) ou Atomabsorptionsspektrometrie (FAAS) oder Emissions -
spectrométrie d'émission atomique à plasma inductif Spektrometrie mit induktiv gekoppeltem Plasma (ICP-ES),
couplé (ICP-ES), après séparation de la matrice plomb nach Abtrennung der Bleimatrix
This European Prestandard (ENV) was approved by CEN on 9 June 2001 as a prospective standard for provisional application.
The period of validity of this ENV is limited initially to three years. After two years the members of CEN will be requested to submit their
comments, particularly on the question whether the ENV can be converted into a European Standard.
CEN members are required to announce the existence of this ENV in the same way as for an EN and to make the ENV available promptly
at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the ENV) until the final
decision about the possible conversion of the ENV into an EN is reached.
CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,
Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2001 CEN All rights of exploitation in any form and by any means reserved Ref. No. ENV 14029:2001 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------

SIST ENV 14029:2002
ENV 14029:2001 (E)
Contents
page
Foreword.3
1 Scope.4
2 Normative references .5
3 Principle .5
3.1 Preparation of the test solution.5
3.2 Instrumental techniques.5
4 Apparatus .6
4.1 General.6
4.2 Volumetric glassware .6
4.3 Filtration system .6
4.4 Instruments.
...