Aerospace series - Non-metallic materials - Textiles - Test method - Determination of water soluble chloride and sulfate of aqueous extracts

This European Standard specifies the determination of water soluble chloride and sulphate of aqueous extracts of textile materials. This method has been written in response to an aerospace requirement for a method of extraction using hot water, this method should be used in conjunction with EN 4426.

Luft- und Raumfahrt - Nichtmetallische Werkstoffe - Textilien - Prüfverfahren - Bestimmung von wasserlöslichem Chlorid und Sulfat in wässerigen Lösungen

Série aérospatiale - Matériaux non-métalliques - Textiles - Méthode d'essai - Détermination des chlorures et des sulfates des résidus aqueux

Aeronavtika - Nekovinski materiali - Tekstilije - Preskusne metode - Določanje vodotopnega klorida in sulfata v vodni raztopini

General Information

Status
Published
Publication Date
02-Jan-2014
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
23-Dec-2013
Due Date
27-Feb-2014
Completion Date
03-Jan-2014

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Luft- und Raumfahrt - Nichtmetallische Werkstoffe - Textilien - Prüfverfahren - Bestimmung von wasserlöslichem Chlorid und Sulfat in wässerigen LösungenSérie aérospatiale - Matériaux non-métalliques - Textiles - Méthode d'essai - Détermination des chlorures et des sulfates des résidus aqueuxAerospace series - Non-metallic materials - Textiles - Test method - Determination of water soluble chloride and sulfate of aqueous extracts49.025.60TekstilijeTextilesICS:Ta slovenski standard je istoveten z:EN 4503:2013SIST EN 4503:2014en01-februar-2014SIST EN 4503:2014SLOVENSKI
STANDARD



SIST EN 4503:2014



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 4503
July 2013 ICS 49.025.60 English Version
Aerospace series - Non-metallic materials - Textiles - Test method - Determination of water soluble chloride and sulfate of aqueous extracts
Série aérospatiale - Matériaux non-métalliques - Textiles - Méthode d'essai - Détermination des chlorures et des sulfates des résidus aqueux
Luft- und Raumfahrt - Nichtmetallische Werkstoffe - Textilien - Prüfverfahren - Bestimmung von wasserlöslichem Chlorid und Sulfat in wässerigen Lösungen This European Standard was approved by CEN on 8 May 2013.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2013 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 4503:2013: ESIST EN 4503:2014



EN 4503:2013 (E) 2 Contents Page Foreword . 3 Introduction. 4 1 Scope . 5 2 Normative references . 5 3 Terms and definitions . 5 4 Health, safety and environment . 6 5 Principle/Technique . 6 6 Resources. 6 7 Test samples/test pieces . 7 8 Test procedure . 8 9 Expression of results . 9 10 Measurement uncertainties . 10 11 Designation . 10 12 Test report . 10
SIST EN 4503:2014



EN 4503:2013 (E) 3 Foreword This document (EN 4503:2013) has been prepared by the Aerospace and Defence Industries Association of Europe - Standardization (ASD-STAN). After enquiries and votes carried out in accordance with the rules of this Association, this Standard has received the approval of the National Associations and the Official Services of the member countries of ASD, prior to its presentation to CEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2014, and conflicting national standards shall be withdrawn at the latest by January 2014. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 4503:2014



EN 4503:2013 (E) 4 Introduction This standard is part of the series of EN non-metallic materials standards for aerospace applications. The general organisation of this series is described in EN 4385. This standard is a level 3 document as defined in EN 4385. SIST EN 4503:2014



EN 4503:2013 (E) 5
1 Scope This European Standard specifies the determination of water soluble chloride and sulphate of aqueous extracts of textile materials. This method has been written in response to an aerospace requirement for a method of extraction using hot water, this method should be used in conjunction with EN 4426. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 4385, Aerospace series — Non-metallic materials – General organisation of standardization — Links between types of standards
EN 4426, Aerospace series — Non-metallic materials — Textiles — Test method — Determination of conductivity and pH of aqueous extracts 1)
EN 20139, Textiles — Standard atmospheres for conditioning and testing (ISO 139) EN ISO 3696, Water for analytical laboratory use — Specification and test methods (ISO 3696) ISO 383, Laboratory glassware — Interchangeable conical ground joints ISO 4793, Laboratory sintered (fritted) filters — Porosity grading, classification and designation 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 chloride free water soluble Cl− ion which could combine with free H+ ions to produce acidic conditions which would be detrimental to the ageing of fabrics 3.2 sulfates free water soluble SO4C ion which could combine with free H+ ions to produce acidic conditions which would be detrimental to the ageing of fabrics
1) Published as ASD-STAN Prestandard at the date of publication of this standard SIST EN 4503:2014



EN 4503:2013 (E) 6 4 Health, safety and environment This standard does not necessarily include all health and safety requirements associated with its use. Persons using this standard shall be familiar with normal laboratory/test house practices. It is the responsibility of the user to establish satisfactory health and safety practices and to ensure conformity with any European, National or local laws/regulations. 5 Principle/Technique An aqueous extract is prepared using distilled water. The soluble chloride and sulphate are then measured by gravimetric method. A volumetric method may also be used to determine the amount of soluble chloride. 6 Resources 6.1 Apparatus/facilities 6.1.1 Round bottomed flasks of chemically resistant glass with a volume of 250 ml and a ground glass neck of size 24/29 in accordance with ISO 383 6.1.2 A glass stopper incorporating a stopcock with P.T.F.E. core liner to prevent sticking of the glass core in the neck of the stopcock NOTE Grease shall not be used for this purpose. 6.1.3 Water-cooled condensers 6.1.4 Laboratory balance, accurate to 0,000 2 g 6.1.5 Sinter glass crucibles, porosity 4 in accordance with ISO 4793 6.1.6 Titration vessel and reference half-cell, with suitable p
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