SIST EN 725-2:2009

Advanced technical ceramics - Methods of test for ceramic powders - Part 2: Determination of impurities in barium titanate

This part of EN 725 describes a method for the determination of impurities in barium titanate powders using inductively coupled plasma optical emission spectroscopy (ICP-OES).
The method is applicable only to stoichiometric barium titanate. The maximum concentrations measured for each impurity are as follows:
   Sr   4 mg/g (4 000 ppm)
   Ca   500 ug/g (500 ppm)
   K   200 ug/g (200 ppm)
   Na, Mg, Al, Fe, Nb   100 g/g (100 ppm)
The minimum concentration or detection limits are from 1 ug/g to 5 ug/g (1 ppm to 5 ppm).

Hochleistungskeramik - Prüfverfahren für keramische Pulver - Teil 2: Bestimmung von Verunreinigungen in Bariumtitanatpulvern

Céramiques techniques avancées - Méthodes d'essai pour poudres céramiques - Partie 2 : Détermination des impuretés dans le titanate de baryum

La présente partie de l’EN 725 décrit une méthode permettant la détermination des impuretés présentes dans les poudres de titanate de baryum par spectrométrie d’émission avec plasma à couplage induit par haute fréquence et détecteur optique (ICP-OES).
La méthode ne s’applique qu’au titanate de baryum st chiométrique. Les concentrations maximales mesurées pour chaque impureté sont les suivantes :
   Sr   4 mg/g (4 000 ppm)
   Ca   500 µg/g (500 ppm)
   K   200 µg/g (200 ppm)
   Na, Mg, Al, Fe, Nb   100 µg/g (100 ppm)
Les limites de concentration minimale ou de détection s’échelonnent entre 1 µg/g et 5 µg/g (1 ppm et 5 ppm).

Sodobna tehnična keramika - Preskusne metode za keramične praške - 2. del: Ugotavljanje nečistoč v barijevem titanatu

General Information

• Status: Withdrawn
• Publication Date: 20-Nov-2008
• Withdrawal Date: 23-Nov-2022
• ICS: 81.060.30 - Advanced ceramics
• Technical Committee: I13 - Imaginarni 13
• Current Stage: 9900 - Withdrawal (Adopted Project)
• Start Date: 24-Nov-2022
• Due Date: 17-Dec-2022
• Completion Date: 24-Nov-2022
• Ref Project: EN 725-2:2007 - Advanced technical ceramics - Methods of test for ceramic powders - Part 2: Determination of impurities in barium titanate

Relations

• Replaced By: SIST EN ISO 21813:2023 - Fine ceramics (advanced ceramics, advanced technical ceramics) - Methods for chemical analysis of high purity barium titanate powders (ISO 21813:2019)
• Effective Date: 16-Nov-2022
• Replaces: SIST ENV 725-2:2000 - Advanced technical ceramics - Methods of test for ceramic powders - Part 2: Determination of impurities in barium titanate
• Effective Date: 01-Jan-2009

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 725-2:2009
01-januar-2009
1DGRPHãþD
SIST ENV 725-2:2000
6RGREQDWHKQLþQDNHUDPLND3UHVNXVQHPHWRGH]DNHUDPLþQHSUDãNHGHO
8JRWDYOMDQMHQHþLVWRþYEDULMHYHPWLWDQDWX
Advanced technical ceramics - Methods of test for ceramic powders - Part 2:
Determination of impurities in barium titanate
Hochleistungskeramik - Prüfverfahren für keramische Pulver - Teil 2: Bestimmung von
Verunreinigungen in Bariumtitanatpulvern
Céramiques techniques avancées - Méthodes d'essai pour poudres céramiques - Partie
2 : Détermination des impuretés dans le titanate de baryum
Ta slovenski standard je istoveten z: EN 725-2:2007
ICS:
81.060.30 Sodobna keramika Advanced ceramics
SIST EN 725-2:2009 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 725-2:2009

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SIST EN 725-2:2009
EUROPEAN STANDARD
EN 725-2
NORME EUROPÉENNE
EUROPÄISCHE NORM
November 2007
ICS 81.060.30 Supersedes ENV 725-2:1994
English Version
Advanced technical ceramics - Methods of test for ceramic
powders - Part 2: Determination of impurities in barium titanate
Céramiques techniques avancées - Méthodes d'essai pour Hochleistungskeramik - Prüfverfahren für keramische
poudres céramiques - Partie 2 : Détermination des Pulver - Teil 2: Bestimmung von Verunreinigungen in
impuretés dans le titanate de baryum Bariumtitanatpulvern
This European Standard was approved by CEN on 23 September 2007.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the
official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2007 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 725-2:2007: E
worldwide for CEN national Members.

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SIST EN 725-2:2009
EN 725-2:2007 (E)
Contents Page
Foreword.3
1 Scope .4
2 Normative references .4
3 Principle.4
4 Reagents.4
5 Apparatus .5
6 Preparation of sample solution.5
6.1 Sample calcination .5
6.2 Test sample .5
6.3 Dissolution of the test sample.5
7 Calibration .6
7.1 Standard addition method .6
7.2 Calibration method .6
8 Procedure .6
8.1 ICP spectrometer operation.6
8.2 Standard addition method .7
8.3 Calibration method .7
9 Test report .7

2

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SIST EN 725-2:2009
EN 725-2:2007 (E)
Foreword
This document (EN 725-2:2007) has been prepared by Technical Committee CEN/TC 184 “Advanced
technical ceramics”, the secretariat of which is held by BSI.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by May 2008, and conflicting national standards shall be withdrawn at the
latest by May 2008.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes ENV 725-2:1994.
EN 725 Advanced technical ceramics — Methods of test for ceramic powders was prepared in Parts as
follows:
Part 1: Determination of impurities in alumina
Part 2: Determination of impurities in barium titanate
Part 3: Determination of the oxygen content of non-oxides by thermal extraction with a carrier gas
Part 4: Determination of oxygen content in aluminium nitride by XRF analysis
Part 5 Determination of particle size distribution
Part 6: Determination of the specific surface area [withdrawn]
Part 7: Determination of the absolute density [withdrawn]
Part 8: Determination of tapped bulk density
Part 9: Determination of un-tapped bulk density
Part 10: Determination of compaction properties
Part 11: Determination of densification on natural sintering
Part 12: Chemical analysis of zirconia
Part 6 and part 7 of this series were superseded in 2005 by EN ISO 18757 and EN ISO 18753.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherla
...