SIST EN ISO 5511:1998

Oilseeds - Determination of oil content - Method using continuous-wave low-resolution nuclear magnetic resonance spectrometry (Rapid method) (ISO 5511:1992)

Under normal conditions of use, it does not apply to oilseeds which do not yield oil which is completely liquid at 20 °C (e.g. shea, palm, illipe, cocoa, etc.). The method has been successfully tested on the following oilseeds: rapeseed, soya, sunflower seed and groundnuts. The reference method for the determination of the oil content of oilseeds is specified in ISO 659.

Ölsamen - Bestimmung des Ölgehaltes - Kernresonanzspektroskopie mit niedriger Auflösung (Schnellverfahren) (ISO 5511:1992)

Diese Internationale Norm legt ein Schnellverfahren zur Bestimmung des Ölgehalts von Ölsamen unter Anwendung der magnetischen Kernresonanzspektroskopie mit niedriger Auflösung fest. Unter üblichen Anwendungsbedingungen gilt es nicht für Ölsamen, deren Ölgehalt bei 20 °C nicht vollständig flüssig ist (z.B. Sheafett, Palmöl, Illipefett, Kakaobutter usw.). Erfolgreich geprüft wurde dieses Verfahren an Rapssamen, Soja, Sonnenblumenkernen und Erdnüssen.

Graines oléagineuses - Détermination de la teneur en huile - Méthode par spectrométrie de résonance magnétique nucléaire a basse résolution et a onde continue (Méthode rapide) (ISO 5511:1992)

La présente Norme internationale prescrit une méthode rapide de détermination de la teneur en huile des graines oléagineuses, par spectrométrie de résonance magnétique nucléaire à basse résolution et à onde continue. Elle ne s'applique pas, dans les conditions usuelles d'emploi, aux graines oléagineuses ne donnant pas une huile entièrement liquide à 20 °C (karité, palmiste, illipé, cacao, etc.). La présente méthode a été expérimentée avec succès sur les graines oléagineuses suivantes: colza, soja, tournesol et arachide.
NOTE 1 La détermination de la teneur en huile des graines oléagineuses fait l'objet d'une méthode de référence spécifiée dans l'ISO 659.

Oljna semena - Določevanje olja - Hitra spektrometrijska metoda z uporabo jedrske magnetne resonance nizke ločljivosti (rapidna metoda) (ISO 5511:1992)

General Information

• Status: Withdrawn
• Publication Date: 31-Oct-1998
• Withdrawal Date: 31-Aug-2020
• ICS: 67.200.20 - Oilseeds
• Technical Committee: KŽP - Agricultural food products
• Current Stage: 9900 - Withdrawal (Adopted Project)
• Start Date: 25-Aug-2020
• Due Date: 17-Sep-2020
• Completion Date: 01-Sep-2020
• Ref Project: EN ISO 5511:1996 - Oilseeds - Determination of oil content - Method using continuous-wave low-resolution nuclear magnetic resonance spectrometry (Rapid method) (ISO 5511:1992)

Relations

• Corrected By: SIST EN ISO 5511:1998/AC:1998 - Oilseeds - Determination of oil content - Method using continuous-wave low-resolution nuclear magnetic resonance spectrometry (Rapid method)
• Effective Date: 22-Dec-2008

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 5511:1998
01-november-1998
2OMQDVHPHQD'RORþHYDQMHROMD+LWUDVSHNWURPHWULMVNDPHWRGD]XSRUDERMHGUVNH
PDJQHWQHUHVRQDQFHQL]NHORþOMLYRVWLUDSLGQDPHWRGD,62
Oilseeds - Determination of oil content - Method using continuous-wave low-resolution
nuclear magnetic resonance spectrometry (Rapid method) (ISO 5511:1992)
Ölsamen - Bestimmung des Ölgehaltes - Kernresonanzspektroskopie mit niedriger
Auflösung (Schnellverfahren) (ISO 5511:1992)
Graines oléagineuses - Détermination de la teneur en huile - Méthode par spectrométrie
de résonance magnétique nucléaire a basse résolution et a onde continue (Méthode
rapide) (ISO 5511:1992)
Ta slovenski standard je istoveten z: EN ISO 5511:1996
ICS:
67.200.20 Oljnice Oilseeds
SIST EN ISO 5511:1998 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 5511:1998

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SIST EN ISO 5511:1998

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SIST EN ISO 5511:1998

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SIST EN ISO 5511:1998

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SIST EN ISO 5511:1998

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SIST EN ISO 5511:1998
INTERNATIONAL
STANDARD
Second edition
1992-07-0 1
Oilseeds - Determination of oil content -
Method using continuous-wave low-resolution
nuclear magnetic resonance spectrometry
(Rapid method)
Graines oleagineuses - Dt%ermination de la teneur en huile - Methode
par spectrometrie de resonance magnetique nucleaire a basse resolution
et ~3 onde continue (Methode rapide)
Reference number
ISO 5511:1992(E)

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SIST EN ISO 5511:1998
ISO 5511:1992(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide
federation of national Standards bodies (ISO member bodies). The work
of preparing International Standards is normally carried out through ISO
technical committees. Esch member body interested in a subject for
which a technical committee has been established has the right to be
represented on that committee. International organizations, govern-
mentai and non-governmental, in liaison with ISO, also take part in the
work. ISO collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are
circulated to the member bodies for voting. Publication as an lnter-
national Standard requires approval by at least 75 % of the member
bodies casting a vote.
International Standard ISO 5511 was prepared by Technical Committee
ISO/TC 34, Agricultural food products, Sub-Committee SC 2, Oleaginous
seeds and fruits.
This second edition cancels and replaces the first edition
(ISO 5511:1984), of which it constitutes a technical revision.
Annex A of this International Standard is for information only.
0 ISO 1992
All rights reserved. NO part of this publication may be reproduced or utilized in any ferm
or by any means, electronie or mechanical, including photocopying and microfilm, without
Permission in writing from the publisher.
International Organization for Standardization
Gase Postale 56 l CH-1211 Geneve 20 l Switzerland
Printed in Switzeriand
ii

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SIST EN ISO 5511:1998
ISO 5511:1992(E)
INTERNATIONAL STANDARD
Oilseeds - Determination of oil content - Method using
continuous-wave low-resolution nuclear magnetic resonance
spectrometry (Rapid method)
3 Definitions
1 Scope
This International Standard specifies a rapid method For the purposes of this International Standard, the
for the determination of the oil content of oilseeds following definitions apply.
using continuous-wave low-resolution nuclear mag-
netic resonance spectrometry. 3.1 oil content: The mass fraction of organic sub-
stances, which are liquid at the temperature of
Under normal conditions of use, it does not apply to
measurement (in principle 20 “C) of the oilseeds,
oilseeds which do not yield oil which is completely
determined using the method specified in this Inter-
liquid at 20 “C (e.g. shea, Palm, illipe, cocoa, etc.).
national Standard.
This method has been successfully tested on the
The oil content is expressed as a percentage by
following oilseeds: rapeseed, soya, sunflower seed
mass.
and groundnuts.
3.2 Single test result: Result obtained by carrying
NOTE 1 The reference method for the determination of
out a specified test method one time according to
the oil content of oilseeds is specified in ISO 659.
the prescribed procedure.
3.3 repeatability conditions: Conditions where
2 Normative references
mutally independent test results are obtained with
the Same method on identical test material in the
The following Standards contain provisions which,
Same laboratory by the Same Operator using the
through reference in this text, constitute provisions
Same equipment within short intervals of time.
of this International Standard. At the time of publi-
[ISO 5725:1986, 3.1.71
cation, the editions indicated were valid. All stan-
dards are subject to revision, and Parties to
agreements based on this International Standard
4 Principle
are encouraged to investigate the possibility of ap-
plying the most recent editions of the Standards in-
Determination using continuous-wave Iow-resolution
dicated below. Members of IEC and ISO maintain
nuclear magnetic resonance (NMR) spectrometry of
registers of currently valid International Standards.
the content of liquid components containing hydro-
gen which are present in oilseeds which have been
ISO 659:1988, Oilseeds - Determination of hexane
previously dried at 103 “C + 2 ‘C, and taking into
extract (or light petroleum extract), called “oil con-
account the effect of solids (Gilseed residue). .
tent ”.
ISO 664:1990, Oilseeds - Reduction of laboratory
5 Materials
Sample fo fest Sample.
5.1 Calibration oil, crude oil from seeds of the
Determination of moisfure
ISO 665:1977, Oilseeds -
Same botanical species and of similar geographical
and volatile matter contenf.
origin and Chemical composition to those of the
extracted in the laboratory
seeds for analysis,
ISO 771:1977, Oilseed residues - Determination of
carrying out the analysis, in accordance with the
moisture and volafile maffer content.
1

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SIST EN ISO 5511:1998
ISO 5511:1992(E)
method specified in ISO 659, less than 1 month pre- carried out strictly at the Same temperature. lt is
viously.
recommended, if the necessary apparatus is avail-
able, to control thermostatically the “effective” patt
Store the oil under conditions preventing
dry
of the instrument and to place the seeds, before
Oxidation.
measurement, in insulated metal blocks at the
measuring temperature. Otherwise, carry out a
5.2 Oilseed residue, from seeds of the Same bot-
simplified calibration of the apparatus every 30 min
anical species, and of similar geographicai origin
(see 9.2.5).
and Chemical composition, to those of the seeds for
analysis, from which the oil has been extracted in
9.1 Check an repeatability (if required)
the laboratory carrying out the analysis, in accord-
ante with the method specified in ISO 659, less than
If it is required to establish whether the repeatability
1 month previously.
requirement (see clause 11) is met, carry out two
Single determinations, each including the two inter-
6 Apparatus mediate determinations (9.6) under repeatability
conditions (see 3.3).
Usual laboratory apparatus and, in particular, the
following.
9.2 Calibration of the instrument
6.1 Apparatus required for the drying method (see
9.2.1 Adjust the NMR spectrometer (6.2) in accord-
ISO 665).
ante with the manufacturer ’s instructions, then ad-
just to Zero after placing an empty measuring tube
6.2 Continuous-wave low-resolution NMR spec-
(6.3) in the magnetic field.
trometer
9.2.2 Into four measuring tubes identical to that
6.3 Measuring tubes, preferably with closures, used for the adjustment (i.e. also giving a reading
suitable for use with the NMR spectrometer (6.2) and of Zero when they are placed empty in the magnetic
of the largest possible capacity, made from a non- field), weigh, to the nearest 0,Ol g, 5 g, 10 g, 20 g,
conducting non-magnetic material which does not
and,
...