Preparation of steel substrates before application of paints and related products - Tests for the assessment of surface cleanliness - Part 6: Extraction of water soluble contaminants for analysis (Bresle method) (ISO 8502-6:2020)

This document specifies a method of extracting, for analysis, water soluble contaminants from a surface by use of flexible cells in the form of adhesive patches or sleeves which can be attached to any surface, regardless of its shape (flat or curved) and its orientation (facing in any direction, including downwards).
The method described is suitable for use in the field to determine the presence of water soluble contaminants before painting or a similar treatment.
This document does not cover the subsequent analysis of the contaminants that have been dissolved.
Methods of analysis suitable for field use are described in other parts of ISO 8502.
NOTE The extraction method might give a false negative or not take all the water-soluble material off the surface because of: a) Soluble materials hiding in the crevices or under folds of metal; b) Soluble materials under corrosion layers, passivation layers produced by corrosion inhibitors, oil, grease, or other non-visible thin films.

Vorbereitung von Stahloberflächen vor dem Auftragen von Beschichtungsstoffen - Prüfungen zum Bewerten der Oberflächenreinheit - Teil 6: Lösen von wasserlöslichen Verunreinigungen zur Analyse - Bresle-Verfahren (ISO 8502-6:2020)

Dieses Dokument legt ein Verfahren zum Extrahieren von wasserlöslichen Verunreinigungen von einer Oberfläche zur Analyse fest, bei dem verformbare Zellen in Form von selbstklebenden Pflastern oder Hülsen verwendet werden, die auf jede Oberfläche, unabhängig von deren Form (eben oder gekrümmt) und Lage (in jeder Richtung, auch nach unten) geklebt werden können.
Das Verfahren ist als Feldverfahren geeignet, um wasserlösliche Verunreinigungen vor dem Beschichten oder ähnlichen Behandlungen zu bestimmen.
Dieses Dokument befasst sich nicht mit der anschließenden Analyse der gelösten Verunreinigungen. Analysenverfahren, die als Feldverfahren geeignet sind, werden in anderen Teilen von ISO 8502 beschrieben.
ANMERKUNG   Das Extraktionsverfahren könnte ein falschnegatives Ergebnis zur Folge haben oder nicht alle wasserlöslichen Stoffe von der Oberfläche lösen, da a) lösliche Stoffe sich in Spalten oder unter Faltungen des Metalls verbergen; b) lösliche Stoffe auch unter Korrosionsschichten, Passivierungsschichten, erzeugt durch Korrosions¬inhibitoren, Öl, Fett oder anderen nicht sichtbaren, dünnen Schichten sein können.

Préparation des subjectiles d'acier avant application de peintures et de produits assimilés - Essais pour apprécier la propreté d'une surface - Partie 6: Extraction des contaminants solubles en vue de l'analyse (Méthode de Bresle) (ISO 8502-6:2020)

Le présent document spécifie une méthode d'extraction en surface, en vue de l'analyse, des contaminants solubles dans l'eau, au moyen de cellules souples telles que des pastilles adhésives ou des manchons qui peuvent être fixés sur toute surface, sans se soucier de leur forme (plate ou ronde) et de leur orientation (dans toutes les directions, y compris vers le bas).
La méthode décrite convient pour l'emploi in situ en vue de déterminer la présence de contaminants solubles dans l'eau avant de peindre ou d'effectuer un traitement similaire.
Le présent document ne traite pas de l'analyse consécutive des contaminants qui ont été dissous. Les méthodes d'analyse appropriées à l'emploi in situ sont décrites dans d'autres parties de l'ISO 8502.
NOTE Il est possible que la méthode d'extraction donne un résultat faux négatif ou qu'elle ne permette pas d'extraire de la surface toutes les substances solubles dans l'eau, pour les raisons suivantes: a) Des substances solubles dissimulées dans des fissures ou sous des pliures de métal; b) Des substances solubles dissimulées sous les couches de corrosion, les couches de passivation produites par les inhibiteurs de corrosion, dans l'huile, la graisse, ou d'autres fines couches (films) invisibles.

Priprava jeklenih podlag pred nanašanjem barvnih in sorodnih premazov - Preskusi za ocenjevanje čistosti površine - 6. del: Ekstrakcija v vodi topnih nečistoč za analizo (Breslova metoda) (ISO 8502-6:2020)

General Information

Status
Published
Public Enquiry End Date
03-Jul-2019
Publication Date
10-Jun-2020
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
04-Jun-2020
Due Date
09-Aug-2020
Completion Date
11-Jun-2020

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SLOVENSKI STANDARD
SIST EN ISO 8502-6:2020
01-julij-2020
Nadomešča:
SIST EN ISO 8502-6:2006
Priprava jeklenih podlag pred nanašanjem barvnih in sorodnih premazov -
Preskusi za ocenjevanje čistosti površine - 6. del: Ekstrakcija v vodi topnih
nečistoč za analizo (Breslova metoda) (ISO 8502-6:2020)

Preparation of steel substrates before application of paints and related products - Tests

for the assessment of surface cleanliness - Part 6: Extraction of water soluble
contaminants for analysis (Bresle method) (ISO 8502-6:2020)
Vorbereitung von Stahloberflächen vor dem Auftragen von Beschichtungsstoffen -

Prüfungen zum Bewerten der Oberflächenreinheit - Teil 6: Lösen von wasserlöslichen

Verunreinigungen zur Analyse - Bresle-Verfahren (ISO 8502-6:2020)

Préparation des subjectiles d'acier avant application de peintures et de produits

assimilés - Essais pour apprécier la propreté d'une surface - Partie 6: Extraction des

contaminants solubles en vue de l'analyse (Méthode de Bresle) (ISO 8502-6:2020)
Ta slovenski standard je istoveten z: EN ISO 8502-6:2020
ICS:
25.220.10 Priprava površine Surface preparation
87.020 Postopki za nanašanje Paint coating processes
barvnih premazov
SIST EN ISO 8502-6:2020 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 8502-6:2020
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SIST EN ISO 8502-6:2020
EN ISO 8502-6
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2020
EUROPÄISCHE NORM
ICS 25.220.10 Supersedes EN ISO 8502-6:2006
English Version
Preparation of steel substrates before application of paints
and related products - Tests for the assessment of surface
cleanliness - Part 6: Extraction of water soluble
contaminants for analysis (Bresle method)(ISO 8502-
6:2020)

Préparation des subjectiles d'acier avant application de Vorbereitung von Stahloberflächen vor dem Auftragen

peintures et de produits assimilés - Essais pour von Beschichtungsstoffen - Prüfungen zum Bewerten

apprécier la propreté d'une surface - Partie 6: der Oberflächenreinheit - Teil 6: Lösen von

Extraction des contaminants solubles en vue de wasserlöslichen Verunreinigungen zur Analyse -

l'analyse (Méthode de Bresle) (ISO 8502-6:2020) Bresle-Verfahren (ISO 8502-6:2020)

This European Standard was approved by CEN on 1 May 2020.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this

European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references

concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN

member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by

translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management

Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2020 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 8502-6:2020 E

worldwide for CEN national Members.
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SIST EN ISO 8502-6:2020
EN ISO 8502-6:2020 (E)
Contents Page

European foreword ....................................................................................................................................................... 3

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SIST EN ISO 8502-6:2020
EN ISO 8502-6:2020 (E)
European foreword

This document (EN ISO 8502-6:2020) has been prepared by Technical Committee ISO/TC 35 "Paints

and varnishes" in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” the

secretariat of which is held by DIN.

This European Standard shall be given the status of a national standard, either by publication of an

identical text or by endorsement, at the latest by November 2020, and conflicting national standards

shall be withdrawn at the latest by November 2020.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. CEN shall not be held responsible for identifying any or all such patent rights.

This document supersedes EN ISO 8502-6:2006.

According to the CEN-CENELEC Internal Regulations, the national standards organizations of the

following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,

Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,

Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of

North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the

United Kingdom.
Endorsement notice

The text of ISO 8502-6:2020 has been approved by CEN as EN ISO 8502-6:2020 without any

modification.
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SIST EN ISO 8502-6:2020
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SIST EN ISO 8502-6:2020
INTERNATIONAL ISO
STANDARD 8502-6
Third edition
2020-04
Preparation of steel substrates before
application of paints and related
products — Tests for the assessment
of surface cleanliness —
Part 6:
Extraction of water soluble
contaminants for analysis (Bresle
method)
Préparation des subjectiles d'acier avant application de peintures
et de produits assimilés — Essais pour apprécier la propreté d'une
surface —
Partie 6: Extraction des contaminants solubles en vue de l'analyse
(Méthode de Bresle)
Reference number
ISO 8502-6:2020(E)
ISO 2020
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SIST EN ISO 8502-6:2020
ISO 8502-6:2020(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2020

All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may

be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting

on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address

below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Fax: +41 22 749 09 47
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2020 – All rights reserved
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SIST EN ISO 8502-6:2020
ISO 8502-6:2020(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

Introduction ..................................................................................................................................................................................................................................v

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 2

5 Apparatus and materials.............................................................................................................................................................................. 2

6 Procedure..................................................................................................................................................................................................................... 3

6.1 Selection of test surface ................................................................................................................................................................... 3

6.2 Blank test ..................................................................................................................................................................................................... 3

6.3 Extraction by patch or sleeve by injection ...................................................................................................................... 3

6.4 Extraction by sleeve by pre-filling .......................................................................................................................................... 5

7 Analyses ......................................................................................................................................................................................................................... 5

8 Test report ................................................................................................................................................................................................................... 5

Annex A (normative) Leak test for type testing of adhesive cells (patches and sleeves) ...............................9

Bibliography .............................................................................................................................................................................................................................11

© ISO 2020 – All rights reserved iii
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SIST EN ISO 8502-6:2020
ISO 8502-6:2020(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are

described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the

different types of ISO documents should be noted. This document was drafted in accordance with the

editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of

any patent rights identified during the development of the document will be in the Introduction and/or

on the ISO list of patent declarations received (see www .iso .org/ patents).

Any trade name used in this document is information given for the convenience of users and does not

constitute an endorsement.

For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and

expressions related to conformity assessment, as well as information about ISO's adherence to the

World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see www .iso .org/

iso/ foreword .html.

This document was prepared by Technical Committee ISO/TC 35, Paints and varnishes, Subcommittee

SC 12, Preparation of steel substrates before application of paints and related products, . in collaboration

with the European Committee for Standardization (CEN) Technical Committee CEN/TC 139, Paints and

varnishes, in accordance with the Agreement on technical cooperation between ISO and CEN (Vienna

Agreement).

This third edition cancels and replaces the second edition (ISO 8502-6:2006), which has been technically

revised.
The main changes compared to the previous edition are as follows:

— inclusion of the sleeve type extraction cells to be used with water extraction;

— specification that only water is used as a solvent for this method.
A list of all parts in the ISO 8502 series can be found on the ISO website.

Any feedback or questions on this document should be directed to the user’s national standards body. A

complete listing of these bodies can be found at www .iso .org/ members .html.
iv © ISO 2020 – All rights reserved
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SIST EN ISO 8502-6:2020
ISO 8502-6:2020(E)
Introduction

The performance of protective coatings of paint and related products applied to steel is significantly

affected by the state of the steel surface immediately prior to painting. The principal factors that are

known to influence this performance are:
a) the presence of rust and mill scale;

b) the presence of surface contaminants, including salts, dust, oils and greases;

c) the surface profile.

The ISO 8501 series, ISO 8502 series and ISO 8503 series have been prepared to provide methods of

assessing these factors, while ISO 8504 series provides guidance on the preparation methods that are

available for cleaning steel substrates, indicating the capabilities of each in attaining specified levels of

cleanliness.

These series of International Standards do not contain recommendations for the protective coating

systems to be applied to the steel surface. Neither do they contain recommendations for the surface

quality requirements for specific situations, even though surface quality can have a direct influence

on the choice of protective coating to be applied and on its performance. Such recommendations are

found in other documents such as national standards and codes of practice. Users of these International

Standards should ensure that the qualities specified are:

— compatible and appropriate both for the environmental conditions to which the steel will be exposed

and for the protective coating system to be used;
— within the capability of the cleaning procedure specified.

The four series of International Standards referred to above deal with the following aspects of

preparation of steel substrates:
— ISO 8501 covers the visual assessment of surface cleanliness;
— ISO 8502 covers the tests for the assessment of surface cleanliness;

— ISO 8503 covers the surface roughness characteristics of blast-cleaned steel substrates;

— ISO 8504 covers the surface preparation methods.

This document is one of many parts of ISO 8502 that specify tests for the assessment of surface

cleanliness. In relation to such tests, there are several methods for the extraction, for analysis, of

soluble contaminants on surfaces to be painted. One of these methods is based on the swabbing

of comparatively large test surfaces. This technique provides average values of the contamination

present, but it might conceal localized concentrations of contaminants. Also, swabbing might not ensure

sufficient penetration to dissolve all the deep-seated contamination such as ferrous salts.

There are other methods, however, which use small cells for the liquid used to remove and collect the

surface contaminants. The cells are attached to test surfaces where soluble contaminants could be

expected, e.g. where pitting has occurred and prevent loss of extraction solution from evaporate. This

closed cell technique usually provides more accurate, point values of the contamination present.

This document describes a simple, inexpensive field test using flexible cells in the form of adhesive cells

designed to be filled with water. The method was originally developed by a Swedish scientist, Dr. A.

Bresle, using one of the cell types included in this document.
© ISO 2020 – All rights reserved v
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SIST EN ISO 8502-6:2020
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SIST EN ISO 8502-6:2020
INTERNATIONAL STANDARD ISO 8502-6:2020(E)
Preparation of steel substrates before application of paints
and related products — Tests for the assessment of surface
cleanliness —
Part 6:
Extraction of water soluble contaminants for analysis
(Bresle method)
1 Scope

This document specifies a method of extracting, for analysis, water soluble contaminants from a

surface by use of flexible cells in the form of adhesive patches or sleeves which can be attached to any

surface, regardless of its shape (flat or curved) and its orientation (facing in any direction, including

downwards).

The method described is suitable for use in the field to determine the presence of water soluble

contaminants before painting or a similar treatment.

This document does not cover the subsequent analysis of the contaminants that have been dissolved.

Methods of analysis suitable for field use are described in other parts of ISO 8502.

NOTE The extraction method might give a false negative or not take all the water-soluble material off the

surface because of: a) Soluble materials hiding in the crevices or under folds of metal; b) Soluble materials under

corrosion layers, passivation layers produced by corrosion inhibitors, oil, grease, or other non-visible thin films.

2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

ISO 554, Standard atmospheres for conditioning and/or testing — Specifications
ISO 3696, Water for analytical laboratory use — Specification and test methods

ISO 8501-1, Preparation of steel substrates before application of paints and related products — Visual

assessment of su
...

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