Standard Test Method for Extrusion Rate and Application Life of Elastomeric Sealants

SIGNIFICANCE AND USE
4.1 The results obtained by this test method are simply a measure of the time required to extrude a known volume of sealant through a known orifice under a predetermined pressure.  
4.2 This test method is not considered a measure of cure rate.
SCOPE
1.1 This test method covers two laboratory procedures for determining the extrusion rate and application life (or “pot life”) of elastomeric chemically curing sealants for use in building construction.  
Note 1: These sealants are supplied with various rheological properties ranging from pourable liquids to nonsagging pastes. Single-component sealants are supplied ready for use upon opening the container, and their rate of cure is determined by the climatic conditions to which they are exposed. Multicomponent sealants are supplied as a base component and a curing agent separately packaged. After mixing the two parts, the sealant is ready for application, and curing begins immediately.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.  
1.3 There is no known ISO equivalent to this test method.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C603 − 14
Standard Test Method for
Extrusion Rate and Application Life of Elastomeric
1
Sealants
This standard is issued under the fixed designation C603; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 4. Significance and Use
4.1 The results obtained by this test method are simply a
1.1 This test method covers two laboratory procedures for
measure of the time required to extrude a known volume of
determining the extrusion rate and application life (or “pot
sealant through a known orifice under a predetermined pres-
life”) of elastomeric chemically curing sealants for use in
sure.
building construction.
4.2 This test method is not considered a measure of cure
NOTE 1—These sealants are supplied with various rheological proper-
rate.
ties ranging from pourable liquids to nonsagging pastes. Single-
componentsealantsaresuppliedreadyforuseuponopeningthecontainer,
5. Apparatus
and their rate of cure is determined by the climatic conditions to which
they are exposed. Multicomponent sealants are supplied as a base
5.1 Caulking Gun, 177-mL (6-fl oz) capacity, air-powered.
component and a curing agent separately packaged. After mixing the two
parts, the sealant is ready for application, and curing begins immediately.
5.2 Polyethylene Cartridge, 177-mL(6-fl oz), with the front
end having an inside diameter of 13.7 6 0.05 mm (0.540 6
1.2 The values stated in SI units are to be regarded as the
0.002 in.).
standard. The values given in parentheses are provided for
information only.
5.3 Air Supply, providing 345 kPa (50-psi) pressure and
having the necessary connection fittings for attachment to the
1.3 There is no known ISO equivalent to this test method.
air-powered caulking gun.
1.4 This standard does not purport to address all of the
5.4 Timing Device (clock or watch), calibrated in seconds.
safety concerns, if any, associated with its use. It is the
5.5 500-mL (1-pt) Container
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
6. Procedure
bility of regulatory limitations prior to use.
6.1 Extrusion Rate of Single-Component Sealant—First
condition the unopened container for at least 16 h at standard
2. Referenced Documents
conditions. Then place a sufficient amount of sealant into the
2
2.1 ASTM Standards:
177-mL(6-fl oz) cartridge to fill it completely with the plunger
C717 Terminology of Building Seals and Sealants
in place, fully retracted. Using no nozzle on the cartridge, gun
the sealant at 345 kPa (50-psi) pressure into the 500-mL (1-pt)
3. Terminology
container, measuring the time in seconds required to empty the
cartridge.
3.1 Refer to Terminology C717 for definitions of the fol-
lowing terms used in this standard: standard conditions.
NOTE 2—When the printed instructions of the sealant manufacturer so
recommended, heat the sealant before extruding it into the container.
6.2 Extrusion Rate or Application Life or both, of Mixed
1
ThistestmethodisunderthejurisdictionofASTMCommitteeC24onBuilding
Multicomponent Sealant—First condition the unopened con-
Seals and Sealants and is the direct responsibility of Subcommittee C24.20 on
tainers of both sealant and curing agent for at least 16 h at
General Test Methods.
standard conditions. Then mix 400 g of the sealant with the
CurrenteditionapprovedJune1,2014.PublishedJuly2014.Originallyapproved
proper amount of curing agent, stirring the mixture by hand for
in 1969. Last previous edition approved in 2008 as C603 - 04(2008). DOI:
10.1520/C0603-14.
5 min. Place a sufficient amount of the mixed compound into
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
the 177-mL (6-fl oz) cartridge to fill it completely with the
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
plunger in place, fully retracted, and set the filled cartridge
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. aside, in a vertical position, at standard conditions, for 3 h
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C603 − 14
(Note 3). Then, using no nozzle on the cartridge, gun the 7.1.2 The time, in seconds, required to empty the cartridge
sealant at 345 kPa (50-psi) pressure into the 500-mL (1-pt) (the extrusion rate), and
container, measuring the time in seconds required to empty the 7.1.3 Any vari
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C603 − 04 (Reapproved 2008) C603 − 14
Standard Test Method for
Extrusion Rate and Application Life of Elastomeric
1
Sealants
This standard is issued under the fixed designation C603; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope
1.1 This test method covers two laboratory procedures for determining the extrusion rate and application life (or “pot life”) of
elastomeric chemically curing sealants for use in building construction.
NOTE 1—These sealants are supplied with various rheological properties ranging from pourable liquids to nonsagging pastes. Single-component
sealants are supplied ready for use upon opening the container, and their rate of cure is determined by the climatic conditions to which they are exposed.
Multicomponent sealants are supplied as a base component and a curing agent separately packaged. After mixing the two parts, the sealant is ready for
application, and curing begins immediately.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information
only.
1.3 There is no known ISO equivalent to this test method.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C717 Terminology of Building Seals and Sealants
3. Terminology
3.1 Definitions—For definitions of terms used in test method, see Terminology C717.
3.1 Refer to Terminology C717 for definitions of the following terms used in this standard: standard conditions.
4. Significance and Use
4.1 The results obtained by this test method are simply a measure of the time required to extrude a known volume of sealant
through a known orifice under a predetermined pressure.
4.2 This test method is not considered a measure of cure rate.
5. Apparatus
5.1 Caulking Gun, 177-mL (6-fl oz) capacity, air-powered.
5.2 Polyethylene Cartridge, 177-mL (6-fl oz), with the front end having an inside diameter of 13.7 6 0.05 mm (0.540 6 0.002
in.).
5.3 Air Supply, providing 345 kPa (50-psi) pressure and having the necessary connection fittings for attachment to the
air-powered caulking gun.
1
This test method is under the jurisdiction of ASTM Committee C24 on Building Seals and Sealants and is the direct responsibility of Subcommittee C24.20 on General
Test Methods.
Current edition approved May 1, 2008June 1, 2014. Published June 2008July 2014. Originally approved in 1969. Last previous edition approved in 20042008 as
C603 - 04.C603 - 04(2008). DOI: 10.1520/C0603-04R08.10.1520/C0603-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C603 − 14
5.4 Timing Device (clock or watch), calibrated in seconds.
5.5 500-mL (1-pt) Container
6. Standard Test Conditions
6.1 Unless otherwise specified by those authorizing the tests, standard conditions for both tests are room temperature of 23 6
2°C (73.4 6 3.6°F) and 50 6 5 % relative humidity.
6. Procedure
6.1 Extrusion Rate of Single-Component Sealant—First condition the unopened container for at least 16 h at standard
conditions. Then place a sufficient amount of sealant into the 177-mL (6-fl oz) cartridge to fill it completely with the plunger in
place, fully retracted. Using no nozzle on the cartridge, gun the sealant at 345 kPa (50-psi) pressure into the 500-mL (1-pt)
container, measuring the time in seconds required to empty the cartridge.
NOTE 2—When the printed instructions of the sealant manufacturer so recommended, heat the sealant before extruding it into the container.
6.2 Extrusion Rate or Application Life or both, of Mixed Multicomponent Sealant—First condition the unopened containers of
both sealant and curing agent for
...

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