ASTM C1635-06
(Test Method)Standard Test Method to Evaluate Adhesion/Cohesion Properties of a Sealant at Fixed Extension
Standard Test Method to Evaluate Adhesion/Cohesion Properties of a Sealant at Fixed Extension
SCOPE
1.1 This test method describes a laboratory procedure for measuring the adhesion/cohesion properties of a sealant when subjected to tensile loads resulting from an applied specified strain. The adhesion/cohesion properties are evaluated before, during, and after water immersion.
1.2 This test method examines the adhesive and cohesive performance of a sealant on a specified substrate at a strain equivalent to a multiple of the strain/movement capability designated by the manufacturer for the given sealant per Specification C 920.
1.3 The values stated in SI (metric) units are to be regarded as the standard. The inch values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.4 Comparable Test
1.4.1 ISO 10590, Building construction - Jointing products - Sealants - Determination of adhesion/cohesion properties at maintained extension after immersion in water
1.4.2 ISO 8340, Building construction - Jointing products - Sealants - Determination of tensile properties at maintained extension
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Designation: C1635 − 06
StandardTest Method to
Evaluate Adhesion/Cohesion Properties of a Sealant at
Fixed Extension
This standard is issued under the fixed designation C1635; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope C920Specification for Elastomeric Joint Sealants
C1375Guide for Substrates Used in Testing Building Seals
1.1 This test method describes a laboratory procedure for
and Sealants
measuring the adhesion/cohesion properties of a sealant when
subjected to tensile loads resulting from an applied specified
3. Terminology
strain. The adhesion/cohesion properties are evaluated before,
during, and after water immersion.
3.1 Definitions:
3.1.1 casting spacers—thespacersusedinthefabricationof
1.2 This test method examines the adhesive and cohesive
the joints made from wet sealant
performance of a sealant on a specified substrate at a strain
3.1.2 separators—the device or item used to maintain the
equivalent to a multiple of the strain/movement capability
designated by the manufacturer for the given sealant per specimens at fixed extension.
Specification C920.
4. Summary of Test Method
1.3 The values stated in SI (metric) units are to be regarded
as the standard. The inch values given in parentheses are for 4.1 Test specimens made in accordance with dimensions set
information only. forth in Test Method C719 are fabricated and allowed to cure.
1.4 This standard does not purport to address all of the
4.2 Test specimens are extended at standard conditions to a
safety concerns, if any associated with its use. It is the
specified strain and blocked at the strain for a specified period
responsibility of the user of this standard to establish appro-
of time.
priate safety and health practices and determine the applica-
4.3 The test specimens are examined for adhesive or cohe-
bility of regulatory limitations prior to use.
sive failure, or both, of the sealant at 0, 24 and 168 h.
1.5 Comparable Test:
4.4 A duplicate set of three test specimens are cured at
1.5.1 ISO 10590, Building construction - Jointing products
standard conditions, extended to a specified strain, and then
- Sealants - Determination of adhesion/cohesion properties at
immersed (totally) in deionized water or specified medium (3
maintained extension after immersion in water
specimens/liter of liquid).
1.5.2 ISO 8340, Building construction - Jointing products -
Sealants - Determination of tensile properties at maintained
4.5 Immersed test specimens are observed at 0, 24 and 168
extension
and other additional specified hours.
4.6 This test method uses ASTM standard substrates as
2. Referenced Documents
described in Guide C1375. This test method does not exclude
2.1 ASTM Standards:
the use of any other substrate that provides a suitable flat
C717Terminology of Building Seals and Sealants
surface.
C719Test Method for Adhesion and Cohesion of Elasto-
meric Joint Sealants Under Cyclic Movement (Hockman
5. Significance and Use
Cycle)
5.1 Inanysealantapplication,thesealantmustbecapableof
maintaining an adhesive bond to the substrate when held in
ThistestmethodisunderthejurisdictionofASTMCommitteeC24onBuilding
strain for its intended service life.
Seals and Sealants and is the direct responsibility of Subcommittee C24.30 on
Adhesion
5.2 This test method is an indicator of a sealant’s ability to
Current edition approved Jan. 1, 2006. Published February 2006. DOI: 10.1520/
adhere under strain to a given substrate.
C1635-06.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
5.3 The default test strain is the movement ability of the
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
sealant as designated by the manufacturer. The default joint
Standards volume information, refer to the standard’s Document Summary page on
1 1
the ASTM website. configuration is 12.7 × 12.7 × 50.8 mm ( ⁄2 × ⁄2 × 2 in.). Other
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
C1635 − 06
strains and joint configurations may be used and reported as 7.2 Curing Method
noted in Section 8 and Table 1. 7.2.1 Cure specimens under one of the following cycles:
7.2.1.1 Standard Conditions—23 62°C(73.4 63.6°F),50
6. Apparatus and Materials
6 5% relative humidity for a minimum of 21 days.
6.1 Container,forimmersionmadeofamaterialcompatible 7.2.1.2 Alternately,cureforatotalof21daysasfollows: (a)
7 days at standard conditions above; (b) 7 days at 38 6 2°C
with the immersion medium.
(100 6 3.6 °F) and 95% relative humidity; (c) 7 days at
6.2 Device, to provide a strain on the test specimen.
standard conditions.
6.3 Spatulas, for use in applying the sealant.
7.2.1.3 The sealant manufacturer may request conditions
other than those specified provided the temperature does not
6.4 Caulking Gun, for extruding sealant from cartridges
exceed 50°C (122°F).
when applicable.
7.2.2 Remove the casting spacers from the specimens after
6.5 Substrates—Twelve substrates minimum of 25.4 × 76.2
curing.
mm (1 × 3 in.) of the same finish are required for each test
7.2.2.1 During the second week of the curing period, make
sample.
attempts to free the compound from the casting spacer blocks
6.6 Casting Spacers—Made from polytetrafluoroethylene
at the ends and bottom without damaging the sealant bead.
(PTFE) or a suitable rigid material shall be used with each test
7.2.2.2 Separate the casting spacer blocks from the sealant
specimen to which the test sealant will not bond and will
assoonaspracticalduringthecuringperiodwithoutdamaging
provide the appropriate joint dimensions and configurations.
the sealant.
6.7 Substrate Cleaning Materials:
7.3 Extend all specimens until the separation between the
substrates provides the desired strain. Apply this strain at a
6.8 Primer (if needed).
minimum of 3 mm/h ( ⁄8 in./h).
6.9 Separators,toprovideaconstantstrainonthespecimen
7.4 When the specimens have reached their specified
whilst maintaining parallel bond surfaces.
extension, block the specimens with the appropriate separator
6.10 Deionized Water, or other specified liquid medium for
and remove from the extension device/machine. Do not re-
immersion
move separators for the duration of test.
6.11 Suitable Probe Type Measuring Device, capable of
7.5 Place
...
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