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ASTM D8133-17

(Test Method)

Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry

Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry

SIGNIFICANCE AND USE
5.1 Identification and Quantification of Phthalates—DBP, BBP, DEHP, DNOP, DINP and DIDP are required for regulated articles. Regulations include: EU—Directive 2005/84/EC, US—Consumer Product Safety Improvement Act of 2008 – section 108, Japan—Health, Labor and Welfare Ministry guideline No. 336 (2010). This test method provides a procedure to identify and quantify regulated phthalates in PVC.  
5.2 Other techniques successfully used to separate and identify phthalates in PVC include TD-GC/MS (ASTM D7823), GC/MS, HPLC/UV, HPLC/MS, FTIR, and GC/FID (flame ionization detector).
SCOPE
1.1 This test method provides a procedure to quantify six phthalates by solvent extraction of plasticized PVC articles followed by analysis of the extract by gas chromatography/mass spectrometry. The phthalates which are quantified are BBP, DBP, DEHP, DNOP, DINP, and DIDP.
Note 1: The method can be extended to other phthalates.  
1.2 Within the context of this method, “low level” is defined as 1000 ppm.  
1.3 The values in SI units are to be regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 2: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
31-Jul-2017
ICS
83.080.20 - Thermoplastic materials
Technical Committee
D20 - Plastics
Drafting Committee
D20.70 - Analytical Methods
Current Stage
Ref Project

Relations

Replaced By
ASTM D8133-18 - Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry
Effective Date
01-Nov-2018
Referred By
ASTM D7176-22 - Standard Specification for Non-Reinforced Polyvinyl Chloride (PVC) Geomembranes Used in Buried Applications
Effective Date
01-Aug-2017

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ASTM D8133-17 - Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass SpectrometryASTM D8133-17 - Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry
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ASTM D8133-17 - Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D8133 − 17
Standard Test Method for
Determination of Low Level, Regulated Phthalates in
Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas
1
Chromatography/Mass Spectrometry
This standard is issued under the fixed designation D8133; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope ers in Poly (Vinyl Chloride) (PVC) by Gas Chromatogra-
phy
1.1 This test method provides a procedure to quantify six
D7823 Test Method for Determination of Low Level, Regu-
phthalates by solvent extraction of plasticized PVC articles
lated Phthalates in Poly (Vinyl Chloride) Plastics by
followed by analysis of the extract by gas chromatography/
Thermal Desorption—Gas Chromatography/Mass Spec-
mass spectrometry. The phthalates which are quantified are
trometry
BBP, DBP, DEHP, DNOP, DINP, and DIDP.
D7993 Guide for Analyzing Complex Phthalates
NOTE 1—The method can be extended to other phthalates.
E177 Practice for Use of the Terms Precision and Bias in
1.2 Withinthecontextofthismethod,“lowlevel”isdefined ASTM Test Methods
E355 Practice for Gas Chromatography Terms and Relation-
as 1000 ppm.
ships
1.3 The values in SI units are to be regarded as standard.
E594 Practice for Testing Flame Ionization Detectors Used
1.4 This standard does not purport to address all of the
in Gas or Supercritical Fluid Chromatography
safety concerns, if any, associated with its use. It is the
E691 Practice for Conducting an Interlaboratory Study to
responsibility of the user of this standard to establish appro-
Determine the Precision of a Test Method
priate safety, health, and environmental practices and deter-
IEEE/ASTM SI-10 Practice for Use of the International
mine the applicability of regulatory limitations prior to use.
System of Units (SI), the Modernized Metric System
2.2 ASTM Adjuncts:ADJD7823-EA
NOTE 2—There is no known ISO equivalent to this standard.
Vinyl Plasticizer Library—Total Ion Chromatograms and
1.5 This international standard was developed in accor-
Mass Spectra
dance with internationally recognized principles on standard-
3
2.3 CPSC Standard:
ization established in the Decision on Principles for the
CPSC-CH-C1001–09.3 Standard Operating Procedure for
Development of International Standards, Guides and Recom-
Determination of Phthalates
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
3. Terminology
2. Referenced Documents
3.1 Definitions:
2
3.1.1 For definition of plastic terms used in this standard,
2.1 ASTM Standards:
see Terminologies D883 and D1600.
D883 Terminology Relating to Plastics
D1600 Terminology forAbbreviatedTerms Relating to Plas-
3.2 For units, symbols, and abbreviations used in this
tics
standard refer to Practices E594, E355,or IEEE/ASTM SI-10.
D3465 Test Method for Purity of Monomeric Plasticizers by
3.3 Compounds and Instrumentation:
Gas Chromatography
3.3.1 (DOA) Hexanedioic acid, 1,6-bis(2-ethylhexyl) ester
D7083 Practice for Determination of Monomeric Plasticiz-
CAS #103-23-1
3.3.2 (DINCH) 1,2-Cyclohexanedicarboxylic acid, dinonyl
1
This test method is under the jurisdiction ofASTM Committee D20 on Plastics ester, branched and linear CAS #474919-59-0
and is the direct responsibility of Subcommittee D20.70 on Analytical Methods.
3.3.3 (DBP) 1,2-Benzenedicarboxylic acid, 1,2-di-n-butyl
Current edition approved Aug. 1, 2017. Published November 2017. DOI:
ester CAS #84-74-2
10.1520/D8133-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available from U.S. Consumer Product Safety Commission (CPSC), 4330 East
the ASTM website. West Hwy., Bethesda, MD 20814, http://www.cpsc.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D8133 − 17
solvent and sample matrix).
3.3.4 (BBP) Benzyl butyl phthalate CAS #85-68-7
3.3.5 (DEHP) Bis(2-Ethyhexyl) Phthalate CAS #117-81-7
5. Significance and Use
3.3.6 (DNOP) Di(n-Octyl) phthalate CAS #117-84-0
3.3.7 (DINP) 1,2-Benzenedicarboxylic acid, di-C8-10-
5.1 Identification and Quantification of Phthalates—DBP,
branched alkyl esters, C9-rich (Jayflex) CAS #68515-48-0
BBP,DEHP,DNOP,DINPandDIDParerequiredforregulated
3.3.8 (DINP) 1,2-Benzenedicarboxylic acid, 1,2-diisononyl
articles. Regulations include: EU—Directive 2005/84/EC,
(Palatinol) CAS #28553-12-0
US—Consumer Product Safety Improvement Act of 2008 –
...

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