ASTM E2113-18

Standard Test Method for Length Change Calibration of Thermomechanical Analyzers

SIGNIFICANCE AND USE
5.1 Performance verification or calibration is essential to the accurate determination of quantitative dimension change measurements.  
5.2 This test method may be used for instrument performance validation, regulatory compliance, research and development and quality assurance purposes.
SCOPE
1.1 This test method describes calibration of the length change (deflection) measurement or thermal expansion of thermomechanical analyzers (TMAs) within the temperature range from –150 °C to 1000 °C using the thermal expansion of a suitable reference material.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

• Status: Historical
• Publication Date: 31-May-2018
• ICS: 83.080.01 - Plastics in general
• Technical Committee: E37 - Thermal Measurements
• Drafting Committee: E37.10 - Fundamental, Statistical and Mechanical Properties

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E2113 − 18
Standard Test Method for
1
Length Change Calibration of Thermomechanical Analyzers
This standard is issued under the fixed designation E2113; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Terminology
3.1 Specific technical terms used in this test method are
1.1 This test method describes calibration of the length
described in Terminologies E473, E1142, and E2161 including
change (deflection) measurement or thermal expansion of
calibration, Celsius, coeffıcient of linear thermal expansion,
thermomechanical analyzers (TMAs) within the temperature
Kelvin, reference material, repeatability, reproducibility, and
range from –150 °C to 1000 °C using the thermal expansion of
thermomechanical analysis.
a suitable reference material.
1.2 The values stated in SI units are to be regarded as
4. Summary of Test Method
standard. No other units of measurement are included in this
4.1 Thermomechanical analyzers (TMAs) or related devices
standard.
are commonly used to determine coefficient of linear thermal
1.3 This standard does not purport to address all of the
expansion of solid materials (for example, Test Method E831).
safety concerns, if any, associated with its use. It is the
The test specimen is heated at a linear rate over the temperature
responsibility of the user of this standard to establish appro-
range of interest and the change in length (dimension) is
priate safety, health, and environmental practices and deter-
electronically recorded.
mine the applicability of regulatory limitations prior to use.
4.2 Performance verification or calibration of the length
1.4 This international standard was developed in accor-
change measurement is needed to obtain accurate coefficient of
dance with internationally recognized principles on standard-
thermal expansion data.
ization established in the Decision on Principles for the
4.3 The thermal expansion of a reference material is re-
Development of International Standards, Guides and Recom-
corded using a thermomechanical analyzer. The recorded
mendations issued by the World Trade Organization Technical
thermal expansion is compared to the known value of the
Barriers to Trade (TBT) Committee.
reference material. The resultant ratio, a calibration coefficient,
may then be applied to the determination of unknown speci-
2. Referenced Documents
mens to obtain accurate results.
2
2.1 ASTM Standards:
5. Significance and Use
E473 Terminology Relating to Thermal Analysis and Rhe-
ology
5.1 Performance verification or calibration is essential to the
E831 Test Method for Linear Thermal Expansion of Solid
accurate determination of quantitative dimension change mea-
Materials by Thermomechanical Analysis
surements.
E1142 Terminology Relating to Thermophysical Properties
5.2 This test method may be used for instrument perfor-
E1363 Test Method for Temperature Calibration of Thermo-
mance validation, regulatory compliance, research and devel-
mechanical Analyzers
opment and quality assurance purposes.
E2161 Terminology Relating to Performance Validation in
Thermal Analysis and Rheology
6. Apparatus
6.1 Thermomechanical Analyzer (TMA)—The essential in-
strumentation required to provide the minimum thermome-
1
This test method is under the jurisdiction of ASTM Committee E37 on Thermal chanical analytical or thermodilatometric capability for this test
Measurements and is the direct responsibility of Subcommittee E37.10 on
method includes:
Fundamental, Statistical and Mechanical Properties.
6.1.1 A Rigid Specimen Holder, of inert, low expansivity
Current edition approved June 1, 2018. Published June 2018. Originally
-1 -1
material [<0.5 µm m °C ] to center the specimen in the
approved in 2000. Last previous edition approved in 2013 as E2113 – 13. DOI:
10.1520/E2113-18.
furnace and to fix the specimen to mechanical ground.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
6.1.2 A Rigid Expansion Probe, of inert, low expansivity
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
-1 -1
material [<0.5 µm m °C ] which contacts the specimen with
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. an applicable compressive or tensile force.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E2113 − 18
6.1.3 A Sensing Element, linear over a minimum of 2 mm, 6.1.9 A Data Collection Device, to provide a means of
to measure the displacement
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2113 − 13 E2113 − 18
Standard Test Method for
1
Length Change Calibration of Thermomechanical Analyzers
This standard is issued under the fixed designation E2113; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method describes calibration of the length change (deflection) measurement or thermal expansion of
thermomechanical analyzers (TMAs) within the temperature range from –150 °C to 1000°C 1000 °C using the thermal expansion
of a suitable reference material.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This test method differs from ISO 11359-1 by providing an alternative calibration procedure.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
E473 Terminology Relating to Thermal Analysis and Rheology
E831 Test Method for Linear Thermal Expansion of Solid Materials by Thermomechanical Analysis
E1142 Terminology Relating to Thermophysical Properties
E1363 Test Method for Temperature Calibration of Thermomechanical Analyzers
1
This test method is under the jurisdiction of ASTM Committee E37 on Thermal Measurements and is the direct responsibility of Subcommittee E37.10 on Fundamental,
Statistical and Mechanical Properties.
Current edition approved Aug. 1, 2013June 1, 2018. Published August 2013June 2018. Originally approved in 2000. Last previous edition approved in 20092013 as
E2113 – 09.E2113 – 13. DOI: 10.1520/E2113-13.10.1520/E2113-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E2113 − 18
E2161 Terminology Relating to Performance Validation in Thermal Analysis and Rheology
2.2 Other Standards:
3
ISO 11359-1 Plastics—Thermomechanical analysis (TMA)—Part 1: General principles
3. Terminology
3.1 Specific technical terms used in this test method are described in Terminologies E473, E1142, and E2161 includeincluding
calibration, Celsius, coeffıcient of linear thermal expansion, Kelvin, reference material, repeatability, reproducibility, and
thermomechanical analysis.
4. Summary of Test Method
4.1 Thermomechanical analyzers (TMAs) or related devices are commonly used to determine coefficient of linear thermal
expansion of solid materials (for example, Test Method E831). The test specimen is heated at a linear rate over the temperature
range of interest and the change in length (dimension) is electronically recorded.
4.2 Performance verification or calibration of the length change measurement is needed to obtain accurate coefficient of thermal
expansion data.
4.3 The thermal expansion of a reference material is recorded using a thermomechanical analyzer. The recorded thermal
expansion is compared to the known value of the reference material. The resultant ratio, a calibration coefficient, may then be
applied to the determination of unknown specimens to obtain accurate results.
5. Significance and Use
5.1 Performance verification or calibration is essential to the accurate determination of quantitative dimension change
measurements.
5.2 This test method may be used for instrument performance validation, regulatory compliance, research and development and
quality assurance purposes.
6. Apparatus
6.1 Thermomechanical Analyzer (TMA)—The essential instrumentation required to provide the minimum thermomechanical
analytical or thermodilat
...