iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM G33-99(2020)

(Practice)

Standard Practice for Recording Data from Atmospheric Corrosion Tests of Metallic-Coated Steel Specimens

Standard Practice for Recording Data from Atmospheric Corrosion Tests of Metallic-Coated Steel Specimens

SIGNIFICANCE AND USE
3.1 Use of this practice will maximize the benefits to be gained from atmospheric testing of metallic-coated steel. It will also aid in comparing results from one location to another where similar tests have been conducted.
SCOPE
1.1 This practice covers a procedure for recording data of atmospheric corrosion tests of metallic-coated steel specimens. Its objective is the assurance of (1) complete identification of materials before testing, (2) objective reporting of material appearance during visual inspections, and (3) adequate photographic, micrographic, and chemical laboratory examinations at specific stages of deterioration, and at the end of the tests.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Oct-2020
ICS
77.060 - Corrosion of metals
Technical Committee
G01 - Corrosion of Metals
Drafting Committee
G01.04 - Corrosion of Metals in Natural Atmospheric and Aqueous Environments
Current Stage
Ref Project

Relations

Refers
ASTM E376-19 - Standard Practice for Measuring Coating Thickness by Magnetic-Field or Eddy Current (Electromagnetic) Testing Methods
Effective Date
01-May-2019
Refers
ASTM E376-17 - Standard Practice for Measuring Coating Thickness by Magnetic-Field or Eddy Current (Electromagnetic) Testing Methods
Effective Date
01-Nov-2017
Refers
ASTM G46-94(2013) - Standard Guide for Examination and Evaluation of Pitting Corrosion
Effective Date
01-May-2013
Refers
ASTM E376-11 - Standard Practice for Measuring Coating Thickness by Magnetic-Field or Eddy-Current (Electromagnetic) Testing Methods
Effective Date
01-Jul-2011
Refers
ASTM E376-06 - Standard Practice for Measuring Coating Thickness by Magnetic-Field or Eddy-Current (Electromagnetic) Examination Methods
Effective Date
01-Dec-2006
Refers
ASTM G46-94(2005) - Standard Guide for Examination and Evaluation of Pitting Corrosion
Effective Date
01-May-2005
Refers
ASTM E376-03 - Standard Practice for Measuring Coating Thickness by Magnetic-Field or Eddy-Current (Electromagnetic) Examination Methods
Effective Date
10-Mar-2003
Refers
ASTM G46-94(1999) - Standard Guide for Examination and Evaluation of Pitting Corrosion
Effective Date
10-Jan-1999
Refers
ASTM E376-96 - Standard Practice for Measuring Coating Thickness by Magnetic-Field or Eddy-Current (Electromagnetic) Test Methods
Effective Date
10-Dec-1996

Buy Standard

ASTM G33-99(2020) - Standard Practice for Recording Data from Atmospheric Corrosion Tests of Metallic-Coated Steel SpecimensASTM G33-99(2020) - Standard Practice for Recording Data from Atmospheric Corrosion Tests of Metallic-Coated Steel Specimens
PreviousNext
Standard
ASTM G33-99(2020) - Standard Practice for Recording Data from Atmospheric Corrosion Tests of Metallic-Coated Steel Specimens
English language
3 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)


This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: G33 − 99 (Reapproved 2020)
Standard Practice for
Recording Data from Atmospheric Corrosion Tests of
Metallic-Coated Steel Specimens
This standard is issued under the fixed designation G33; the number immediately following the designation indicates the year of original
adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Significance and Use
1.1 This practice covers a procedure for recording data of 3.1 Use of this practice will maximize the benefits to be
atmospheric corrosion tests of metallic-coated steel specimens. gainedfromatmospherictestingofmetallic-coatedsteel.Itwill
Its objective is the assurance of (1) complete identification of also aid in comparing results from one location to another
materials before testing, (2) objective reporting of material where similar tests have been conducted.
appearance during visual inspections, and (3) adequate
4. Data to be Recorded Before Testing
photographic, micrographic, and chemical laboratory examina-
4.1 Material Characteristics:
tions at specific stages of deterioration, and at the end of the
4.1.1 Coating and Basis Metal:
tests.
4.1.1.1 Type of coating (zinc, aluminum, nickel-chromium,
1.2 This standard does not purport to address all of the
and so forth).
safety concerns, if any, associated with its use. It is the
4.1.1.2 Method of application (hot-dip, electroplated,
responsibility of the user of this standard to establish appro-
electroless, mechanical plated, and so forth),
priate safety, health, and environmental practices and deter-
(1) Area coated (if not 100 % of surface),
mine the applicability of regulatory limitations prior to use.
(2) Pre-treatment (basis metal: flux, sand-blast, and so
1.3 This international standard was developed in accor-
forth), and
dance with internationally recognized principles on standard-
(3) Post-treatment (heating, sealing, and so forth),
ization established in the Decision on Principles for the
4.1.1.3 Coating composition,
Development of International Standards, Guides and Recom-
4.1.1.4 Basis metal product.
mendations issued by the World Trade Organization Technical
(1) Basis metal composition, and
Barriers to Trade (TBT) Committee.
(2) Metallurgical history prior to coating (if any).
4.1.1.5 Chemical treatment of coating.
2. Referenced Documents
4.1.1.6 Black and white photograph of typical surface area
2.1 ASTM Standards:
illustrating texture (1:1 magnification ratio).
A90/A90M Test Method for Weight [Mass] of Coating on
4.1.1.7 Micrograph of typical coating cross section (magni-
Iron and Steel Articles with Zinc or Zinc-Alloy Coatings
fication and etchant to be specified).
A428/A428M Test Method for Weight [Mass] of Coating on
4.1.2 Coating Weight and Thickness:
Aluminum-Coated Iron or Steel Articles
4.1.2.1 Weight by stripping. (See Test Method A90/A90M
E376 Practice for Measuring Coating Thickness by
or A428/A428M.)
Magnetic-Field or Eddy Current (Electromagnetic) Test-
(1) Method.
ing Methods
4.1.2.2 Measured Thickness.
G46 Guide for Examination and Evaluation of Pitting Cor-
(1) Method (for example, eddy current, back scattering,
rosion
magnetic),
NOTE 1—If a magnetic type instrument is used, refer to Practice E376.
(2) Number of determinations,
This practice is under the jurisdiction of ASTM Committee G01 on Corrosion
(3) Mean,
of Metals and is the direct responsibility of Subcommittee G01.04 on Corrosion of
Metals in Natural Atmospheric and Aqueous Environments.
(4) Standard deviation, and
Current edition approved Nov. 1, 2020. Published November 2020. Originally
(5) Range (spread of determinations).
approved in 1972. Last previous edition approved in 2015 as G33–99(2015). DOI:
10.1520/G0033-99R20.
4.2 Specimen Identification and Exposure Location:
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
4.2.1 Marking (method to be specified).
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.2.2 Specimen position in test area.
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. 4.2.3 Angle of exposure from horizontal.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
G33 − 99 (2020)
4.2.4 Direction of specimen faces. 5.3.3.1 The following terms should be used to describe
4.2.5 Location of test area. surface irregularities:
(1) Blistering—Any separation of the coating from the
4.2.6 Description of test area (location of nearby industry,
substrate not accompanied by peeling,
ocean,andsoforth,andrecordeddataonspecificcontaminants
(2) Peeling—Separation of the coating from the substrate
where possible).
initiating at an edge of or cut in the coating and causing an
4.2.7 Exposure starting date:
exposure of the substrate,
4.2.7.1 Weather conditions (for example, bright, cloudy,
(3) Cracking—Any fissure in the coating other than a
sunshine, rain, and so forth),
mechanical cut,
4.3 Specimen Characteristics:
(4) Checking—Cracking in a cross-hatch manner resem-
4.3.1 Description (sheet, wire, hardware, and so forth).
bling mud cracking,
4.3.2 Specimen size:
(5) Rust—Corrosion products of iron characterized by
4.3.2.1 Specimen surface dimensions.
rough, reddish brown particles. Rust is always rough to the
4.3.2.2 Gage or thickness.
touch,
4.3.3 Specimen weight (when applicable).
(6) Tubercles—Knob-like protrusions of corrosion
4.3.4 Edge condition (to be specified).
products,
4.3.5 Specimen
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM G49-85(2023)e1(Practice)
Standard Practice for Preparation and Use of Direct Tension Stress-Corrosion Test Specimens

SIGNIFICANCE AND USE
4.1 Axially loaded tension specimens provide one of the most versatile methods of performing a stress-corrosion test because of the flexibility permitted in the choice of type and size of test specimen, stressing procedures, and range of stress levels.  
4.2 The uniaxial stress system is simple; hence, this test method is often used for studies of stress-corrosion mechanisms. This type of test is amenable to the simultaneous exposure of unstressed specimens (no applied load) with stressed specimens and subsequent tension testing to distinguish between the effects of true stress corrosion and mechanical overload (2). Additional considerations in regard to the significance of the test results and their interpretation are given in Sections 6 and 10.  
4.3 Wide variations in test results may be obtained for a given material and specimen orientation with different specimen sizes and stressing procedures. This consideration is significant especially in the standardization of a test procedure for interlaboratory comparisons or quality control.
SCOPE
1.1 This practice covers procedures for designing, preparing, and using ASTM standard tension test specimens for investigating susceptibility to stress-corrosion cracking. Axially loaded specimens may be stressed quantitatively with equipment for application of either a constant load, constant strain, or with a continuously increasing strain.  
1.2 Tension test specimens are adaptable for testing a wide variety of product forms as well as parts joined by welding, riveting, or various other methods.  
1.3 The exposure of specimens in a corrosive environment is treated only briefly because other standards are being prepared to deal with this aspect. Meanwhile, the investigator is referred to Practices G35, G36, G37, and G44, and to ASTM Special Technical Publication 425 (1).2  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM G87-02(2023)(Practice)
Standard Practice for Conducting Moist SO2 Tests

SIGNIFICANCE AND USE
3.1 Moist air containing sulfur dioxide quickly produces easily visible corrosion on many metals in a form resembling that occurring in industrial environments. It is therefore a test medium well suited to detect pores or other sources of weakness in protective coatings and deficiencies in corrosion resistance associated with unsuitable alloy composition or treatments.  
3.2 The results obtained in the test should not be regarded as a general guide to the corrosion resistance of the tested materials in all environments where these materials may be used. Performance of different materials in the test should only be taken as a general guide to the relative corrosion resistance of these materials in moist SO2 service.
SCOPE
1.1 This practice covers the apparatus and procedure to be used in conducting qualitative assessment tests in accordance with the requirements of material or product specifications by means of specimen exposure to condensed moisture containing sulfur dioxide.  
1.2 The exposure conditions may be varied to suit particular requirements and this practice includes provisions for use of different concentrations of sulfur dioxide and for tests either running continuously or in cycles of alternate exposure to the sulfur dioxide containing atmosphere and to the ambient atmosphere.  
1.3 The variant of the test to be used, the exposure period required, the type of test specimen, and the criteria of failure are not prescribed by this practice. Such details are provided in appropriate material and product purchase specifications.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  For a specific warning statement, see 4.3.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM G35-23(Practice)
Standard Practice for Determining the Susceptibility of Stainless Steels and Related Nickel-Chromium-Iron Alloys to Stress-Corrosion Cracking in Polythionic Acids

SIGNIFICANCE AND USE
4.1 Polythionic acids are chemically described as H2SxO6, where x is usually 3, 4, or 5 (1)3 though can be more than 50 (2). These acid environments provide a way of evaluating the resistance of stainless steels and related alloys to intergranular stress corrosion cracking. Failure is accelerated by the presence of increasing amounts of intergranular precipitate. Results for the polythionic acid test have not been correlated exactly with those of intergranular corrosion tests (Test Methods G28). Also, this test may not be relevant to stress corrosion cracking in chlorides or caustic environments.  
4.2 The polythionic acid environment may produce areas of shallow intergranular attack in addition to the more localized and deeper cracking mode of attack. Examination of failed specimens is necessary to confirm that failure occurred by cracking rather than mechanical failure of reduced sections.
SCOPE
1.1 This practice covers procedures for preparing and conducting the polythionic acid test at room temperature, 22 °C to 25 °C (72 °F to 77 °F), to determine the relative susceptibility of stainless steels or other related materials (nickel-chromium-iron alloys) to intergranular stress corrosion cracking.  
1.2 This practice can be used to evaluate stainless steels or other materials in the “as received” condition or after being subjected to high-temperature service, 482 °C to 815 °C (900 °F to 1500 °F), for prolonged periods of time.  
1.3 This practice can be applied to wrought products, castings, and weld metal of stainless steels or other related materials to be used in environments containing sulfur or sulfides. Other materials capable of being sensitized can also be tested in accordance with this test.  
1.4 This practice may be used with a variety of stress corrosion test specimens, surface finishes, and methods of applying stress.  
1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For more specific precautionary statements, see Section 7.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM G102-23(Practice)
Standard Practice for Calculation of Corrosion Rates and Related Information from Electrochemical Measurements

SIGNIFICANCE AND USE
3.1 Electrochemical corrosion rate measurements often provide results in terms of electrical current. Although the conversion of these current values into mass loss rates or penetration rates is based on Faraday’s Law, the calculations can be complicated for alloys and metals with elements having multiple valence values. This practice is intended to provide guidance in calculating mass loss and penetration rates for such alloys. Some typical values of equivalent weights for a variety of metals and alloys are provided.  
3.2 Electrochemical corrosion rate measurements may provide results in terms of electrical resistance. The conversion of these results to either mass loss or penetration rates requires additional electrochemical information. Some approaches for estimating this information are given.  
3.3 Use of this practice will aid in producing more consistent corrosion rate data from electrochemical results. This will make results from different studies more comparable and minimize calculation errors that may occur in transforming electrochemical results to corrosion rate values.
SCOPE
1.1 This practice covers the providing of guidance in converting the results of electrochemical measurements to rates of uniform corrosion. Calculation methods for converting corrosion current density values to either mass loss rates or average penetration rates are given for most engineering alloys. In addition, some guidelines for converting polarization resistance values to corrosion rates are provided.  
1.2 The values stated in SI units are to be regarded as standard. Other units of measurement are included in this standard because of their usage.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    8 pages
    English language
    sale 15% off
  • Standard
    8 pages
    English language
    sale 15% off
ASTM
ASTM G123-00(2022)e1(Test Method)
Standard Test Method for Evaluating Stress-Corrosion Cracking of Stainless Alloys with Different Nickel Content in Boiling Acidified Sodium Chloride Solution

SIGNIFICANCE AND USE
5.1 This test method is designed to compare alloys and may be used as one method of screening materials prior to service. In general, this test method is more useful for stainless steels than the boiling magnesium chloride test of Practice G36. The boiling magnesium chloride test cracks materials with the nickel levels found in relatively resistant austenitic and duplex stainless steels, thus making comparisons and evaluations for many service environments difficult.  
5.2 This test method is intended to simulate cracking in water, especially cooling waters that contain chloride. It is not intended to simulate cracking that occurs at high temperatures (greater than 200 °C or 390 °F) with chloride or hydroxide.
Note 1: The degree of cracking resistance found in full-immersion tests may not be indicative of that for some service conditions comprising exposure to the water-line or in the vapor phase where chlorides may concentrate.  
5.3 Correlation with service experience should be obtained when possible. Different chloride environments may rank materials in a different order.  
5.4 In interlaboratory testing, this test method cracked annealed UNS S30400 and S31600 but not more resistant materials, such as annealed duplex stainless steels or higher nickel alloys, for example, UNS N08020 (for example 20Cb-33 stainless). These more resistant materials are expected to crack when exposed to Practice G36 as U-bends. Materials which withstand this sodium chloride test for a longer period than UNS S30400 or S31600 may be candidates for more severe service applications.  
5.5 The repeatability and reproducibility data from Section 12 and Appendix X1 must be considered prior to use. Interlaboratory variation in results may be expected as occurs with many corrosion tests. Acceptance criteria are not part of this test method and if needed are to be negotiated by the user and the producer.
SCOPE
1.1 This test method covers a procedure for conducting stress-corrosion cracking tests in an acidified boiling sodium chloride solution. This test method is performed in 25 % (by mass) sodium chloride acidified to pH 1.5 with phosphoric acid. This test method is concerned primarily with the test solution and glassware, although a specific style of U-bend test specimen is suggested.  
1.2 This test method is designed to provide better correlation with chemical process industry experience for stainless steels than the more severe boiling magnesium chloride test of Practice G36. Some stainless steels which have provided satisfactory service in many environments readily crack in Practice G36, but have not cracked during interlaboratory testing (see Section 12) using this sodium chloride test method.  
1.3 This boiling sodium chloride test method was used in an interlaboratory test program to evaluate wrought stainless steels, including duplex (ferrite-austenite) stainless and an alloy with up to about 33 % nickel. It may also be employed to evaluate these types of materials in the cast or welded conditions.  
1.4 This test method detects major effects of composition, heat treatment, microstructure, and stress on the susceptibility of materials to chloride stress-corrosion cracking. Small differences between samples such as heat-to-heat variations of the same grade are not likely to be detected.  
1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 8.  
1.7 This international standard was developed in accordance with internationally recogni...

  • Standard
    10 pages
    English language
    sale 15% off
ASTM
ASTM G30-22(Practice)
Standard Practice for Making and Using U-Bend Stress-Corrosion Test Specimens

SIGNIFICANCE AND USE
5.1 The U-bend specimen may be used for any metal alloy sufficiently ductile to be formed into the U-shape without mechanically cracking. The specimen is most easily made from strip or sheet but can be machined from plate, bar, castings, or weldments; wire specimens may be used also.  
5.2 Since the U-bend usually contains large amounts of elastic and plastic strain, it provides one of the most severe tests available for smooth (as opposed to notched or precracked) stress-corrosion test specimens. The stress conditions are not usually known and a wide range of stresses exist in a single stressed specimen. The specimen is therefore unsuitable for studying the effects of different applied stresses on stress-corrosion cracking or for studying variables that have only a minor effect on cracking. The advantage of the U-bend specimen is that it is simple and economical to make and use. It is most useful for detecting large differences between the stress-corrosion cracking resistance of (a) different metals in the same environment, (b) one metal in different metallurgical conditions in the same environment, or (c) one metal in several environments.
SCOPE
1.1 This practice covers procedures for making and using U-bend specimens for the evaluation of stress-corrosion cracking in metals. The U-bend specimen is generally a rectangular strip that is bent 180° around a predetermined radius and maintained in this constant strain condition during the stress-corrosion test. Bends slightly less than or greater than 180° are sometimes used. Typical U-bend configurations showing several different methods of maintaining the applied stress are shown in Fig. 1.  
FIG. 1 Typical Stressed U-bends  
1.2 U-bend specimens usually contain both elastic and plastic strain. In some cases (for example, very thin sheet or small diameter wire) it is possible to form a U-bend and produce only elastic strain. However, bent-beam (Practice G39 or direct tension (Practice G49)) specimens are normally used to study stress-corrosion cracking of strip or sheet under elastic strain only.  
1.3 This practice is concerned only with the test specimen and not the environmental aspects of stress-corrosion testing, which are discussed elsewhere (1)2 and in Practices G35, G36, G37, G41, G44, G103 and Test Method G123.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM G111-21a(Guide)
Standard Guide for Corrosion Tests in High Temperature or High Pressure Environment, or Both

SIGNIFICANCE AND USE
5.1 Autoclave tests are commonly used to evaluate the corrosion performance of metallic and non-metallic materials under simulated HP and HTHP service conditions. Examples of service environments in which HP and HTHP corrosion tests have been used include chemical processing, petroleum production and refining, food processing, pressurized cooling water, electric power systems, and aerospace propulsion.  
5.2 For the applications of corrosion testing listed in 5.1, the service environment involves handling corrosive and potentially hazardous media under conditions of high pressure or high temperature, or both. The temperature and pressure, among other parameters, usually drive the composition and properties of the aqueous phase and, hence, the severity of the corrosion process. Consequently, the laboratory evaluation of corrosion severity cannot be performed in conventional low pressure glassware without making potentially invalid assumptions as to the potential effects of high temperature and pressure on corrosion severity.  
5.3 Therefore, there is a substantial need to provide standardized methods by which corrosion testing can be performed under HP and HTHP. In many cases, however, the standards used for exposure of specimens in conventional low-pressure glassware experiments cannot be followed due to the limitations of access, volume, and visibility arising from the construction of high-pressure test cells. This guide refers to existing corrosion standards and practices, as applicable, and then goes further in areas in which specific guidelines for performing HP and HTHP corrosion testing are needed.
SCOPE
1.1 This guide covers procedures, specimens, and equipment for conducting laboratory corrosion tests on metallic materials under conditions of high pressure (HP) or the combination of high temperature and high pressure (HTHP). See 3.2 for definitions of high pressure and temperature.  
1.2 The procedures and methods in this guide are applicable for conducting mass loss corrosion, localized corrosion, and electrochemical tests as well as for use in environmentally induced cracking tests that need to be conducted under HP or HTHP conditions.  
1.3 The primary purpose for this guide is to promote consistency of corrosion test results. Furthermore, this guide will aid in the comparison of corrosion data between laboratories or testing organizations that utilize different equipment.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    8 pages
    English language
    sale 15% off
  • Guide
    8 pages
    English language
    sale 15% off
ASTM
ASTM G46-21(Guide)
Standard Guide for Examination and Evaluation of Pitting Corrosion

SIGNIFICANCE AND USE
4.1 It is important to be able to determine the extent of pitting, either in a service application in which it is necessary to predict the remaining life in a metal structure, or in laboratory test programs that are used to select the most pitting-resistant materials for service. The purpose of the study is crucial in determining the appropriate examination and evaluation steps.  
4.2 Some typical purposes of laboratory tests include, but are not limited to, evaluating performance of alloys, determining whether an alloy is resistant to the environment, evaluating how environmental conditions including corrosion inhibitor affect or prevent pitting, and evaluating whether a lot of metal is sufficiently resistant for its use in a particular application or environment.  
4.3 Some typical purposes of field studies include, but are not limited to, determining if pits are likely to grow and cause leak or release of process fluid, and assisting a determination of whether to replace or repair damage from pits (remaining life assessment).
SCOPE
1.1 This guide covers the selection of procedures that can be used in the examination and evaluation of pitted metals. These procedures include both nondestructive and destructive approaches.  
1.2 The procedures covered in this guide include those that may be used in laboratory evaluations of corroded metal specimens and field examinations and inspections.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3.1 Exception—In X1.2.1, mils per year (MPY) are regarded as standard for the target corrosion rate.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    13 pages
    English language
    sale 15% off
  • Guide
    13 pages
    English language
    sale 15% off
ASTM
ASTM G37-98(2021)(Practice)
Standard Practice for Use of Mattsson's Solution of pH 7.2 to Evaluate the Stress-Corrosion Cracking Susceptibility of Copper-Zinc Alloys

SIGNIFICANCE AND USE
4.1 This test environment is believed to give an accelerated ranking of the relative or absolute degree of stress-corrosion cracking susceptibility for different brasses. It has been found to correlate well with the corresponding service ranking in environments that cause stress-corrosion cracking which is thought to be due to the combined presence of traces of moisture and ammonia vapor. The extent to which the accelerated ranking correlates with the ranking obtained after long-term exposure to environments containing corrodents other than ammonia is not at present known. Examples of such environments may be severe marine atmospheres (Cl−), severe industrial atmospheres (predominantly SO2), and super-heated ammonia-free steam.  
4.2 It is not possible at present to specify any particular time to failure (defined on the basis of any particular failure criteria) in pH 7.2 Mattsson’s solution that corresponds to a distinction between acceptable and unacceptable stress-corrosion behavior in brass alloys. Such particular correlations must be determined individually.  
4.3 Mattsson's solution of pH 7.2 may also cause stress independent general and intergranular corrosion of brasses to some extent. This leads to the possibility of confusing stress-corrosion failures with mechanical failures induced by corrosion-reduced net cross sections. This danger is particularly great with small cross section specimens, high applied stress levels, long exposure periods and stress-corrosion resistant alloys. Careful metallographic examination is recommended for correct diagnosis of the cause of failure. Alternatively, unstressed control specimens may be exposed to evaluate the extent to which stress independent corrosion degrades mechanical properties.
SCOPE
1.1 This practice covers the preparation and use of Mattsson’s solution of pH 7.2 as an accelerated stress-corrosion cracking test environment for brasses (copper-zinc base alloys). The variables (to the extent that these are known at present) that require control are described together with possible means for controlling and standardizing these variables.  
1.2 This practice is recommended only for brasses (copper-zinc base alloys). The use of this test environment is not recommended for other copper alloys since the results may be erroneous, providing completely misleading rankings. This is particularly true of alloys containing aluminum or nickel as deliberate alloying additions.  
1.3 This practice is intended primarily where the test objective is to determine the relative stress-corrosion cracking susceptibility of different brasses under the same or different stress conditions or to determine the absolute degree of stress corrosion cracking susceptibility, if any, of a particular brass or brass component under one or more specific stress conditions. Other legitimate test objectives for which this test solution may be used do, of course, exist. The tensile stresses present may be known or unknown, applied or residual. The practice may be applied to wrought brass products or components, brass castings, brass weldments, and so forth, and to all brasses. Strict environmental test conditions are stipulated for maximum assurance that apparent variations in stress-corrosion susceptibility are attributable to real variations in the material being tested or in the tensile stress level and not to environmental variations.  
1.4 This practice relates solely to the preparation and control of the test environment. No attempt is made to recommend surface preparation or finish, or both, as this may vary with the test objectives. Similarly, no attempt is made to recommend particular stress-corrosion test specimen configurations or methods of applying the stress. Test specimen configurations that may be used are referenced in Practice G30 and STP 425.2  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included ...

  • Standard
    4 pages
    English language
    sale 15% off
ASTM
ASTM G39-99(2021)(Practice)
Standard Practice for Preparation and Use of Bent-Beam Stress-Corrosion Test Specimens

SIGNIFICANCE AND USE
5.1 The bent-beam specimen is designed for determining the stress-corrosion behavior of alloy sheets and plates in a variety of environments. The bent-beam specimens are designed for testing at stress levels below the elastic limit of the alloy. For testing in the plastic range, U-bend specimens should be employed (see Practice G30). Although it is possible to stress bent-beam specimens into the plastic range, the stress level cannot be calculated for plastically-stressed three- and four-point loaded specimens as well as the double-beam specimens. Therefore, the use of bent-beam specimens in the plastic range is not recommended for general use.
SCOPE
1.1 This practice covers procedures for designing, preparing, and using bent-beam stress-corrosion specimens.  
1.2 Different specimen configurations are given for use with different product forms, such as sheet or plate. This practice is applicable to specimens of any metal that are stressed to levels less than the elastic limit of the material, and therefore, the applied stress can be accurately calculated or measured (see Note 1). Stress calculations by this practice are not applicable to plastically stressed specimens.  
Note 1: It is the nature of these practices that only the applied stress can be calculated. Since stress-corrosion cracking is a function of the total stress, for critical applications and proper interpretation of results, the residual stress (before applying external stress) or the total elastic stress (after applying external stress) should be determined by appropriate nondestructive methods, such as X-ray diffraction (1).2  
1.3 Test procedures are given for stress-corrosion testing by exposure to gaseous and liquid environments.  
1.4 The bent-beam test is best suited for flat product forms, such as sheet, strip, and plate. For plate material the bent-beam specimen is more difficult to use because more rugged specimen holders must be built to accommodate the specimens. A double-beam modification of a four-point loaded specimen to utilize heavier materials is described in 10.5.  
1.5 The exposure of specimens in a corrosive environment is treated only briefly since other practices deal with this aspect, for example, Practices D1141, G30, G36, G44, G50, and G85. The experimenter is referred to ASTM Special Technical Publication 425 (2).  
1.6 The bent-beam practice generally constitutes a constant strain (deflection) test. Once cracking has initiated, the state of stress at the tip of the crack as well as in uncracked areas has changed, and therefore, the known or calculated stress or strain values discussed in this practice apply only to the state of stress existing before initiation of cracks.  
1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.8  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (For more specific safety hazard information see Section 7 and 12.1.)  
1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    8 pages
    English language
    sale 15% off